A green sample preparation method for the determination of bisphenols in honeys
•Structural analogues are substituting BPA in production of some consumer products > micro-QuEChERS extraction and the analysis UHPLC-MS/MS was developed and validated > the method was then tested on algerian and tunisian honey samples. Bisphenol A is the most studied compound due to its adver...
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| Vydáno v: | Green Analytical Chemistry Ročník 5; s. 100059 |
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| Hlavní autoři: | , , , , , , , , |
| Médium: | Journal Article |
| Jazyk: | angličtina |
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Elsevier B.V
01.06.2023
Elsevier |
| Témata: | |
| ISSN: | 2772-5774, 2772-5774 |
| On-line přístup: | Získat plný text |
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| Abstract | •Structural analogues are substituting BPA in production of some consumer products > micro-QuEChERS extraction and the analysis UHPLC-MS/MS was developed and validated > the method was then tested on algerian and tunisian honey samples.
Bisphenol A is the most studied compound due to its adverse effects on human health and is one of the most widely used products in contact materials worldwide. However, in recent years, due to stringent restrictions on the use of BPA, structural analogues are substituting BPA in the production of some consumer products. A method based on the Micro-QuEChERS technique and ultra-high performance liquid chromatography coupled to tandem mass spectrometry (UHPLC-MS/MS) was proposed, derived from a previous method based on standard QuEChERS and HPLC-MS/MS. The proposed method was compared with the previous method using the analytical Eco-scale as a verification tool. The results highlight that the proposed method achieved a metric value of 79 points, higher than the required value of 75 points for 'excellent green analysis'. The method was then tested on Algerian and Tunisian honey samples of different floral origins. The results showed that the developed method was satisfactory in terms of recovery, sensitivity, and analysis time, showing good applicability even in a complex matrix such as honey. Low levels of contamination of residues of bisphenol-analogues were found and it can therefore be concluded that the samples analysed do not pose a health risk to consumers with regard to these compounds.
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| AbstractList | Bisphenol A is the most studied compound due to its adverse effects on human health and is one of the most widely used products in contact materials worldwide. However, in recent years, due to stringent restrictions on the use of BPA, structural analogues are substituting BPA in the production of some consumer products. A method based on the Micro-QuEChERS technique and ultra-high performance liquid chromatography coupled to tandem mass spectrometry (UHPLC-MS/MS) was proposed, derived from a previous method based on standard QuEChERS and HPLC-MS/MS. The proposed method was compared with the previous method using the analytical Eco-scale as a verification tool. The results highlight that the proposed method achieved a metric value of 79 points, higher than the required value of 75 points for 'excellent green analysis'. The method was then tested on Algerian and Tunisian honey samples of different floral origins. The results showed that the developed method was satisfactory in terms of recovery, sensitivity, and analysis time, showing good applicability even in a complex matrix such as honey. Low levels of contamination of residues of bisphenol-analogues were found and it can therefore be concluded that the samples analysed do not pose a health risk to consumers with regard to these compounds. •Structural analogues are substituting BPA in production of some consumer products > micro-QuEChERS extraction and the analysis UHPLC-MS/MS was developed and validated > the method was then tested on algerian and tunisian honey samples. Bisphenol A is the most studied compound due to its adverse effects on human health and is one of the most widely used products in contact materials worldwide. However, in recent years, due to stringent restrictions on the use of BPA, structural analogues are substituting BPA in the production of some consumer products. A method based on the Micro-QuEChERS technique and ultra-high performance liquid chromatography coupled to tandem mass spectrometry (UHPLC-MS/MS) was proposed, derived from a previous method based on standard QuEChERS and HPLC-MS/MS. The proposed method was compared with the previous method using the analytical Eco-scale as a verification tool. The results highlight that the proposed method achieved a metric value of 79 points, higher than the required value of 75 points for 'excellent green analysis'. The method was then tested on Algerian and Tunisian honey samples of different floral origins. The results showed that the developed method was satisfactory in terms of recovery, sensitivity, and analysis time, showing good applicability even in a complex matrix such as honey. Low levels of contamination of residues of bisphenol-analogues were found and it can therefore be concluded that the samples analysed do not pose a health risk to consumers with regard to these compounds. [Display omitted] |
| ArticleNumber | 100059 |
| Author | Litrenta, Federica Lo Turco, Vincenzo Benameur, Qada Albergamo, Ambrogina Di Bella, Giuseppa Sgrò, Benedetta Potortì, Angela Giorgia Ben Mansour, Hedi Beltifa, Asma |
| Author_xml | – sequence: 1 givenname: Angela Giorgia surname: Potortì fullname: Potortì, Angela Giorgia organization: Department of Biomedical, Dental and Morphological and Functional Imaging Sciences (Biomorf), University of Messina, Polo Universitario dell'Annunziata, Messina 98168, Italy – sequence: 2 givenname: Federica surname: Litrenta fullname: Litrenta, Federica organization: Department of Biomedical, Dental and Morphological and Functional Imaging Sciences (Biomorf), University of Messina, Polo Universitario dell'Annunziata, Messina 98168, Italy – sequence: 3 givenname: Benedetta surname: Sgrò fullname: Sgrò, Benedetta organization: Department of Biomedical, Dental and Morphological and Functional Imaging Sciences (Biomorf), University of Messina, Polo Universitario dell'Annunziata, Messina 98168, Italy – sequence: 4 givenname: Giuseppa orcidid: 0000-0001-8103-6942 surname: Di Bella fullname: Di Bella, Giuseppa email: gdibella@unime.it organization: Department of Biomedical, Dental and Morphological and Functional Imaging Sciences (Biomorf), University of Messina, Polo Universitario dell'Annunziata, Messina 98168, Italy – sequence: 5 givenname: Ambrogina surname: Albergamo fullname: Albergamo, Ambrogina organization: Department of Biomedical, Dental and Morphological and Functional Imaging Sciences (Biomorf), University of Messina, Polo Universitario dell'Annunziata, Messina 98168, Italy – sequence: 6 givenname: Hedi surname: Ben Mansour fullname: Ben Mansour, Hedi organization: Research Unit of Analysis and Process Applied on the Environment (APAE-UR17ES32) - Higher Institute of Applied Sciences and Technology, Universirty of Monastir, Mahdia, Tunisia – sequence: 7 givenname: Asma surname: Beltifa fullname: Beltifa, Asma organization: Research Unit of Analysis and Process Applied on the Environment (APAE-UR17ES32) - Higher Institute of Applied Sciences and Technology, Universirty of Monastir, Mahdia, Tunisia – sequence: 8 givenname: Qada surname: Benameur fullname: Benameur, Qada organization: Department of Agronomy, Faculty of Nature and Life Sciences, University Abdelhamid Ibn Badis of Mostaganem, Algeria – sequence: 9 givenname: Vincenzo surname: Lo Turco fullname: Lo Turco, Vincenzo organization: Department of Biomedical, Dental and Morphological and Functional Imaging Sciences (Biomorf), University of Messina, Polo Universitario dell'Annunziata, Messina 98168, Italy |
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| Keywords | Green analysis Honey samples Bisphenol analogues Micro extraction UHPL-MS/MS |
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