Chemical and mechanical reprocessed resins and bio-composites based on five epoxidized vegetable oils thermosets reinforced with flax fibers or PLA woven

Bio-epoxy resins based on five epoxidized vegetable oils were formulated with an aromatic disulfide crosslinker with diacid functionality, 2,2′-dithiodibenzoic acid (DTBA), to obtain recyclable epoxy thermosets. Flax fibres (FF) and PLA woven were used as bio-based reinforcements for these matrices....

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Published in:	Composites science and technology Vol. 205; p. 108678
Main Authors:	Di Mauro, Chiara, Genua, Aratz, Rymarczyk, Monica, Dobbels, Caroline, Malburet, Samuel, Graillot, Alain, Mija, Alice
Format:	Journal Article
Language:	English
Published:	Barking Elsevier Ltd 22.03.2021 Elsevier BV Elsevier
Subjects:	Bio-based composites Chemical Sciences Crosslinking Crosslinking polymerization Differential scanning calorimetry Dynamic mechanical analysis Epoxidized vegetable oils Epoxy resins Fibers Flax Flax and PLA fibres Mechanical properties Polymer matrix composites Recyclable resins & composites Second-generation composites Thermodynamic properties Thermogravimetric analysis Vegetable oils Water absorption Recyclable resins & composites Flax and PLA fibres Second-generation composites Bio-based composites Epoxidized vegetable oils
ISSN:	0266-3538, 1879-1050
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Abstract	Bio-epoxy resins based on five epoxidized vegetable oils were formulated with an aromatic disulfide crosslinker with diacid functionality, 2,2′-dithiodibenzoic acid (DTBA), to obtain recyclable epoxy thermosets. Flax fibres (FF) and PLA woven were used as bio-based reinforcements for these matrices. Different percentages of reinforcement were tested and the effect of the natural fibres on the matrix's crosslinking reaction was studied by DSC analysis. Then, the obtained materials were analyzed by Differential Scanning Calorimetry (DSC), Thermogravimetric Analysis (TGA), Dynamic Mechanical Analysis (DMA), water absorption and Scanning Electron Microscopy (SEM). The reinforcements improved the thermal and mechanical properties of the neat resins, with tan δ values varying from 91 to 148 °C showing a good compatibility matrix-FF but a reduced one in case of matrix-PLA woven. The dynamic nature of the networks crosslinking allowed the chemical and mechanical recycling of both resins and bio-composites. Moreover, the obtained results show the possibility to recuperate the natural FF filler for the preparation of second-life generation bio-composites. [Display omitted]
AbstractList	Bio-epoxy resins based on five epoxidized vegetable oils were formulated with an arom. disulfide crosslinker with diacid functionality, 2,2'-dithiodibenzoic acid (DTBA), to obtain recyclable epoxy thermosets. Flax fibers (FF) and PLA woven were used as bio-based reinforcements for these matrixes. Different percentages of reinforcement were tested and the effect of the natural fibers on the matrix's crosslinking reaction was studied by DSC anal. Then, the obtained materials were analyzed by differential scanning calorimetry, thermogravimetric anal., dynamic mech. anal., water absorption and SEM. The reinforcements improved the thermal and mech. properties of the neat resins, with tan δ values varying from 91 to 148°C showing a good compatibility matrix-FF but a reduced one in case of matrix-PLA woven. The dynamic nature of the networks crosslinking allowed the chem. and mech. recycling of both resins and bio-composites. Moreover, the obtained results show the possibility to recuperate the natural FF filler for the prepn. of second-life generation bio-composites. Bio-epoxy resins based on five epoxidized vegetable oils were formulated with an aromatic disulfide crosslinker with diacid functionality, 2,2′-dithiodibenzoic acid (DTBA), to obtain recyclable epoxy thermosets. Flax fibres (FF) and PLA woven were used as bio-based reinforcements for these matrices. Different percentages of reinforcement were tested and the effect of the natural fibres on the matrix's crosslinking reaction was studied by DSC analysis. Then, the obtained materials were analyzed by Differential Scanning Calorimetry (DSC), Thermogravimetric Analysis (TGA), Dynamic Mechanical Analysis (DMA), water absorption and Scanning Electron Microscopy (SEM). The reinforcements improved the thermal and mechanical properties of the neat resins, with tan δ values varying from 91 to 148 °C showing a good compatibility matrix-FF but a reduced one in case of matrix-PLA woven. The dynamic nature of the networks crosslinking allowed the chemical and mechanical recycling of both resins and bio-composites. Moreover, the obtained results show the possibility to recuperate the natural FF filler for the preparation of second-life generation bio-composites. [Display omitted] Bio-epoxy resins based on five epoxidized vegetable oils were formulated with an aromatic disulfide crosslinker with diacid functionality, 2,2′-dithiodibenzoic acid (DTBA), to obtain recyclable epoxy thermosets. Flax fibres (FF) and PLA woven were used as bio-based reinforcements for these matrices. Different percentages of reinforcement were tested and the effect of the natural fibres on the matrix's crosslinking reaction was studied by DSC analysis. Then, the obtained materials were analyzed by Differential Scanning Calorimetry (DSC), Thermogravimetric Analysis (TGA), Dynamic Mechanical Analysis (DMA), water absorption and Scanning Electron Microscopy (SEM). The reinforcements improved the thermal and mechanical properties of the neat resins, with tan δ values varying from 91 to 148 °C showing a good compatibility matrix-FF but a reduced one in case of matrix-PLA woven. The dynamic nature of the networks crosslinking allowed the chemical and mechanical recycling of both resins and bio-composites. Moreover, the obtained results show the possibility to recuperate the natural FF filler for the preparation of second-life generation bio-composites.
ArticleNumber	108678
Author	Graillot, Alain Di Mauro, Chiara Rymarczyk, Monica Dobbels, Caroline Genua, Aratz Mija, Alice Malburet, Samuel
Author_xml	– sequence: 1 givenname: Chiara surname: Di Mauro fullname: Di Mauro, Chiara organization: Université Côte D'Azur, Institut de Chimie de Nice, UMR CNRS 7272, 28 Av Valrose, 06108, Nice, France – sequence: 2 givenname: Aratz surname: Genua fullname: Genua, Aratz organization: CIDETEC, Basque Research and Technology Alliance (BRTA), Paseo Miramon196, Donostia-San Sebastian, 20014, Spain – sequence: 3 givenname: Monica surname: Rymarczyk fullname: Rymarczyk, Monica organization: Centexbel-VKC, Technologiepark 70, 9052, Gent-Zwijnaarde, Belgium – sequence: 4 givenname: Caroline surname: Dobbels fullname: Dobbels, Caroline organization: Flipts & Dobbels, Groenestraat 220, B-8800, Roeselare, Belgium – sequence: 5 givenname: Samuel surname: Malburet fullname: Malburet, Samuel organization: SPECIFIC POLYMERS, Parc Via Domitia, 150 Avenue des Cocardières, 34160, Castries, France – sequence: 6 givenname: Alain surname: Graillot fullname: Graillot, Alain organization: SPECIFIC POLYMERS, Parc Via Domitia, 150 Avenue des Cocardières, 34160, Castries, France – sequence: 7 givenname: Alice orcidid: 0000-0001-5208-5956 surname: Mija fullname: Mija, Alice email: Alice.MIJA@univ-cotedazur.fr organization: Université Côte D'Azur, Institut de Chimie de Nice, UMR CNRS 7272, 28 Av Valrose, 06108, Nice, France
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Keywords	Recyclable resins & composites Flax and PLA fibres Second-generation composites Bio-based composites Epoxidized vegetable oils
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Snippet	Bio-epoxy resins based on five epoxidized vegetable oils were formulated with an aromatic disulfide crosslinker with diacid functionality, 2,2′-dithiodibenzoic... Bio-epoxy resins based on five epoxidized vegetable oils were formulated with an arom. disulfide crosslinker with diacid functionality, 2,2'-dithiodibenzoic...
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SubjectTerms	Bio-based composites Chemical Sciences Crosslinking Crosslinking polymerization Differential scanning calorimetry Dynamic mechanical analysis Epoxidized vegetable oils Epoxy resins Fibers Flax Flax and PLA fibres Mechanical properties Polymer matrix composites Recyclable resins & composites Second-generation composites Thermodynamic properties Thermogravimetric analysis Vegetable oils Water absorption
Title	Chemical and mechanical reprocessed resins and bio-composites based on five epoxidized vegetable oils thermosets reinforced with flax fibers or PLA woven
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