Co-delivery of rapamycin- and piperine-loaded polymeric nanoparticles for breast cancer treatment

P-glycoprotein (P-gp) efflux is the major cause of multidrug resistance (MDR) in tumors when using anticancer drugs, moreover, poor bioavailability of few drugs is also due to P-gp efflux in the gut. Rapamycin (RPM) is in the clinical trials for breast cancer treatment, but its P-gp substrate proper...

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Vydáno v:Drug delivery Ročník 23; číslo 7; s. 2608 - 2616
Hlavní autoři: Katiyar, Sameer S., Muntimadugu, Eameema, Rafeeqi, Towseef Amin, Domb, Abraham J., Khan, Wahid
Médium: Journal Article
Jazyk:angličtina
Vydáno: England Taylor & Francis 01.09.2016
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ISSN:1071-7544, 1521-0464
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Abstract P-glycoprotein (P-gp) efflux is the major cause of multidrug resistance (MDR) in tumors when using anticancer drugs, moreover, poor bioavailability of few drugs is also due to P-gp efflux in the gut. Rapamycin (RPM) is in the clinical trials for breast cancer treatment, but its P-gp substrate property leads to poor oral bioavailability and efficacy. The objective of this study is to formulate and evaluate nanoparticles of RPM, along with a chemosensitizer (piperine, PIP) for improved oral bioavailability and efficacy. Poly(d,l-lactide-co-glycolide) (PLGA) was selected as polymer as it has moderate MDR reversal activity, which may provide additional benefits. The nanoprecipitation method was used to prepare PLGA nanoparticles with particle size below 150 nm, loaded with both drugs (RPM and PIP). Prepared nanoparticles showed sustained in vitro drug release for weeks, with initial release kinetics of zero order with non-Fickian transport, subsequently followed by Higuchi kinetics with Fickian diffusion. An everted gut sac method was used to study the effect of P-gp efflux on drug transport. This reveals that the uptake of the RPM (P-gp substrate) has been increased in the presence of chemosensitizer. Pharmacokinetic studies showed better absorption profile of RPM from polymeric nanoparticles compared to its suspension counterpart and improved bioavailability of 4.8-folds in combination with a chemosensitizer. An in vitro cell line study indicates higher efficacy of nanoparticles compared to free drug solution. Results suggest that the use of a combination of PIP with RPM nanoparticles would be a promising approach in the treatment of breast cancer.
AbstractList P-glycoprotein (P-gp) efflux is the major cause of multidrug resistance (MDR) in tumors when using anticancer drugs, moreover, poor bioavailability of few drugs is also due to P-gp efflux in the gut. Rapamycin (RPM) is in the clinical trials for breast cancer treatment, but its P-gp substrate property leads to poor oral bioavailability and efficacy. The objective of this study is to formulate and evaluate nanoparticles of RPM, along with a chemosensitizer (piperine, PIP) for improved oral bioavailability and efficacy. Poly(d,l-lactide-co-glycolide) (PLGA) was selected as polymer as it has moderate MDR reversal activity, which may provide additional benefits. The nanoprecipitation method was used to prepare PLGA nanoparticles with particle size below 150 nm, loaded with both drugs (RPM and PIP). Prepared nanoparticles showed sustained in vitro drug release for weeks, with initial release kinetics of zero order with non-Fickian transport, subsequently followed by Higuchi kinetics with Fickian diffusion. An everted gut sac method was used to study the effect of P-gp efflux on drug transport. This reveals that the uptake of the RPM (P-gp substrate) has been increased in the presence of chemosensitizer. Pharmacokinetic studies showed better absorption profile of RPM from polymeric nanoparticles compared to its suspension counterpart and improved bioavailability of 4.8-folds in combination with a chemosensitizer. An in vitro cell line study indicates higher efficacy of nanoparticles compared to free drug solution. Results suggest that the use of a combination of PIP with RPM nanoparticles would be a promising approach in the treatment of breast cancer.
Author Khan, Wahid
Rafeeqi, Towseef Amin
Muntimadugu, Eameema
Domb, Abraham J.
Katiyar, Sameer S.
Author_xml – sequence: 1
  givenname: Sameer S.
  surname: Katiyar
  fullname: Katiyar, Sameer S.
  organization: Department of Pharmaceutics, National Institute of Pharmaceutical Education and Research (NIPER)
– sequence: 2
  givenname: Eameema
  surname: Muntimadugu
  fullname: Muntimadugu, Eameema
  organization: Department of Pharmaceutics, National Institute of Pharmaceutical Education and Research (NIPER)
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  givenname: Towseef Amin
  surname: Rafeeqi
  fullname: Rafeeqi, Towseef Amin
  organization: Central Research Institute of Unani Medicine (CRIUM)
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  givenname: Abraham J.
  surname: Domb
  fullname: Domb, Abraham J.
  email: avid@ekmd.huji.ac.il
  organization: Faculty of Medicine, School of Pharmacy, The Hebrew University of Jerusalem, Jerusalem College of Engineering (JCE)
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  givenname: Wahid
  surname: Khan
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  email: wahid@niperhyd.ac.in
  organization: Department of Pharmaceutics, National Institute of Pharmaceutical Education and Research (NIPER)
BackLink https://www.ncbi.nlm.nih.gov/pubmed/26036652$$D View this record in MEDLINE/PubMed
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Keywords PLGA
nanoparticles
piperine
Breast cancer
P-glycoprotein efflux
oral bioavailability
chemosensitizer
rapamycin
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Snippet P-glycoprotein (P-gp) efflux is the major cause of multidrug resistance (MDR) in tumors when using anticancer drugs, moreover, poor bioavailability of few...
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SubjectTerms Alkaloids - administration & dosage
Alkaloids - chemistry
Alkaloids - pharmacology
Antineoplastic Agents - administration & dosage
Antineoplastic Agents - chemistry
Antineoplastic Agents - pharmacology
ATP-Binding Cassette, Sub-Family B, Member 1 - chemistry
ATP-Binding Cassette, Sub-Family B, Member 1 - metabolism
ATP-Binding Cassette, Sub-Family B, Member 1 - pharmacology
Benzodioxoles - administration & dosage
Benzodioxoles - chemistry
Benzodioxoles - pharmacology
Biological Availability
Breast cancer
Breast Neoplasms - drug therapy
Cell Line, Tumor
chemosensitizer
Drug Resistance, Multiple
Drug Resistance, Neoplasm - drug effects
Female
Humans
Lactic Acid - chemistry
nanoparticles
Nanoparticles - chemistry
oral bioavailability
P-glycoprotein efflux
Piperidines - administration & dosage
Piperidines - chemistry
Piperidines - pharmacology
piperine
PLGA
Polyglycolic Acid - chemistry
Polyunsaturated Alkamides - administration & dosage
Polyunsaturated Alkamides - chemistry
Polyunsaturated Alkamides - pharmacology
rapamycin
Sirolimus - administration & dosage
Sirolimus - chemistry
Sirolimus - pharmacology
Title Co-delivery of rapamycin- and piperine-loaded polymeric nanoparticles for breast cancer treatment
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