Efficiency of combined MA-XRF and CXRF to give nondestructive insights about changes of a historical painting

Historical paintings with important iconographical changes represent an analytical challenge. Considering the case study of a fifteenth-century French painting studied during its restoration, the efficiency of a combined noninvasive approach of two-dimensional scanning macro-X-ray fluorescence imagi...

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Vydané v:	European physical journal plus Ročník 138; číslo 1; s. 46
Hlavní autori:	Tapia, José, Eveno, Myriam, Calligaro, Thomas, Pichon, Laurent, Laval, Eric, Ravaud, Elisabeth, Reiche, Ina
Médium:	Journal Article
Jazyk:	English
Vydavateľské údaje:	Berlin/Heidelberg Springer Berlin Heidelberg 19.01.2023 Springer Nature B.V Springer
Predmet:	Applied and Technical Physics Atomic Chemical Sciences Complex Systems Composition Condensed Matter Physics Cross-sections Depth profiling Efficiency Electron microscopes Energy Focus Point on Scientific Research in Cultural Heritage 2022 Humanities and Social Sciences Laboratories Mathematical and Computational Physics Molecular Optical and Plasma Physics Optics Physics Physics and Astronomy Radiation Regular Article Scanning electron microscopy Sensors Stratigraphy Theoretical X ray fluorescence analysis X ray imagery X-ray fluorescence France paints confocal micro-XRF pigments scanning macro-XRF elemental imaging stratigraphy
ISSN:	2190-5444, 2190-5444
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Abstract	Historical paintings with important iconographical changes represent an analytical challenge. Considering the case study of a fifteenth-century French painting studied during its restoration, the efficiency of a combined noninvasive approach of two-dimensional scanning macro-X-ray fluorescence imaging (MA-XRF) and a laboratory-based depth-resolved confocal micro-X-ray fluorescence (CXRF) is discussed. Large chemical maps of several elements were obtained by MA-XRF, enabling the identification of zones of interest representing changes in the painting composition. In these areas, depth profiles were measured with CXRF, allowing to evidence overlaying paint layers. The advantages of this technique are that it can give direct information on the stratigraphy of paint layers in a nondestructive way and can reduce the sampling needed, as well as increase the locations analyzed (in our study twenty-two depth-resolved scans). These results complement information obtained by scanning electron microscopy coupled with an energy-dispersive X-ray analyzing system (SEM–EDX) on three cross-sectional samples taken in the areas of interest. Additionally, the three cross sections of the painting were studied by CXRF lateral scans (y) in order to evaluate the efficiency of the CXRF analyses against SEM–EDX. The study shows the benefits of the combination of MA-XRF and CXRF for analyzing painting compositions, as such a high number of cross sections would have been impossible to sample. From an art-historical and conservation perspective, this combined study provides an understanding of the original painting’s paint sequence and its later retouches, helping to make informed conservation treatment decisions. Graphic Abstract
AbstractList	Historical paintings with important iconographical changes represent an analytical challenge. Considering the case study of a fifteenth-century French painting studied during its restoration, the efficiency of a combined noninvasive approach of two-dimensional scanning macro-X-ray fluorescence imaging (MA-XRF) and a laboratory-based depth-resolved confocal micro-X-ray fluorescence (CXRF) is discussed. Large chemical maps of several elements were obtained by MA-XRF, enabling the identification of zones of interest representing changes in the painting composition. In these areas, depth profiles were measured with CXRF, allowing to evidence overlaying paint layers. The advantages of this technique are that it can give direct information on the stratigraphy of paint layers in a nondestructive way and can reduce the sampling needed, as well as increase the locations analyzed (in our study twenty-two depth-resolved scans). These results complement information obtained by scanning electron microscopy coupled with an energy-dispersive X-ray analyzing system (SEM–EDX) on three cross-sectional samples taken in the areas of interest. Additionally, the three cross sections of the painting were studied by CXRF lateral scans (y) in order to evaluate the efficiency of the CXRF analyses against SEM–EDX. The study shows the benefits of the combination of MA-XRF and CXRF for analyzing painting compositions, as such a high number of cross sections would have been impossible to sample. From an art-historical and conservation perspective, this combined study provides an understanding of the original painting’s paint sequence and its later retouches, helping to make informed conservation treatment decisions. Graphic Abstract Historical paintings with important iconographical changes represent an analytical challenge. Considering the case study of a fifteenth-century French painting studied during its restoration, the efficiency of a combined noninvasive approach of two-dimensional scanning macro-X-ray fluorescence imaging (MA-XRF) and a laboratory-based depth-resolved confocal micro-X-ray fluorescence (CXRF) is discussed. Large chemical maps of several elements were obtained by MA-XRF, enabling the identification of zones of interest representing changes in the painting composition. In these areas, depth profiles were measured with CXRF, allowing to evidence overlaying paint layers. The advantages of this technique are that it can give direct information on the stratigraphy of paint layers in a nondestructive way and can reduce the sampling needed, as well as increase the locations analyzed (in our study twenty-two depth-resolved scans). These results complement information obtained by scanning electron microscopy coupled with an energy-dispersive X-ray analyzing system (SEM–EDX) on three cross-sectional samples taken in the areas of interest. Additionally, the three cross sections of the painting were studied by CXRF lateral scans (y) in order to evaluate the efficiency of the CXRF analyses against SEM–EDX. The study shows the benefits of the combination of MA-XRF and CXRF for analyzing painting compositions, as such a high number of cross sections would have been impossible to sample. From an art-historical and conservation perspective, this combined study provides an understanding of the original painting’s paint sequence and its later retouches, helping to make informed conservation treatment decisions. Graphic Abstract
ArticleNumber	46
Author	Reiche, Ina Calligaro, Thomas Ravaud, Elisabeth Laval, Eric Tapia, José Pichon, Laurent Eveno, Myriam
Author_xml	– sequence: 1 givenname: José surname: Tapia fullname: Tapia, José organization: Chimie ParisTech-CNRS, IRCP, UMR8247, PSL Research University – sequence: 2 givenname: Myriam surname: Eveno fullname: Eveno, Myriam organization: Chimie ParisTech-CNRS, IRCP, UMR8247, PSL Research University, Centre de recherche et de restauration des musées de France, C2RMF – sequence: 3 givenname: Thomas surname: Calligaro fullname: Calligaro, Thomas organization: Chimie ParisTech-CNRS, IRCP, UMR8247, PSL Research University, Centre de recherche et de restauration des musées de France, C2RMF, Fédération de Recherche FR3506 CNRS New AGLAE, Centre de recherche et de restauration des musées de France (C2RMF) – sequence: 4 givenname: Laurent surname: Pichon fullname: Pichon, Laurent organization: Centre de recherche et de restauration des musées de France, C2RMF, Fédération de Recherche FR3506 CNRS New AGLAE, Centre de recherche et de restauration des musées de France (C2RMF) – sequence: 5 givenname: Eric surname: Laval fullname: Laval, Eric organization: Centre de recherche et de restauration des musées de France, C2RMF – sequence: 6 givenname: Elisabeth surname: Ravaud fullname: Ravaud, Elisabeth organization: Chimie ParisTech-CNRS, IRCP, UMR8247, PSL Research University, Centre de recherche et de restauration des musées de France, C2RMF – sequence: 7 givenname: Ina orcidid: 0000-0002-9897-6620 surname: Reiche fullname: Reiche, Ina email: ina.reiche@chimieparistech.psl.eu organization: Chimie ParisTech-CNRS, IRCP, UMR8247, PSL Research University, Fédération de Recherche FR3506 CNRS New AGLAE, Centre de recherche et de restauration des musées de France (C2RMF)
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Cites_doi	10.1080/00393630.2016.1142059 10.1016/S0168-583X(03)01321-1 10.1002/xrs.897 10.1007/s00339-016-0457-1 10.1016/j.talanta.2012.02.010 10.1007/s00339-011-6698-0 10.1007/s00339-015-9522-4 10.1186/s40494-014-0017-y 10.1007/s00339-015-9428-1 10.1016/j.sab.2006.12.002 10.1039/B916974A 10.1039/B915912F 10.1016/j.radphyschem.2016.02.031 10.1039/C2JA30157A 10.1016/j.apradiso.2014.07.019 10.1063/1.4744934 10.1039/C4JA00387J 10.1016/j.sab.2004.10.012
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Snippet	Historical paintings with important iconographical changes represent an analytical challenge. Considering the case study of a fifteenth-century French painting...
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SubjectTerms	Applied and Technical Physics Atomic Chemical Sciences Complex Systems Composition Condensed Matter Physics Cross-sections Depth profiling Efficiency Electron microscopes Energy Focus Point on Scientific Research in Cultural Heritage 2022 Humanities and Social Sciences Laboratories Mathematical and Computational Physics Molecular Optical and Plasma Physics Optics Physics Physics and Astronomy Radiation Regular Article Scanning electron microscopy Sensors Stratigraphy Theoretical X ray fluorescence analysis X ray imagery X-ray fluorescence
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Title	Efficiency of combined MA-XRF and CXRF to give nondestructive insights about changes of a historical painting
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