SI-ATRP grafting of polymers from polydopamine-modified cellulose nanocrystals

This work reports on the possibility of using polydopamine (PDA) as a tool to immobilize bromoisobutyryl moieties at the surface of cellulose nanocrystals (CNCs) and initiate Surface Intitiated Atom Transfer Radical Polymerization (SI-ATRP) reactions from these sites. Two different strategies based...

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Veröffentlicht in:	Carbohydrate polymers Jg. 341; S. 122346
Hauptverfasser:	Hou, Yelin, Zhang, Zhen, Harrisson, Simon, Sèbe, Gilles
Format:	Journal Article
Sprache:	Englisch
Veröffentlicht:	England Elsevier Ltd 01.10.2024 Elsevier
Schlagworte:	bromination cellulose Cellulose nanocrystals Chemical Sciences crystal structure dopamine nanocrystals Polydopamine polymerization Polymers Polymethyl methacrylate Polystyrene SI-ATRP styrene Polydopamine Polystyrene Cellulose nanocrystals Polymethyl methacrylate SI-ATRP polymethyl methacrylate polydopamine polystyrene
ISSN:	0144-8617, 1879-1344, 1879-1344
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Abstract	This work reports on the possibility of using polydopamine (PDA) as a tool to immobilize bromoisobutyryl moieties at the surface of cellulose nanocrystals (CNCs) and initiate Surface Intitiated Atom Transfer Radical Polymerization (SI-ATRP) reactions from these sites. Two different strategies based on i) the stepwise modification of the CNCs with dopamine (DA) and α-bromoisobutyryl bromide (BiBB) (Protocol 1) and ii) the one-step treatment of the CNCs with a mixture of DA and BiBB-modified DA (Protocol 2), were compared. Only the CNC particles treated according to Protocol 1 guaranteed efficient anchoring of the SI-ATRP initiating sites in our experimental conditions (with limited impact on the CNCs crystalline structure), the coated layer being leached out by certain solvents in the case of Protocol 2. The brominated particles displaying the best performances were subsequently tested as potential ATRP macroinitiators, using methyl methacrylate (MMA) and styrene (St) as model monomers. Polymer-grafted particles were successfully obtained, with a grafting density twice as high for Sty as for MMA, demonstrating the validity of this strategy. [Display omitted]
AbstractList	This work reports on the possibility of using polydopamine (PDA) as a tool to immobilize bromoisobutyryl moieties at the surface of cellulose nanocrystals (CNCs) and initiate Surface Intitiated Atom Transfer Radical Polymerization (SI-ATRP) reactions from these sites. Two different strategies based on i) the stepwise modification of the CNCs with dopamine (DA) and α-bromoisobutyryl bromide (BiBB) (Protocol 1) and ii) the one-step treatment of the CNCs with a mixture of DA and BiBB-modified DA (Protocol 2), were compared. Only the CNC particles treated according to Protocol 1 guaranteed efficient anchoring of the SI-ATRP initiating sites in our experimental conditions (with limited impact on the CNCs crystalline structure), the coated layer being leached out by certain solvents in the case of Protocol 2. The brominated particles displaying the best performances were subsequently tested as potential ATRP macroinitiators, using methyl methacrylate (MMA) and styrene (St) as model monomers. Polymer-grafted particles were successfully obtained, with a grafting density twice as high for Sty as for MMA, demonstrating the validity of this strategy.This work reports on the possibility of using polydopamine (PDA) as a tool to immobilize bromoisobutyryl moieties at the surface of cellulose nanocrystals (CNCs) and initiate Surface Intitiated Atom Transfer Radical Polymerization (SI-ATRP) reactions from these sites. Two different strategies based on i) the stepwise modification of the CNCs with dopamine (DA) and α-bromoisobutyryl bromide (BiBB) (Protocol 1) and ii) the one-step treatment of the CNCs with a mixture of DA and BiBB-modified DA (Protocol 2), were compared. Only the CNC particles treated according to Protocol 1 guaranteed efficient anchoring of the SI-ATRP initiating sites in our experimental conditions (with limited impact on the CNCs crystalline structure), the coated layer being leached out by certain solvents in the case of Protocol 2. The brominated particles displaying the best performances were subsequently tested as potential ATRP macroinitiators, using methyl methacrylate (MMA) and styrene (St) as model monomers. Polymer-grafted particles were successfully obtained, with a grafting density twice as high for Sty as for MMA, demonstrating the validity of this strategy. This work reports on the possibility of using polydopamine (PDA) as a tool to immobilize bromoisobutyryl moieties at the surface of cellulose nanocrystals (CNCs) and initiate Surface Intitiated Atom Transfer Radical Polymerization (SI-ATRP) reactions from these sites. Two different strategies based on i) the stepwise modification of the CNCs with dopamine (DA) and α-bromoisobutyryl bromide (BiBB) (Protocol 1) and ii) the one-step treatment of the CNCs with a mixture of DA and BiBB-modified DA (Protocol 2), were compared. Only the CNC particles treated according to Protocol 1 guaranteed efficient anchoring of the SI-ATRP initiating sites in our experimental conditions (with limited impact on the CNCs crystalline structure), the coated layer being leached out by certain solvents in the case of Protocol 2. The brominated particles displaying the best performances were subsequently tested as potential ATRP macroinitiators, using methyl methacrylate (MMA) and styrene (St) as model monomers. Polymer-grafted particles were successfully obtained, with a grafting density twice as high for Sty as for MMA, demonstrating the validity of this strategy. This work reports on the possibility of using polydopamine (PDA) as a tool to immobilize bromoisobutyryl moieties at the surface of cellulose nanocrystals (CNCs) and initiate Surface Intitiated Atom Transfer Radical Polymerization (SI-ATRP) reactions from these sites. Two different strategies based on i) the stepwise modification of the CNCs with dopamine (DA) and α-bromoisobutyryl bromide (BiBB) (Protocol 1) and ii) the one-step treatment of the CNCs with a mixture of DA and BiBB-modified DA (Protocol 2), were compared. Only the CNC particles treated according to Protocol 1 guaranteed efficient anchoring of the SI-ATRP initiating sites in our experimental conditions (with limited impact on the CNCs crystalline structure), the coated layer being leached out by certain solvents in the case of Protocol 2. The brominated particles displaying the best performances were subsequently tested as potential ATRP macroinitiators, using methyl methacrylate (MMA) and styrene (St) as model monomers. Polymer-grafted particles were successfully obtained, with a grafting density twice as high for Sty as for MMA, demonstrating the validity of this strategy. [Display omitted]
ArticleNumber	122346
Author	Harrisson, Simon Sèbe, Gilles Hou, Yelin Zhang, Zhen
Author_xml	– sequence: 1 givenname: Yelin surname: Hou fullname: Hou, Yelin organization: Univ. Bordeaux, CNRS, Bordeaux INP, LCPO, UMR 5629, F-33600 Pessac, France – sequence: 2 givenname: Zhen surname: Zhang fullname: Zhang, Zhen email: zhangzhen@m.scnu.edu.cn organization: SCNU-TUE Joint Lab of Device Integrated Responsive Materials (DIRM), Institute of Electronic Paper Displays, South China Academy of Advanced Optoelectronics, South China Normal University, Guangzhou 510006, China – sequence: 3 givenname: Simon surname: Harrisson fullname: Harrisson, Simon organization: Univ. Bordeaux, CNRS, Bordeaux INP, LCPO, UMR 5629, F-33600 Pessac, France – sequence: 4 givenname: Gilles surname: Sèbe fullname: Sèbe, Gilles email: gilles.sebe@u-bordeaux.fr organization: Univ. Bordeaux, CNRS, Bordeaux INP, LCPO, UMR 5629, F-33600 Pessac, France
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CitedBy_id	crossref_primary_10_1016_j_ijbiomac_2025_146354 crossref_primary_10_1002_eem2_70105 crossref_primary_10_1016_j_ijbiomac_2025_142482 crossref_primary_10_1016_j_reactfunctpolym_2024_106137 crossref_primary_10_1016_j_biomaterials_2025_123404 crossref_primary_10_1002_adma_202501542 crossref_primary_10_1080_09205063_2025_2457265 crossref_primary_10_1016_j_lwt_2025_117904 crossref_primary_10_1016_j_ijbiomac_2024_139379 crossref_primary_10_1021_acsapm_5c02861 crossref_primary_10_1016_j_carbpol_2025_123731 crossref_primary_10_1016_j_ijbiomac_2024_136497
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Keywords	Polydopamine Polystyrene Cellulose nanocrystals Polymethyl methacrylate SI-ATRP polymethyl methacrylate polydopamine polystyrene
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Snippet	This work reports on the possibility of using polydopamine (PDA) as a tool to immobilize bromoisobutyryl moieties at the surface of cellulose nanocrystals...
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StartPage	122346
SubjectTerms	bromination cellulose Cellulose nanocrystals Chemical Sciences crystal structure dopamine nanocrystals Polydopamine polymerization Polymers Polymethyl methacrylate Polystyrene SI-ATRP styrene
Title	SI-ATRP grafting of polymers from polydopamine-modified cellulose nanocrystals
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