One-step preparation of SnO2-AuNPs as nanocomposites on photoelectrodes to enhance photoelectrochemical detection of nitrite and superoxide
[Display omitted] •Photoelectrodes modified with nanocomposites of tin oxide and gold nanoparticles.•SnO2-AuNPs nanocomposites enhanced photoelectric conversion.•Successful photoelectrochemical detection of nitrite and superoxide radicals. The integration of plasmonic metal nanoparticles and semicon...
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| Vydáno v: | Journal of electroanalytical chemistry (Lausanne, Switzerland) Ročník 917; s. 116412 |
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| Hlavní autoři: | , , , , , , , , , |
| Médium: | Journal Article |
| Jazyk: | angličtina |
| Vydáno: |
Amsterdam
Elsevier B.V
15.07.2022
Elsevier Science Ltd |
| Témata: | |
| ISSN: | 1572-6657, 1873-2569 |
| On-line přístup: | Získat plný text |
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| Abstract | [Display omitted]
•Photoelectrodes modified with nanocomposites of tin oxide and gold nanoparticles.•SnO2-AuNPs nanocomposites enhanced photoelectric conversion.•Successful photoelectrochemical detection of nitrite and superoxide radicals.
The integration of plasmonic metal nanoparticles and semiconductors improves the photoelectric conversion efficiency. We describe here a simple method for preparing photoelectrodes modified with nanocomposites of tin oxide (SnO2) and gold nanoparticles (AuNPs). This preparation process is more convenient, economical, and efficient than the previous methods. The nanocomposite of SnO2-AuNPs on indium tin oxide (ITO) conductive glass electrodes enhanced photoelectric conversion and increased conductivity. The electrodes prepared with SnO2-AuNPs nanocomposites were used as photoanodes in photoelectrochemical methods for the determination of nitrite (NO2−) and superoxide radical (O2−). The detection of superoxide radicals was achieved by stoichiometric conversion of superoxide radicals to nitrite, which overcomes a common problem of chemical instability of superoxide radicals. The photoelectrochemical method for the determination of NO2− had a detection limit of 0.1 nmol/L and a linear dynamic range from 10−9 to 10−5 mol/L. The method was successfully used to assess the photochemical generation of O2− by irradiating a photosensitizer, rose bengal (RB). The photoelectrochemical responses increased with the concentration of the photosensitizer and the time of photo irradiation (532 nm) as expected. |
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| AbstractList | The integration of plasmonic metal nanoparticles and semiconductors improves the photoelectric conversion efficiency. We describe here a simple method for preparing photoelectrodes modified with nanocomposites of tin oxide (SnO2) and gold nanoparticles (AuNPs). This preparation process is more convenient, economical, and efficient than the previous methods. The nanocomposite of SnO2-AuNPs on indium tin oxide (ITO) conductive glass electrodes enhanced photoelectric conversion and increased conductivity. The electrodes prepared with SnO2-AuNPs nanocomposites were used as photoanodes in photoelectrochemical methods for the determination of nitrite (NO2−) and superoxide radical (O2radical dot−). The detection of superoxide radicals was achieved by stoichiometric conversion of superoxide radicals to nitrite, which overcomes a common problem of chemical instability of superoxide radicals. The photoelectrochemical method for the determination of NO2− had a detection limit of 0.1 nmol/L and a linear dynamic range from 10−9 to 10−5 mol/L. The method was successfully used to assess the photochemical generation of O2radical dot− by irradiating a photosensitizer, rose bengal (RB). The photoelectrochemical responses increased with the concentration of the photosensitizer and the time of photo irradiation (532 nm) as expected. [Display omitted] •Photoelectrodes modified with nanocomposites of tin oxide and gold nanoparticles.•SnO2-AuNPs nanocomposites enhanced photoelectric conversion.•Successful photoelectrochemical detection of nitrite and superoxide radicals. The integration of plasmonic metal nanoparticles and semiconductors improves the photoelectric conversion efficiency. We describe here a simple method for preparing photoelectrodes modified with nanocomposites of tin oxide (SnO2) and gold nanoparticles (AuNPs). This preparation process is more convenient, economical, and efficient than the previous methods. The nanocomposite of SnO2-AuNPs on indium tin oxide (ITO) conductive glass electrodes enhanced photoelectric conversion and increased conductivity. The electrodes prepared with SnO2-AuNPs nanocomposites were used as photoanodes in photoelectrochemical methods for the determination of nitrite (NO2−) and superoxide radical (O2−). The detection of superoxide radicals was achieved by stoichiometric conversion of superoxide radicals to nitrite, which overcomes a common problem of chemical instability of superoxide radicals. The photoelectrochemical method for the determination of NO2− had a detection limit of 0.1 nmol/L and a linear dynamic range from 10−9 to 10−5 mol/L. The method was successfully used to assess the photochemical generation of O2− by irradiating a photosensitizer, rose bengal (RB). The photoelectrochemical responses increased with the concentration of the photosensitizer and the time of photo irradiation (532 nm) as expected. |
| ArticleNumber | 116412 |
| Author | Yao, Jingjing Ying, Ye Liu, Xinling Li, Qi Jiang, Yuning Guo, Xiaoyu Wen, Ying Wu, Yiping Yang, Haifeng Le, X. Chris |
| Author_xml | – sequence: 1 givenname: Qi surname: Li fullname: Li, Qi organization: The Ministry of Education Key Lab of Resource Chemistry, Joint International Research Laboratory of Resource Chemistry, Ministry of Education, and Shanghai Key Laboratory of Rare Earth Functional Materials, College of Chemistry and Materials Science, Shanghai Normal University, Shanghai 200234, China – sequence: 2 givenname: Jingjing surname: Yao fullname: Yao, Jingjing organization: The Ministry of Education Key Lab of Resource Chemistry, Joint International Research Laboratory of Resource Chemistry, Ministry of Education, and Shanghai Key Laboratory of Rare Earth Functional Materials, College of Chemistry and Materials Science, Shanghai Normal University, Shanghai 200234, China – sequence: 3 givenname: Yuning surname: Jiang fullname: Jiang, Yuning organization: The Ministry of Education Key Lab of Resource Chemistry, Joint International Research Laboratory of Resource Chemistry, Ministry of Education, and Shanghai Key Laboratory of Rare Earth Functional Materials, College of Chemistry and Materials Science, Shanghai Normal University, Shanghai 200234, China – sequence: 4 givenname: Xiaoyu surname: Guo fullname: Guo, Xiaoyu organization: The Ministry of Education Key Lab of Resource Chemistry, Joint International Research Laboratory of Resource Chemistry, Ministry of Education, and Shanghai Key Laboratory of Rare Earth Functional Materials, College of Chemistry and Materials Science, Shanghai Normal University, Shanghai 200234, China – sequence: 5 givenname: Ye surname: Ying fullname: Ying, Ye organization: The Ministry of Education Key Lab of Resource Chemistry, Joint International Research Laboratory of Resource Chemistry, Ministry of Education, and Shanghai Key Laboratory of Rare Earth Functional Materials, College of Chemistry and Materials Science, Shanghai Normal University, Shanghai 200234, China – sequence: 6 givenname: Ying surname: Wen fullname: Wen, Ying organization: The Ministry of Education Key Lab of Resource Chemistry, Joint International Research Laboratory of Resource Chemistry, Ministry of Education, and Shanghai Key Laboratory of Rare Earth Functional Materials, College of Chemistry and Materials Science, Shanghai Normal University, Shanghai 200234, China – sequence: 7 givenname: Xinling surname: Liu fullname: Liu, Xinling organization: The Ministry of Education Key Lab of Resource Chemistry, Joint International Research Laboratory of Resource Chemistry, Ministry of Education, and Shanghai Key Laboratory of Rare Earth Functional Materials, College of Chemistry and Materials Science, Shanghai Normal University, Shanghai 200234, China – sequence: 8 givenname: Yiping surname: Wu fullname: Wu, Yiping email: yipingwu@shnu.edu.cn organization: The Ministry of Education Key Lab of Resource Chemistry, Joint International Research Laboratory of Resource Chemistry, Ministry of Education, and Shanghai Key Laboratory of Rare Earth Functional Materials, College of Chemistry and Materials Science, Shanghai Normal University, Shanghai 200234, China – sequence: 9 givenname: Haifeng surname: Yang fullname: Yang, Haifeng email: hfyang@shnu.edu.cn organization: The Ministry of Education Key Lab of Resource Chemistry, Joint International Research Laboratory of Resource Chemistry, Ministry of Education, and Shanghai Key Laboratory of Rare Earth Functional Materials, College of Chemistry and Materials Science, Shanghai Normal University, Shanghai 200234, China – sequence: 10 givenname: X. Chris surname: Le fullname: Le, X. Chris organization: Division of Analytical and Environmental Toxicology, Department of Laboratory Medicine and Pathology, Faculty of Medicine and Dentistry, University of Alberta, 10-102 Clinical Sciences Building, Edmonton, Alberta T6G 2G3, Canada |
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| Keywords | Photoelectrochemical assay Nitrite Superoxide radical Rose bengal Semiconductor–metal nanocomposite |
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•Photoelectrodes modified with nanocomposites of tin oxide and gold nanoparticles.•SnO2-AuNPs nanocomposites enhanced photoelectric... The integration of plasmonic metal nanoparticles and semiconductors improves the photoelectric conversion efficiency. We describe here a simple method for... |
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| SubjectTerms | Glass electrodes Gold Indium tin oxides Nanocomposites Nanoparticles Nitrite Nitrogen dioxide Photoelectricity Photoelectrochemical assay Rose bengal Semiconductor–metal nanocomposite Superoxide radical Tin dioxide |
| Title | One-step preparation of SnO2-AuNPs as nanocomposites on photoelectrodes to enhance photoelectrochemical detection of nitrite and superoxide |
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