La- and Mn-doped cobalt spinel oxygen evolution catalyst for proton exchange membrane electrolysis

Discovery of earth-abundant electrocatalysts to replace iridium for the oxygen evolution reaction (OER) in a proton exchange membrane water electrolyzer (PEMWE) represents a critical step in reducing the cost for green hydrogen production. We report a nanofibrous cobalt spinel catalyst codoped with...

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Veröffentlicht in:	Science (American Association for the Advancement of Science) Jg. 380; H. 6645; S. 609
Hauptverfasser:	Chong, Lina, Gao, Guoping, Wen, Jianguo, Li, Haixia, Xu, Haiping, Green, Zach, Sugar, Joshua D, Kropf, A Jeremy, Xu, Wenqian, Lin, Xiao-Min, Xu, Hui, Wang, Lin-Wang, Liu, Di-Jia
Format:	Journal Article
Sprache:	Englisch
Veröffentlicht:	United States 12.05.2023
ISSN:	1095-9203, 1095-9203
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Abstract	Discovery of earth-abundant electrocatalysts to replace iridium for the oxygen evolution reaction (OER) in a proton exchange membrane water electrolyzer (PEMWE) represents a critical step in reducing the cost for green hydrogen production. We report a nanofibrous cobalt spinel catalyst codoped with lanthanum (La) and manganese (Mn) prepared from a zeolitic imidazolate framework embedded in electrospun polymer fiber. The catalyst demonstrated a low overpotential of 353 millivolts at 10 milliamperes per square centimeter and a low degradation for OER over 360 hours in acidic electrolyte. A PEMWE containing this catalyst at the anode demonstrated a current density of 2000 milliamperes per square centimeter at 2.47 volts (Nafion 115 membrane) or 4000 milliamperes per square centimeter at 3.00 volts (Nafion 212 membrane) and low degradation in an accelerated stress test.
AbstractList	Discovery of earth-abundant electrocatalysts to replace iridium for the oxygen evolution reaction (OER) in a proton exchange membrane water electrolyzer (PEMWE) represents a critical step in reducing the cost for green hydrogen production. We report a nanofibrous cobalt spinel catalyst codoped with lanthanum (La) and manganese (Mn) prepared from a zeolitic imidazolate framework embedded in electrospun polymer fiber. The catalyst demonstrated a low overpotential of 353 millivolts at 10 milliamperes per square centimeter and a low degradation for OER over 360 hours in acidic electrolyte. A PEMWE containing this catalyst at the anode demonstrated a current density of 2000 milliamperes per square centimeter at 2.47 volts (Nafion 115 membrane) or 4000 milliamperes per square centimeter at 3.00 volts (Nafion 212 membrane) and low degradation in an accelerated stress test.Discovery of earth-abundant electrocatalysts to replace iridium for the oxygen evolution reaction (OER) in a proton exchange membrane water electrolyzer (PEMWE) represents a critical step in reducing the cost for green hydrogen production. We report a nanofibrous cobalt spinel catalyst codoped with lanthanum (La) and manganese (Mn) prepared from a zeolitic imidazolate framework embedded in electrospun polymer fiber. The catalyst demonstrated a low overpotential of 353 millivolts at 10 milliamperes per square centimeter and a low degradation for OER over 360 hours in acidic electrolyte. A PEMWE containing this catalyst at the anode demonstrated a current density of 2000 milliamperes per square centimeter at 2.47 volts (Nafion 115 membrane) or 4000 milliamperes per square centimeter at 3.00 volts (Nafion 212 membrane) and low degradation in an accelerated stress test. Discovery of earth-abundant electrocatalysts to replace iridium for the oxygen evolution reaction (OER) in a proton exchange membrane water electrolyzer (PEMWE) represents a critical step in reducing the cost for green hydrogen production. We report a nanofibrous cobalt spinel catalyst codoped with lanthanum (La) and manganese (Mn) prepared from a zeolitic imidazolate framework embedded in electrospun polymer fiber. The catalyst demonstrated a low overpotential of 353 millivolts at 10 milliamperes per square centimeter and a low degradation for OER over 360 hours in acidic electrolyte. A PEMWE containing this catalyst at the anode demonstrated a current density of 2000 milliamperes per square centimeter at 2.47 volts (Nafion 115 membrane) or 4000 milliamperes per square centimeter at 3.00 volts (Nafion 212 membrane) and low degradation in an accelerated stress test.
Author	Xu, Wenqian Xu, Haiping Green, Zach Lin, Xiao-Min Liu, Di-Jia Xu, Hui Li, Haixia Sugar, Joshua D Wen, Jianguo Kropf, A Jeremy Gao, Guoping Chong, Lina Wang, Lin-Wang
Author_xml	– sequence: 1 givenname: Lina orcidid: 0000-0002-2061-6916 surname: Chong fullname: Chong, Lina organization: Chemical Science and Engineering Division, Argonne National Laboratory, Lemont, IL 60439, USA – sequence: 2 givenname: Guoping orcidid: 0000-0002-6106-7423 surname: Gao fullname: Gao, Guoping organization: Material Science Division, Lawrence Berkeley National Laboratory, Berkeley, CA 94720, USA – sequence: 3 givenname: Jianguo orcidid: 0000-0002-3755-0044 surname: Wen fullname: Wen, Jianguo organization: Center for Nanoscale Materials, Argonne National Laboratory, Lemont, IL 60439, USA – sequence: 4 givenname: Haixia surname: Li fullname: Li, Haixia organization: Material Science Division, Lawrence Berkeley National Laboratory, Berkeley, CA 94720, USA – sequence: 5 givenname: Haiping orcidid: 0000-0003-1930-0401 surname: Xu fullname: Xu, Haiping organization: Chemical Science and Engineering Division, Argonne National Laboratory, Lemont, IL 60439, USA – sequence: 6 givenname: Zach orcidid: 0009-0001-3541-7610 surname: Green fullname: Green, Zach organization: Giner Inc., Auburndale, MA 02466, USA – sequence: 7 givenname: Joshua D surname: Sugar fullname: Sugar, Joshua D organization: Sandia National Laboratory, Livermore, CA 94550, USA – sequence: 8 givenname: A Jeremy orcidid: 0000-0002-3329-4493 surname: Kropf fullname: Kropf, A Jeremy organization: Chemical Science and Engineering Division, Argonne National Laboratory, Lemont, IL 60439, USA – sequence: 9 givenname: Wenqian orcidid: 0000-0002-4815-6253 surname: Xu fullname: Xu, Wenqian organization: X-ray Science Division, Advanced Photon Source, Argonne National Laboratory, Lemont, IL 60439, USA – sequence: 10 givenname: Xiao-Min orcidid: 0000-0002-2879-3474 surname: Lin fullname: Lin, Xiao-Min organization: Center for Nanoscale Materials, Argonne National Laboratory, Lemont, IL 60439, USA – sequence: 11 givenname: Hui orcidid: 0000-0001-6829-7187 surname: Xu fullname: Xu, Hui organization: Giner Inc., Auburndale, MA 02466, USA – sequence: 12 givenname: Lin-Wang orcidid: 0000-0001-7061-2692 surname: Wang fullname: Wang, Lin-Wang organization: Material Science Division, Lawrence Berkeley National Laboratory, Berkeley, CA 94720, USA – sequence: 13 givenname: Di-Jia orcidid: 0000-0003-1747-028X surname: Liu fullname: Liu, Di-Jia organization: Pritzker School of Molecular Engineering, University of Chicago, Chicago, IL 60637, USA
BackLink	https://www.ncbi.nlm.nih.gov/pubmed/37167381$$D View this record in MEDLINE/PubMed
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References	40504930 - Science. 2025 Jun 12;388(6752):eadz5020. doi: 10.1126/science.adz5020.
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