A new story in the structural chemistry of cerium(IV) phosphate
Two different cerium(IV) phosphates have been prepared by ageing at 95 °C an aqueous solution made from Ce(NO 3) 6(NH 4) 2, nitric acid, and phosphoric acid with the following conditions: P/Ce=2, [HNO 3]=5.8 M and [Ce 4+]=0.1 M. The control over the formed solid was achieved through the ageing time....
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| Published in: | The Journal of physics and chemistry of solids Vol. 68; no. 5; pp. 795 - 798 |
|---|---|
| Main Authors: | , , , , , |
| Format: | Journal Article Conference Proceeding |
| Language: | English |
| Published: |
Oxford
Elsevier Ltd
01.05.2007
Elsevier |
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| ISSN: | 0022-3697, 1879-2553 |
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| Abstract | Two different cerium(IV) phosphates have been prepared by ageing at 95
°C an aqueous solution made from Ce(NO
3)
6(NH
4)
2, nitric acid, and phosphoric acid with the following conditions: P/Ce=2, [HNO
3]=5.8
M and [Ce
4+]=0.1
M. The control over the formed solid was achieved through the ageing time. After 18
h, a metastable compound (
A), corresponding to Ce(PO
4)
1.5(H
2O)(H
3O)
0.5(H
2O)
0.5, is obtained, while after 5 days a stable one (
B), corresponding to Ce(PO
4)(HPO
4)
0.5(H
2O)
0.5, is recovered. Both solids exhibit a P/Ce ratio of 1.5. Their structures,
31P solid state NMR, and thermal behaviors are compared. |
|---|---|
| AbstractList | Two different cerium(IV) phosphates have been prepared by ageing at 95
°C an aqueous solution made from Ce(NO
3)
6(NH
4)
2, nitric acid, and phosphoric acid with the following conditions: P/Ce=2, [HNO
3]=5.8
M and [Ce
4+]=0.1
M. The control over the formed solid was achieved through the ageing time. After 18
h, a metastable compound (
A), corresponding to Ce(PO
4)
1.5(H
2O)(H
3O)
0.5(H
2O)
0.5, is obtained, while after 5 days a stable one (
B), corresponding to Ce(PO
4)(HPO
4)
0.5(H
2O)
0.5, is recovered. Both solids exhibit a P/Ce ratio of 1.5. Their structures,
31P solid state NMR, and thermal behaviors are compared. |
| Author | Quarton, Michel Jolivet, Jean-Pierre Ribot, François Chanéac, Corinne Wallez, Gilles Nazaraly, Micaela |
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| Keywords | A. Inorganic compounds D. NMR C. TGA C. X-ray diffraction Aqueous solutions Thermogravimetry Aging Cerium phosphates XRD Nuclear magnetic resonance Solid structure |
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| Snippet | Two different cerium(IV) phosphates have been prepared by ageing at 95
°C an aqueous solution made from Ce(NO
3)
6(NH
4)
2, nitric acid, and phosphoric acid... |
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| SubjectTerms | A. Inorganic compounds C. TGA C. X-ray diffraction Condensed matter: structure, mechanical and thermal properties D. NMR Exact sciences and technology Inorganic compounds Physics Structure of solids and liquids; crystallography Structure of specific crystalline solids |
| Title | A new story in the structural chemistry of cerium(IV) phosphate |
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