30 Li+‐Accommodating Covalent Organic Frameworks as Ultralong Cyclable High‐Capacity Li‐Ion Battery Electrodes

Covalent organic frameworks (COFs) have attracted considerable attention as a facile and versatile design platform for advanced energy storage materials owing to their structural diversity, ordered porous structures, and chemical stability. In this study, a redox‐active COF (TP–OH–COF) that can acco...

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Published in:	Advanced functional materials Vol. 32; no. 9
Main Authors:	Zhai, Lipeng, Li, Gaojie, Yang, Xiubei, Park, Sodam, Han, Diandian, Mi, Liwei, Wang, Yanjie, Li, Zhongping, Lee, Sang‐Young
Format:	Journal Article
Language:	English
Published:	Hoboken Wiley Subscription Services, Inc 01.02.2022
Subjects:	Carbonyls Chemical synthesis covalent organic frameworks Electrode materials Energy storage high capacity Lithium-ion batteries Materials science redox‐active carbonyl sites Tethering
ISSN:	1616-301X, 1616-3028
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Abstract	Covalent organic frameworks (COFs) have attracted considerable attention as a facile and versatile design platform for advanced energy storage materials owing to their structural diversity, ordered porous structures, and chemical stability. In this study, a redox‐active COF (TP–OH–COF) that can accommodate 30 Li+ ions is synthesized for potential use as an ultralong cyclable high‐capacity lithium‐ion battery electrode material. The TP–OH–COF is synthesized using triformylpholoroglucinol and 2,5‐diaminohydroquinone dihydrochloride under solvothermal conditions. The accommodation of such exceptional Li+ ion content in the TP–OH–COF is achieved by alternately tethering redox‐active hydroxyl and carbonyl sites on the pore walls. Owing to this unique chemical/structural feature, the TP–OH–COF delivers a high specific capacity of 764.1 mAh g–1, and capacity retention of 63% after 8000 cycles at a fast current density of 5.0 A g–1. A redox‐active COF with alternate tethering of redox‐active hydroxyl and carbonyl sites on the pore walls is demonstrated as an organic‐based, ultralong cyclable high‐capacity LIB anode material. This COF electrode accommodated 30 Li+ ions owing to its unique framework structure and materials chemistry, which has never been reported in previous studies on COF‐based electrode materials.
AbstractList	Covalent organic frameworks (COFs) have attracted considerable attention as a facile and versatile design platform for advanced energy storage materials owing to their structural diversity, ordered porous structures, and chemical stability. In this study, a redox‐active COF (TP–OH–COF) that can accommodate 30 Li + ions is synthesized for potential use as an ultralong cyclable high‐capacity lithium‐ion battery electrode material. The TP–OH–COF is synthesized using triformylpholoroglucinol and 2,5‐diaminohydroquinone dihydrochloride under solvothermal conditions. The accommodation of such exceptional Li + ion content in the TP–OH–COF is achieved by alternately tethering redox‐active hydroxyl and carbonyl sites on the pore walls. Owing to this unique chemical/structural feature, the TP–OH–COF delivers a high specific capacity of 764.1 mAh g –1 , and capacity retention of 63% after 8000 cycles at a fast current density of 5.0 A g –1 . Covalent organic frameworks (COFs) have attracted considerable attention as a facile and versatile design platform for advanced energy storage materials owing to their structural diversity, ordered porous structures, and chemical stability. In this study, a redox‐active COF (TP–OH–COF) that can accommodate 30 Li+ ions is synthesized for potential use as an ultralong cyclable high‐capacity lithium‐ion battery electrode material. The TP–OH–COF is synthesized using triformylpholoroglucinol and 2,5‐diaminohydroquinone dihydrochloride under solvothermal conditions. The accommodation of such exceptional Li+ ion content in the TP–OH–COF is achieved by alternately tethering redox‐active hydroxyl and carbonyl sites on the pore walls. Owing to this unique chemical/structural feature, the TP–OH–COF delivers a high specific capacity of 764.1 mAh g–1, and capacity retention of 63% after 8000 cycles at a fast current density of 5.0 A g–1. A redox‐active COF with alternate tethering of redox‐active hydroxyl and carbonyl sites on the pore walls is demonstrated as an organic‐based, ultralong cyclable high‐capacity LIB anode material. This COF electrode accommodated 30 Li+ ions owing to its unique framework structure and materials chemistry, which has never been reported in previous studies on COF‐based electrode materials.
Author	Han, Diandian Mi, Liwei Yang, Xiubei Park, Sodam Wang, Yanjie Li, Zhongping Zhai, Lipeng Lee, Sang‐Young Li, Gaojie
Author_xml	– sequence: 1 givenname: Lipeng surname: Zhai fullname: Zhai, Lipeng organization: Zhongyuan University of Technology – sequence: 2 givenname: Gaojie surname: Li fullname: Li, Gaojie organization: Zhongyuan University of Technology – sequence: 3 givenname: Xiubei surname: Yang fullname: Yang, Xiubei organization: Zhongyuan University of Technology – sequence: 4 givenname: Sodam surname: Park fullname: Park, Sodam organization: Yonsei University – sequence: 5 givenname: Diandian surname: Han fullname: Han, Diandian organization: Zhongyuan University of Technology – sequence: 6 givenname: Liwei surname: Mi fullname: Mi, Liwei email: liwei_mi@zut.edu.cn, mlwzzu@163.com organization: Zhongyuan University of Technology – sequence: 7 givenname: Yanjie surname: Wang fullname: Wang, Yanjie organization: Zhongyuan University of Technology – sequence: 8 givenname: Zhongping orcidid: 0000-0002-0146-5526 surname: Li fullname: Li, Zhongping email: lizhongping2021@yonsei.ac.kr organization: Yonsei University – sequence: 9 givenname: Sang‐Young orcidid: 0000-0001-7153-0517 surname: Lee fullname: Lee, Sang‐Young email: syleek@yonsei.ac.kr organization: Yonsei University
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Snippet	Covalent organic frameworks (COFs) have attracted considerable attention as a facile and versatile design platform for advanced energy storage materials owing...
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SubjectTerms	Carbonyls Chemical synthesis covalent organic frameworks Electrode materials Energy storage high capacity Lithium-ion batteries Materials science redox‐active carbonyl sites Tethering
Title	30 Li+‐Accommodating Covalent Organic Frameworks as Ultralong Cyclable High‐Capacity Li‐Ion Battery Electrodes
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