Integrated adsorption-membrane filtration process for antibiotic removal from aqueous solution

This study investigated the removal of two widely used antibiotics, norfloxacin (NOR) and ofloxacin (OFL) from aqueous solution by employing a novel integrated adsorption cum membrane filtration process. The application potential of the adsorbent was investigated by evaluating the effect of differen...

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Published in:	Powder technology Vol. 321; pp. 259 - 269
Main Authors:	Sharma, Vibhu, Vinoth Kumar, R., Pakshirajan, Kannan, Pugazhenthi, G.
Format:	Journal Article
Language:	English
Published:	Lausanne Elsevier B.V 01.11.2017 Elsevier BV
Subjects:	Adsorbates Adsorbents Adsorption Anion exchange Anion exchanging Antibiotics Aqueous solutions Ceramic membrane ceramics Data processing electrostatic interactions Electrostatic properties Filtration Fluoroquinolone Fourier transform infrared spectroscopy Hybrid process hydrophobic bonding Hydrophobicity Kinetics Membrane filtration Microfiltration Modified Ni-Al LDH Norfloxacin Ofloxacin pH effects powders Process parameters sorption isotherms Steric hindrance Ceramic membrane Fluoroquinolone Adsorption Hybrid process Modified Ni-Al LDH
ISSN:	0032-5910, 1873-328X
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Abstract	This study investigated the removal of two widely used antibiotics, norfloxacin (NOR) and ofloxacin (OFL) from aqueous solution by employing a novel integrated adsorption cum membrane filtration process. The application potential of the adsorbent was investigated by evaluating the effect of different process parameters; including solution pH, initial antibiotic concentration and adsorbent dosage. Among these parameters, solution pH significantly affected the removal of antibiotics due to its strong effect on the charges of the adsorbent and the adsorbate. The removal efficiency decreased with an increase in the initial antibiotics concentration and increased with an increase in the adsorbent amount. A maximum removal of 98.7% for NOR and 94.61% for OFL was achieved with 10mg/L initial concentration and at a solution pH of 7. A high removal of NOR as compared with that of OFL was attributed to a high steric hindrance of OFL due to its bulky structure. The adsorption kinetic data for both the antibiotics followed the pseudo second order kinetics, and the sorption isotherm data was best described by the Langmuir model. Further, adsorption of the two antibiotics involved a combination of electrostatic interaction, anion exchange and hydrophobic interaction mechanisms. The FTIR spectrum of the modified LDH obtained before and after adsorption confirmed the adsorbate-adsorbent interaction. Finally, the microfiltration technique using a ceramic membrane was effectively employed to separate the loaded adsorbent from solution to recover and reuse the adsorbent with an aim to reduce the overall cost of the adsorption process. [Display omitted] •Hybrid adsorption cum membrane microfiltration introduced for antibiotics removal•SDS modified Ni-Al LDH contributed as an adsorbent to wastewater treatment.•Low cost microfiltration membrane applied to reduce the overall operation cost•Modified LDH is better for adsorption of NOR (98.7%) and OFL (94.6%).•Established scheme can be employed efficient removal of fluoroquinolone antibiotics.
AbstractList	This study investigated the removal of two widely used antibiotics, norfloxacin (NOR) and ofloxacin (OFL) from aqueous solution by employing a novel integrated adsorption cum membrane filtration process. The application potential of the adsorbent was investigated by evaluating the effect of different process parameters; including solution pH, initial antibiotic concentration and adsorbent dosage. Among these parameters, solution pH significantly affected the removal of antibiotics due to its strong effect on the charges of the adsorbent and the adsorbate. The removal efficiency decreased with an increase in the initial antibiotics concentration and increased with an increase in the adsorbent amount. A maximum removal of 98.7% for NOR and 94.61% for OFL was achieved with 10 mg/L initial concentration and at a solution pH of 7. A high removal of NOR as compared with that of OFL was attributed to a high steric hindrance of OFL due to its bulky structure. The adsorption kinetic data for both the antibiotics followed the pseudo second order kinetics, and the sorption isotherm data was best described by the Langmuir model. Further, adsorption of the two antibiotics involved a combination of electrostatic interaction, anion exchange and hydrophobic interaction mechanisms. The FTIR spectrum of the modified LDH obtained before and after adsorption confirmed the adsorbate-adsorbent interaction. Finally, the microfiltration technique using a ceramic membrane was effectively employed to separate the loaded adsorbent from solution to recover and reuse the adsorbent with an aim to reduce the overall cost of the adsorption process. This study investigated the removal of two widely used antibiotics, norfloxacin (NOR) and ofloxacin (OFL) from aqueous solution by employing a novel integrated adsorption cum membrane filtration process. The application potential of the adsorbent was investigated by evaluating the effect of different process parameters; including solution pH, initial antibiotic concentration and adsorbent dosage. Among these parameters, solution pH significantly affected the removal of antibiotics due to its strong effect on the charges of the adsorbent and the adsorbate. The removal efficiency decreased with an increase in the initial antibiotics concentration and increased with an increase in the adsorbent amount. A maximum removal of 98.7% for NOR and 94.61% for OFL was achieved with 10mg/L initial concentration and at a solution pH of 7. A high removal of NOR as compared with that of OFL was attributed to a high steric hindrance of OFL due to its bulky structure. The adsorption kinetic data for both the antibiotics followed the pseudo second order kinetics, and the sorption isotherm data was best described by the Langmuir model. Further, adsorption of the two antibiotics involved a combination of electrostatic interaction, anion exchange and hydrophobic interaction mechanisms. The FTIR spectrum of the modified LDH obtained before and after adsorption confirmed the adsorbate-adsorbent interaction. Finally, the microfiltration technique using a ceramic membrane was effectively employed to separate the loaded adsorbent from solution to recover and reuse the adsorbent with an aim to reduce the overall cost of the adsorption process. [Display omitted] •Hybrid adsorption cum membrane microfiltration introduced for antibiotics removal•SDS modified Ni-Al LDH contributed as an adsorbent to wastewater treatment.•Low cost microfiltration membrane applied to reduce the overall operation cost•Modified LDH is better for adsorption of NOR (98.7%) and OFL (94.6%).•Established scheme can be employed efficient removal of fluoroquinolone antibiotics. This study investigated the removal of two widely used antibiotics, norfloxacin (NOR) and ofloxacin (OFL) from aqueous solution by employing a novel integrated adsorption cum membrane filtration process. The application potential of the adsorbent was investigated by evaluating the effect of different process parameters; including solution pH, initial antibiotic concentration and adsorbent dosage. Among these parameters, solution pH significantly affected the removal of antibiotics due to its strong effect on the charges of the adsorbent and the adsorbate. The removal efficiency decreased with an increase in the initial antibiotics concentration and increased with an increase in the adsorbent amount. A maximum removal of 98.7% for NOR and 94.61% for OFL was achieved with 10mg/L initial concentration and at a solution pH of 7. A high removal of NOR as compared with that of OFL was attributed to a high steric hindrance of OFL due to its bulky structure. The adsorption kinetic data for both the antibiotics followed the pseudo second order kinetics, and the sorption isotherm data was best described by the Langmuir model. Further, adsorption of the two antibiotics involved a combination of electrostatic interaction, anion exchange and hydrophobic interaction mechanisms. The FTIR spectrum of the modified LDH obtained before and after adsorption confirmed the adsorbate-adsorbent interaction. Finally, the microfiltration technique using a ceramic membrane was effectively employed to separate the loaded adsorbent from solution to recover and reuse the adsorbent with an aim to reduce the overall cost of the adsorption process.
Author	Pakshirajan, Kannan Pugazhenthi, G. Vinoth Kumar, R. Sharma, Vibhu
Author_xml	– sequence: 1 givenname: Vibhu surname: Sharma fullname: Sharma, Vibhu organization: Department of Chemical Engineering, Indian Institute of Technology Guwahati, Guwahati 781039, Assam, India – sequence: 2 givenname: R. surname: Vinoth Kumar fullname: Vinoth Kumar, R. organization: Department of Chemical Engineering, Indian Institute of Technology Guwahati, Guwahati 781039, Assam, India – sequence: 3 givenname: Kannan surname: Pakshirajan fullname: Pakshirajan, Kannan organization: Department of Biosciences and Bioengineering, Indian Institute of Technology Guwahati, Guwahati 781039, Assam, India – sequence: 4 givenname: G. surname: Pugazhenthi fullname: Pugazhenthi, G. email: pugal@iitg.ernet.in organization: Department of Chemical Engineering, Indian Institute of Technology Guwahati, Guwahati 781039, Assam, India
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Snippet	This study investigated the removal of two widely used antibiotics, norfloxacin (NOR) and ofloxacin (OFL) from aqueous solution by employing a novel integrated...
SourceID	proquest crossref elsevier
SourceType	Aggregation Database Enrichment Source Index Database Publisher
StartPage	259
SubjectTerms	Adsorbates Adsorbents Adsorption Anion exchange Anion exchanging Antibiotics Aqueous solutions Ceramic membrane ceramics Data processing electrostatic interactions Electrostatic properties Filtration Fluoroquinolone Fourier transform infrared spectroscopy Hybrid process hydrophobic bonding Hydrophobicity Kinetics Membrane filtration Microfiltration Modified Ni-Al LDH Norfloxacin Ofloxacin pH effects powders Process parameters sorption isotherms Steric hindrance
Title	Integrated adsorption-membrane filtration process for antibiotic removal from aqueous solution
URI	https://dx.doi.org/10.1016/j.powtec.2017.08.040 https://www.proquest.com/docview/1966850938 https://www.proquest.com/docview/2116915100
Volume	321
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