In situ DRIFTS investigation on the SCR of NO with NH3 over V2O5 catalyst supported by activated semi-coke
At the reaction temperature (200°C), the active sites for NO adsorption and oxidation are mostly provided by ASC and NH3 is mainly absorbed on the Lewis acid sites provided by V2O5. •High NO conversion rate with excellent selectivity to N2 is obtained when 3wt.% V2O5 is loaded onto ASC for NO remova...
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| Vydané v: | Applied surface science Ročník 313; s. 660 - 669 |
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| Hlavní autori: | , , , , , |
| Médium: | Journal Article |
| Jazyk: | English |
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Amsterdam
Elsevier B.V
15.09.2014
Elsevier |
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| ISSN: | 0169-4332 |
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| Abstract | At the reaction temperature (200°C), the active sites for NO adsorption and oxidation are mostly provided by ASC and NH3 is mainly absorbed on the Lewis acid sites provided by V2O5.
•High NO conversion rate with excellent selectivity to N2 is obtained when 3wt.% V2O5 is loaded onto ASC for NO removal.•Active sites for the adsorption–oxidation of NO and NH3 are proved to be respectively provided by ASC and V2O5.•Both Lewis and Brønsted acid sites for NH3 adsorption co-exist on the V2O5/ASC catalyst and the Lewis acid sites play the leading role at the reaction temperature.•The SCR reaction pathways over the V2O5/ASC catalyst involve the coordinated ammonia with gaseous NO (E–R mechanism) as well as the adsorbed NO2 (L–H mechanism).
3wt.% of V2O5 is loaded onto the activated semi-coke (V2O5/ASC) via impregnation method and used for low temperature selective catalytic reduction (SCR) of NOx with NH3. The prepared V2O5/ASC catalyst yields an over 90% NO conversion rate with excellent N2 selectivity at 250°C with a space velocity of 12,000h−1. The adsorption state of different species and reaction behaviors under various conditions are systematically examined with in situ diffuse reflectance infrared Fourier transform spectroscopy (in situ DRIFTS). It is evidenced that NH3 and NO are absorbed on different active sites over the V2O5/ASC catalyst. At the reaction temperature (200°C) in this study, NH3 is mainly absorbed on the Lewis acid sites provided by V2O5, and NO is mainly absorbed on the active sites originated from the support ASC. In addition, the NH3-SCR process takes place according to two pathways, including reaction between the coordinated NH3 and gaseous NO (E–R mechanism), and reaction between the absorbed NO2 and coordinated NH3 (L–H mechanism). The latter one plays a primary role for the improved low-temperature SCR performance of V2O5/ASC catalyst. |
|---|---|
| AbstractList | 3wt.% of V2O5 is loaded onto the activated semi-coke (V2O5/ASC) via impregnation method and used for low temperature selective catalytic reduction (SCR) of NO x with NH3. The prepared V2O5/ASC catalyst yields an over 90% NO conversion rate with excellent N2 selectivity at 250 degree C with a space velocity of 12,000h-1. The adsorption state of different species and reaction behaviors under various conditions are systematically examined with in situ diffuse reflectance infrared Fourier transform spectroscopy (in situ DRIFTS). It is evidenced that NH3 and NO are absorbed on different active sites over the V2O5/ASC catalyst. At the reaction temperature (200 degree C) in this study, NH3 is mainly absorbed on the Lewis acid sites provided by V2O5, and NO is mainly absorbed on the active sites originated from the support ASC. In addition, the NH3-SCR process takes place according to two pathways, including reaction between the coordinated NH3 and gaseous NO (E-R mechanism), and reaction between the absorbed NO2 and coordinated NH3 (L-H mechanism). The latter one plays a primary role for the improved low-temperature SCR performance of V2O5/ASC catalyst. At the reaction temperature (200°C), the active sites for NO adsorption and oxidation are mostly provided by ASC and NH3 is mainly absorbed on the Lewis acid sites provided by V2O5. •High NO conversion rate with excellent selectivity to N2 is obtained when 3wt.% V2O5 is loaded onto ASC for NO removal.•Active sites for the adsorption–oxidation of NO and NH3 are proved to be respectively provided by ASC and V2O5.•Both Lewis and Brønsted acid sites for NH3 adsorption co-exist on the V2O5/ASC catalyst and the Lewis acid sites play the leading role at the reaction temperature.•The SCR reaction pathways over the V2O5/ASC catalyst involve the coordinated ammonia with gaseous NO (E–R mechanism) as well as the adsorbed NO2 (L–H mechanism). 3wt.% of V2O5 is loaded onto the activated semi-coke (V2O5/ASC) via impregnation method and used for low temperature selective catalytic reduction (SCR) of NOx with NH3. The prepared V2O5/ASC catalyst yields an over 90% NO conversion rate with excellent N2 selectivity at 250°C with a space velocity of 12,000h−1. The adsorption state of different species and reaction behaviors under various conditions are systematically examined with in situ diffuse reflectance infrared Fourier transform spectroscopy (in situ DRIFTS). It is evidenced that NH3 and NO are absorbed on different active sites over the V2O5/ASC catalyst. At the reaction temperature (200°C) in this study, NH3 is mainly absorbed on the Lewis acid sites provided by V2O5, and NO is mainly absorbed on the active sites originated from the support ASC. In addition, the NH3-SCR process takes place according to two pathways, including reaction between the coordinated NH3 and gaseous NO (E–R mechanism), and reaction between the absorbed NO2 and coordinated NH3 (L–H mechanism). The latter one plays a primary role for the improved low-temperature SCR performance of V2O5/ASC catalyst. |
| Author | Yan, Zheng Chen, Yan Zhang, Zuotai Wang, Xidong Wang, Jinping Liu, Lili |
| Author_xml | – sequence: 1 givenname: Jinping surname: Wang fullname: Wang, Jinping organization: Beijing Key Laboratory for Solid Waste Utilization and Management, College of Engineering, Peking University, Beijing 100871, China – sequence: 2 givenname: Zheng surname: Yan fullname: Yan, Zheng organization: Liaoning Key Laboratory of Clean Energy and Institute of Clean Energy and Environmental Engineering, College of Energy and Environment, Shenyang Aerospace University, Liaoning 110034, China – sequence: 3 givenname: Lili surname: Liu fullname: Liu, Lili organization: Beijing Key Laboratory for Solid Waste Utilization and Management, College of Engineering, Peking University, Beijing 100871, China – sequence: 4 givenname: Yan surname: Chen fullname: Chen, Yan organization: Beijing Key Laboratory for Solid Waste Utilization and Management, College of Engineering, Peking University, Beijing 100871, China – sequence: 5 givenname: Zuotai surname: Zhang fullname: Zhang, Zuotai organization: Beijing Key Laboratory for Solid Waste Utilization and Management, College of Engineering, Peking University, Beijing 100871, China – sequence: 6 givenname: Xidong surname: Wang fullname: Wang, Xidong email: xidong@pku.edu.cn organization: Beijing Key Laboratory for Solid Waste Utilization and Management, College of Engineering, Peking University, Beijing 100871, China |
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| Keywords | Selective catalytic reduction (SCR) V2O5 Activated semi-coke Mechanism Chemical reduction Catalytic reaction In situ V Supported catalyst O |
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| Snippet | At the reaction temperature (200°C), the active sites for NO adsorption and oxidation are mostly provided by ASC and NH3 is mainly absorbed on the Lewis acid... 3wt.% of V2O5 is loaded onto the activated semi-coke (V2O5/ASC) via impregnation method and used for low temperature selective catalytic reduction (SCR) of NO... |
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| SubjectTerms | Activated Activated semi-coke Catalysts Condensed matter: electronic structure, electrical, magnetic, and optical properties Condensed matter: structure, mechanical and thermal properties Cross-disciplinary physics: materials science; rheology Drift Exact sciences and technology Lewis acid Mechanism Nitrogen dioxide Physics Reflectance Selective catalytic reduction Selective catalytic reduction (SCR) Surface chemistry V2O5 Vanadium pentoxide |
| Title | In situ DRIFTS investigation on the SCR of NO with NH3 over V2O5 catalyst supported by activated semi-coke |
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