Extraction and incorporation of cellulose microfibers from textile wastes into MXene-enhanced PVA-borax hydrogel for multifunctional wearable sensors

Conductive hydrogel has drawn great concern in wearable sensors, human-machine interfaces, artificial intelligence (AI), health monitoring, et al. But it still remains challenge to develop hydrogel through facile and sustainable methods. In this work, a conductive, flexible, bendable and self-healin...

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Published in:	International journal of biological macromolecules Vol. 295; p. 139640
Main Authors:	Hasan, Md. Zahid, Xu, Chuanghua, Motaleb, K.Z.M. Abdul, Ahmed, Md Foysal, Zhuang, Jie, Tan, Sirui, Janutėnienė, Jolanta, Bashar, M. Mahbubul, Tu, Hu, Luo, Lei, Zhang, Ruquan
Format:	Journal Article
Language:	English
Published:	Netherlands Elsevier B.V 01.03.2025
Subjects:	ammonium persulfate artificial intelligence Borates - chemistry borax carboxylation cellulose Cellulose - chemistry Cellulose microfibers crystal structure Electric Conductivity electrical conductivity energy transfer fabrics health services human physiology Humans Hydrogel hydrogels Hydrogels - chemistry nanosheets Nitrites oxidation polyvinyl alcohol Polyvinyl Alcohol - chemistry ramie Tensile Strength Textiles Transition Elements Wearable Electronic Devices Wearable sensor Wearable sensor Cellulose microfibers Hydrogel
ISSN:	0141-8130, 1879-0003, 1879-0003
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Abstract	Conductive hydrogel has drawn great concern in wearable sensors, human-machine interfaces, artificial intelligence (AI), health monitoring, et al. But it still remains challenge to develop hydrogel through facile and sustainable methods. In this work, a conductive, flexible, bendable and self-healing hydrogel (PBCM) composed of polyvinyl alcohol (PVA), borax, cellulose microfibers (CMFs) and MXene nanosheets was fabricated by a simple and efficient strategy. The carboxylated CMFs were extracted from waste ramie fibers via a one-pot ammonium persulfate oxidation method. The crystallinity and tensile strength were increased 70 % and 4 times due to the addition of CMFs and MXene compared to the pristine PVA-borax hydrogel. The incorporation of MXene nanosheets acts as multifunctional cross-linkers and energy transfer platform, promoting the electrical conductivity, stretchability and bendability of hydrogel remarkably. The PBCM-2 hydrogel exhibited the maximum electrical conductivity of 0.81 S/cm. Additionally, the dynamic borate ester linkage imparts self-healing ability to the hydrogel. The resulting PBCM-2 hydrogel demonstrated excellent resistance to fire and pH response properties. Moreover, it showed sensitivity in monitoring various human physiological movements, including finger, wrist, elbow, knee bending and drinking water, indicating its potential for wearable sensing applications like health care and sports training.
AbstractList	Conductive hydrogel has drawn great concern in wearable sensors, human-machine interfaces, artificial intelligence (AI), health monitoring, et al. But it still remains challenge to develop hydrogel through facile and sustainable methods. In this work, a conductive, flexible, bendable and self-healing hydrogel (PBCM) composed of polyvinyl alcohol (PVA), borax, cellulose microfibers (CMFs) and MXene nanosheets was fabricated by a simple and efficient strategy. The carboxylated CMFs were extracted from waste ramie fibers via a one-pot ammonium persulfate oxidation method. The crystallinity and tensile strength were increased 70 % and 4 times due to the addition of CMFs and MXene compared to the pristine PVA-borax hydrogel. The incorporation of MXene nanosheets acts as multifunctional cross-linkers and energy transfer platform, promoting the electrical conductivity, stretchability and bendability of hydrogel remarkably. The PBCM-2 hydrogel exhibited the maximum electrical conductivity of 0.81 S/cm. Additionally, the dynamic borate ester linkage imparts self-healing ability to the hydrogel. The resulting PBCM-2 hydrogel demonstrated excellent resistance to fire and pH response properties. Moreover, it showed sensitivity in monitoring various human physiological movements, including finger, wrist, elbow, knee bending and drinking water, indicating its potential for wearable sensing applications like health care and sports training.Conductive hydrogel has drawn great concern in wearable sensors, human-machine interfaces, artificial intelligence (AI), health monitoring, et al. But it still remains challenge to develop hydrogel through facile and sustainable methods. In this work, a conductive, flexible, bendable and self-healing hydrogel (PBCM) composed of polyvinyl alcohol (PVA), borax, cellulose microfibers (CMFs) and MXene nanosheets was fabricated by a simple and efficient strategy. The carboxylated CMFs were extracted from waste ramie fibers via a one-pot ammonium persulfate oxidation method. The crystallinity and tensile strength were increased 70 % and 4 times due to the addition of CMFs and MXene compared to the pristine PVA-borax hydrogel. The incorporation of MXene nanosheets acts as multifunctional cross-linkers and energy transfer platform, promoting the electrical conductivity, stretchability and bendability of hydrogel remarkably. The PBCM-2 hydrogel exhibited the maximum electrical conductivity of 0.81 S/cm. Additionally, the dynamic borate ester linkage imparts self-healing ability to the hydrogel. The resulting PBCM-2 hydrogel demonstrated excellent resistance to fire and pH response properties. Moreover, it showed sensitivity in monitoring various human physiological movements, including finger, wrist, elbow, knee bending and drinking water, indicating its potential for wearable sensing applications like health care and sports training. Conductive hydrogel has drawn great concern in wearable sensors, human-machine interfaces, artificial intelligence (AI), health monitoring, et al. But it still remains challenge to develop hydrogel through facile and sustainable methods. In this work, a conductive, flexible, bendable and self-healing hydrogel (PBCM) composed of polyvinyl alcohol (PVA), borax, cellulose microfibers (CMFs) and MXene nanosheets was fabricated by a simple and efficient strategy. The carboxylated CMFs were extracted from waste ramie fibers via a one-pot ammonium persulfate oxidation method. The crystallinity and tensile strength were increased 70 % and 4 times due to the addition of CMFs and MXene compared to the pristine PVA-borax hydrogel. The incorporation of MXene nanosheets acts as multifunctional cross-linkers and energy transfer platform, promoting the electrical conductivity, stretchability and bendability of hydrogel remarkably. The PBCM-2 hydrogel exhibited the maximum electrical conductivity of 0.81 S/cm. Additionally, the dynamic borate ester linkage imparts self-healing ability to the hydrogel. The resulting PBCM-2 hydrogel demonstrated excellent resistance to fire and pH response properties. Moreover, it showed sensitivity in monitoring various human physiological movements, including finger, wrist, elbow, knee bending and drinking water, indicating its potential for wearable sensing applications like health care and sports training. Conductive hydrogel has drawn great concern in wearable sensors, human-machine interfaces, artificial intelligence (AI), health monitoring, et al. But it still remains challenge to develop hydrogel through facile and sustainable methods. In this work, a conductive, flexible, bendable and self-healing hydrogel (PBCM) composed of polyvinyl alcohol (PVA), borax, cellulose microfibers (CMFs) and MXene nanosheets was fabricated by a simple and efficient strategy. The carboxylated CMFs were extracted from waste ramie fibers via a one-pot ammonium persulfate oxidation method. The crystallinity and tensile strength were increased 70 % and 4 times due to the addition of CMFs and MXene compared to the pristine PVA-borax hydrogel. The incorporation of MXene nanosheets acts as multifunctional cross-linkers and energy transfer platform, promoting the electrical conductivity, stretchability and bendability of hydrogel remarkably. The PBCM-2 hydrogel exhibited the maximum electrical conductivity of 0.81 S/cm. Additionally, the dynamic borate ester linkage imparts self-healing ability to the hydrogel. The resulting PBCM-2 hydrogel demonstrated excellent resistance to fire and pH response properties. Moreover, it showed sensitivity in monitoring various human physiological movements, including finger, wrist, elbow, knee bending and drinking water, indicating its potential for wearable sensing applications like health care and sports training.
ArticleNumber	139640
Author	Hasan, Md. Zahid Xu, Chuanghua Bashar, M. Mahbubul Tan, Sirui Motaleb, K.Z.M. Abdul Ahmed, Md Foysal Janutėnienė, Jolanta Zhang, Ruquan Zhuang, Jie Tu, Hu Luo, Lei
Author_xml	– sequence: 1 givenname: Md. Zahid surname: Hasan fullname: Hasan, Md. Zahid organization: State Key Laboratory of New Textile Materials and Advanced Processing Technologies, School of Textile Science and Engineering, Wuhan Textile University, Wuhan 430200, China – sequence: 2 givenname: Chuanghua surname: Xu fullname: Xu, Chuanghua organization: State Key Laboratory of New Textile Materials and Advanced Processing Technologies, School of Textile Science and Engineering, Wuhan Textile University, Wuhan 430200, China – sequence: 3 givenname: K.Z.M. Abdul surname: Motaleb fullname: Motaleb, K.Z.M. Abdul organization: Department of Engineering, Faculty of Marine Technologies and Natural Sciences, Klaipeda University, Klaipėda 91224, Lithuania – sequence: 4 givenname: Md Foysal surname: Ahmed fullname: Ahmed, Md Foysal organization: State Key Laboratory of New Textile Materials and Advanced Processing Technologies, School of Textile Science and Engineering, Wuhan Textile University, Wuhan 430200, China – sequence: 5 givenname: Jie surname: Zhuang fullname: Zhuang, Jie organization: State Key Laboratory of New Textile Materials and Advanced Processing Technologies, School of Textile Science and Engineering, Wuhan Textile University, Wuhan 430200, China – sequence: 6 givenname: Sirui surname: Tan fullname: Tan, Sirui organization: State Key Laboratory of New Textile Materials and Advanced Processing Technologies, School of Textile Science and Engineering, Wuhan Textile University, Wuhan 430200, China – sequence: 7 givenname: Jolanta surname: Janutėnienė fullname: Janutėnienė, Jolanta organization: Department of Engineering, Faculty of Marine Technologies and Natural Sciences, Klaipeda University, Klaipėda 91224, Lithuania – sequence: 8 givenname: M. Mahbubul surname: Bashar fullname: Bashar, M. Mahbubul organization: Department of Textile Engineering, Mawlana Bhashani Science and Technology University, Tangail 1902, Bangladesh – sequence: 9 givenname: Hu surname: Tu fullname: Tu, Hu organization: State Key Laboratory of New Textile Materials and Advanced Processing Technologies, School of Textile Science and Engineering, Wuhan Textile University, Wuhan 430200, China – sequence: 10 givenname: Lei surname: Luo fullname: Luo, Lei email: leiluo@wtu.edu.cn organization: State Key Laboratory of New Textile Materials and Advanced Processing Technologies, School of Textile Science and Engineering, Wuhan Textile University, Wuhan 430200, China – sequence: 11 givenname: Ruquan surname: Zhang fullname: Zhang, Ruquan email: zhangruquan@wtu.edu.cn organization: State Key Laboratory of New Textile Materials and Advanced Processing Technologies, School of Textile Science and Engineering, Wuhan Textile University, Wuhan 430200, China
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Snippet	Conductive hydrogel has drawn great concern in wearable sensors, human-machine interfaces, artificial intelligence (AI), health monitoring, et al. But it still...
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SubjectTerms	ammonium persulfate artificial intelligence Borates - chemistry borax carboxylation cellulose Cellulose - chemistry Cellulose microfibers crystal structure Electric Conductivity electrical conductivity energy transfer fabrics health services human physiology Humans Hydrogel hydrogels Hydrogels - chemistry nanosheets Nitrites oxidation polyvinyl alcohol Polyvinyl Alcohol - chemistry ramie Tensile Strength Textiles Transition Elements Wearable Electronic Devices Wearable sensor
Title	Extraction and incorporation of cellulose microfibers from textile wastes into MXene-enhanced PVA-borax hydrogel for multifunctional wearable sensors
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