Syntheses and Crystal Structures of Two Cadmium Methanetetrabenzoates Featured by Open Framework and Infinite Layers
Colorless single crystals of Cd2[μ8‐MTB]·3H2O·DMF (1) were prepared in DMF/H2O solution [1: space group C2/c (no. 15) with a = 1821.30(6), b = 2175.08(6), c = 1269.87(4) pm, β = 129.684(1)°]. The connection between the methane‐p‐benzoate tetraanions (MTB4–) and the Cd2+ cations leads to a three‐dime...
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| Veröffentlicht in: | Zeitschrift für anorganische und allgemeine Chemie (1950) Jg. 645; H. 14; S. 912 - 918 |
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| Format: | Journal Article |
| Sprache: | Englisch |
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Weinheim
Wiley Subscription Services, Inc
31.07.2019
Wiley-VCH Verlag |
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| ISSN: | 0044-2313, 1521-3749 |
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| Abstract | Colorless single crystals of Cd2[μ8‐MTB]·3H2O·DMF (1) were prepared in DMF/H2O solution [1: space group C2/c (no. 15) with a = 1821.30(6), b = 2175.08(6), c = 1269.87(4) pm, β = 129.684(1)°]. The connection between the methane‐p‐benzoate tetraanions (MTB4–) and the Cd2+ cations leads to a three‐dimensional framework with channels extending along [110] and [110] with openings of 670 pm × 360 pm. The channel‐like voids accommodate water molecules and N,N‐dimethylformamide (DMF) molecules not bound to Cd2+. Colorless single crystals of [Cd4(2,2′‐bipy)4(μ7‐MTB)2]·7DMF (2) were prepared in DMF in the presence of 2,2′‐bipyridine [2: space group P1 (no. 2) with a = 1224.84(4), b = 1418.85(5), c = 2033.49(4) pm, α = 85.831(2)°, β = 88.351(2)°, γ = 68.261(1)°]. The coordination of MTB4– to Cd2+ results in infinite layers parallel to (001). The layers, not connected by any hydrogen bonds, contain small openings of about 320 pm × 340 pm. |
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| AbstractList | Colourless single crystals of Cd2[μ8-MTB]*3H2O*DMF (1) were prepared in DMF/H2O solution. 1: Space group C2/c (no. 15) with a = 1821.30(6), b = 2175.08(6), c = 1269.87(4) pm, β = 129.684(1)°. The connection between the methane-p-benzoate tetraanions (MTB4−) and the Cd2+ cations leads to a three-dimensional framework with channels extending along [ 10] and [110] with openings of 670 pm × 360 pm. The channel-like voids accommodate water molecules and N,N-dimethylformamide (DMF) molecules not bound to Cd2+. Colourless single crystals of [Cd4(2,2′-bipy)4(μ7-MTB)2]*7DMF (2) were prepared in DMF in the presence of 2,2'-bipyridine. 2: Space group P (no. 2) with a = 1224.84(4), b = 1418.85(5), c = 2033.49(4) pm, α = 85.831(2)°, β = 88.351(2)°, γ = 68.261(1)°. The coordination of MTB4− to Cd2+ results in infinite layers parallel to (001). The layers, not connected by any hydrogen bonds, contain small openings of about 320 pm × 340 pm. Colorless single crystals of Cd2[μ8‐MTB]·3H2O·DMF (1) were prepared in DMF/H2O solution [1: space group C2/c (no. 15) with a = 1821.30(6), b = 2175.08(6), c = 1269.87(4) pm, β = 129.684(1)°]. The connection between the methane‐p‐benzoate tetraanions (MTB4–) and the Cd2+ cations leads to a three‐dimensional framework with channels extending along [110] and [110] with openings of 670 pm × 360 pm. The channel‐like voids accommodate water molecules and N,N‐dimethylformamide (DMF) molecules not bound to Cd2+. Colorless single crystals of [Cd4(2,2′‐bipy)4(μ7‐MTB)2]·7DMF (2) were prepared in DMF in the presence of 2,2′‐bipyridine [2: space group P1 (no. 2) with a = 1224.84(4), b = 1418.85(5), c = 2033.49(4) pm, α = 85.831(2)°, β = 88.351(2)°, γ = 68.261(1)°]. The coordination of MTB4– to Cd2+ results in infinite layers parallel to (001). The layers, not connected by any hydrogen bonds, contain small openings of about 320 pm × 340 pm. Colorless single crystals of Cd 2 [μ 8 ‐MTB] · 3H 2 O · DMF ( 1 ) were prepared in DMF/H 2 O solution [ 1 : space group C 2/ c (no. 15) with a = 1821.30(6), b = 2175.08(6), c = 1269.87(4) pm, β = 129.684(1)°]. The connection between the methane‐ p ‐benzoate tetraanions (MTB 4– ) and the Cd 2+ cations leads to a three‐dimensional framework with channels extending along [ 1 10] and [110] with openings of 670 pm × 360 pm. The channel‐like voids accommodate water molecules and N , N ‐dimethylformamide (DMF) molecules not bound to Cd 2+ . Colorless single crystals of [Cd 4 (2,2′‐bipy) 4 (μ 7 ‐MTB) 2 ] · 7DMF ( 2 ) were prepared in DMF in the presence of 2,2′‐bipyridine [ 2 : space group P 1 (no. 2) with a = 1224.84(4), b = 1418.85(5), c = 2033.49(4) pm, α = 85.831(2)°, β = 88.351(2)°, γ = 68.261(1)°]. The coordination of MTB 4– to Cd 2+ results in infinite layers parallel to (001). The layers, not connected by any hydrogen bonds, contain small openings of about 320 pm × 340 pm. |
| Author | Köferstein, Roberto Görls, Helmar Harms, Sven Robl, Christian |
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| Keywords | metal organic framework methanetetra-p-benzoates single crystal cadmium porous benzoate building blocks Coordination compounds voids coordination polymer |
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| Snippet | Colorless single crystals of Cd2[μ8‐MTB]·3H2O·DMF (1) were prepared in DMF/H2O solution [1: space group C2/c (no. 15) with a = 1821.30(6), b = 2175.08(6), c =... Colorless single crystals of Cd 2 [μ 8 ‐MTB] · 3H 2 O · DMF ( 1 ) were prepared in DMF/H 2 O solution [ 1 : space group C 2/ c (no. 15) with a = 1821.30(6), b... Colourless single crystals of Cd2[μ8-MTB]*3H2O*DMF (1) were prepared in DMF/H2O solution. 1: Space group C2/c (no. 15) with a = 1821.30(6), b = 2175.08(6), c =... |
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| SubjectTerms | Benzoates Cadmium Chemical Sciences Coordination chemistry Coordination polymer Crystal structure Hydrogen bonds Inorganic chemistry Metal‐organic framework (MOF) Methanetetra‐p‐benzoic acid Single crystals Water chemistry |
| Title | Syntheses and Crystal Structures of Two Cadmium Methanetetrabenzoates Featured by Open Framework and Infinite Layers |
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