Environmental-friendly yellow pigment based on Tb and M (M=Ca or Ba) co-doped Y2O3

A yellow inorganic ceramic pigment with general formula Y1.86−xMxTb0.14O3−x/2 (M=Ca and/or Zn) with x=0.06, 0.32 and 0.64 were synthesized by a modified Pechini method. XRD, SEM and HRTEM/EDX analysis showed the formation of solid solution at 1300°C when x=0.06 and 0.32. The best b* yellow coordinat...

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Published in:	Journal of the European Ceramic Society Vol. 33; no. 15-16; pp. 3359 - 3368
Main Authors:	De la Luz, Verónica, Prades, Marta, Beltrán, Héctor, Cordoncillo, Eloisa
Format:	Journal Article
Language:	English
Published:	Elsevier Ltd 01.12.2013
Subjects:	Ceramic yellow pigment Ceramics Color Colour Environmental friendly Glazes Glazing Lanthanide Pechini method Pigments Solid solutions Yttrium oxide Zinc Lanthanide Yttrium oxide Ceramic yellow pigment Pechini method Environmental friendly
ISSN:	0955-2219, 1873-619X
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Abstract	A yellow inorganic ceramic pigment with general formula Y1.86−xMxTb0.14O3−x/2 (M=Ca and/or Zn) with x=0.06, 0.32 and 0.64 were synthesized by a modified Pechini method. XRD, SEM and HRTEM/EDX analysis showed the formation of solid solution at 1300°C when x=0.06 and 0.32. The best b* yellow coordinates were obtained for Ca and Zn co-doped Y1.86Tb0.14O3 samples. The intensity of the yellow colour in the samples is related to the presence of Tb4+ ions. Samples with higher concentration of Tb4+ ions lead to a better yellow colour. The chemical stability of these pigments was determinate in an industrial glaze. The glazing tests indicated that the powder samples with x=0.06 and 0.32 fired at 1300°C were stable in the glaze. These results make it a potential candidate for environmental friendly yellow ceramic pigment to be used in applications such as pigment for glazes or inkjet printers.
AbstractList	A yellow inorganic ceramic pigment with general formula Y1.86−xMxTb0.14O3−x/2 (M=Ca and/or Zn) with x=0.06, 0.32 and 0.64 were synthesized by a modified Pechini method. XRD, SEM and HRTEM/EDX analysis showed the formation of solid solution at 1300°C when x=0.06 and 0.32. The best b* yellow coordinates were obtained for Ca and Zn co-doped Y1.86Tb0.14O3 samples. The intensity of the yellow colour in the samples is related to the presence of Tb4+ ions. Samples with higher concentration of Tb4+ ions lead to a better yellow colour. The chemical stability of these pigments was determinate in an industrial glaze. The glazing tests indicated that the powder samples with x=0.06 and 0.32 fired at 1300°C were stable in the glaze. These results make it a potential candidate for environmental friendly yellow ceramic pigment to be used in applications such as pigment for glazes or inkjet printers. A yellow inorganic ceramic pigment with the general formula Y1.86-xMxTb0.14O3-x/2 (M = Ca and/or Zn) with x = 0.06, 0.32 and 0.64 was synthesised by a modified Pechini method. XRD, SEM and HRTEM/EDX showed the formation of a solid solution at 1300 C for x = 0.06 and 0.32. The best b* yellow coordinates were obtained for Ca and Zn co-doped Y1.86Tb0.14O3 samples. The intensity of the yellow colour in the samples was related to the presence of Tb4+ ions. Samples with higher concentrations of Tb4+ ions led to a better yellow colour. The chemical stability of these pigments was determinate in an industrial glaze. The glazing tests showed that the powders with x = 0.06 and 0.32 fired at 1300 C were stable in the glaze. These results make this pigment a potential candidate for environmentally friendly yellow ceramic pigments for applications in glazes for ceramic tiles or ink jet printing.
Author	Prades, Marta Beltrán, Héctor De la Luz, Verónica Cordoncillo, Eloisa
Author_xml	– sequence: 1 givenname: Verónica surname: De la Luz fullname: De la Luz, Verónica email: delaluz@uji.es – sequence: 2 givenname: Marta surname: Prades fullname: Prades, Marta email: mprades@uji.es – sequence: 3 givenname: Héctor surname: Beltrán fullname: Beltrán, Héctor email: mir@uji.es – sequence: 4 givenname: Eloisa surname: Cordoncillo fullname: Cordoncillo, Eloisa email: cordonci@uji.es
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Snippet	A yellow inorganic ceramic pigment with general formula Y1.86−xMxTb0.14O3−x/2 (M=Ca and/or Zn) with x=0.06, 0.32 and 0.64 were synthesized by a modified... A yellow inorganic ceramic pigment with the general formula Y1.86-xMxTb0.14O3-x/2 (M = Ca and/or Zn) with x = 0.06, 0.32 and 0.64 was synthesised by a modified...
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SubjectTerms	Ceramic yellow pigment Ceramics Color Colour Environmental friendly Glazes Glazing Lanthanide Pechini method Pigments Solid solutions Yttrium oxide Zinc
Title	Environmental-friendly yellow pigment based on Tb and M (M=Ca or Ba) co-doped Y2O3
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