Improved solid phase extraction for selective and efficient quantification of sunset yellow in different food samples using a novel molecularly imprinted polymer reinforced by Fe3O4@UiO-66-NH2
•Successful preparation of a novel molecularly imprinted polymer reinforced by Fe3O4@UIO-66-NH2 nanocomposite was presented.•Combination of Fe3O4@UIO-66-NH2 and MIP technique exhibited excellent selectivity and high efficiency.•Application in different food samples were successful. The overuse of sy...
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| Veröffentlicht in: | Food chemistry Jg. 357; S. 129782 |
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| Format: | Journal Article |
| Sprache: | Englisch |
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Elsevier Ltd
30.09.2021
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| ISSN: | 0308-8146, 1873-7072, 1873-7072 |
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| Abstract | •Successful preparation of a novel molecularly imprinted polymer reinforced by Fe3O4@UIO-66-NH2 nanocomposite was presented.•Combination of Fe3O4@UIO-66-NH2 and MIP technique exhibited excellent selectivity and high efficiency.•Application in different food samples were successful.
The overuse of synthetic dyes in food products has gradually increased in recent years, resulting food safety and human health has become a global issue. An innovative design of a magnetic molecularly imprinted polymer (Fe3O4@UiO-66-NH2@MIP) for efficient, fast, and selective determination of sunset yellow (SY) from different food products was described in this study. The absorption properties of Fe3O4@UiO-66-NH2@MIP were elucidated by adsorption kinetics, isotherms, reusability, and selectivity experiments. Because of the incorporation of porous Fe3O4@UiO-66-NH2nanocomposite into molecularly imprinted polymer an efficient nanosorbent with a short equilibrium time, a high adsorption capacity, and a good imprinting factor was finally obtained. The porous Fe3O4@UiO-66-NH2@MIP are also used for quantification of the SY. Under optimal conditions, good linearity (R2 0.9964) in the range of 1.0–120 mg L−1 and a low limit of detection (0.41 mg L−1) was observed with satisfactory recoveries (92.50–106.1%) and excellent reusability (RSD ≤ 6.6% after 12 cycles). |
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| AbstractList | •Successful preparation of a novel molecularly imprinted polymer reinforced by Fe3O4@UIO-66-NH2 nanocomposite was presented.•Combination of Fe3O4@UIO-66-NH2 and MIP technique exhibited excellent selectivity and high efficiency.•Application in different food samples were successful.
The overuse of synthetic dyes in food products has gradually increased in recent years, resulting food safety and human health has become a global issue. An innovative design of a magnetic molecularly imprinted polymer (Fe3O4@UiO-66-NH2@MIP) for efficient, fast, and selective determination of sunset yellow (SY) from different food products was described in this study. The absorption properties of Fe3O4@UiO-66-NH2@MIP were elucidated by adsorption kinetics, isotherms, reusability, and selectivity experiments. Because of the incorporation of porous Fe3O4@UiO-66-NH2nanocomposite into molecularly imprinted polymer an efficient nanosorbent with a short equilibrium time, a high adsorption capacity, and a good imprinting factor was finally obtained. The porous Fe3O4@UiO-66-NH2@MIP are also used for quantification of the SY. Under optimal conditions, good linearity (R2 0.9964) in the range of 1.0–120 mg L−1 and a low limit of detection (0.41 mg L−1) was observed with satisfactory recoveries (92.50–106.1%) and excellent reusability (RSD ≤ 6.6% after 12 cycles). The overuse of synthetic dyes in food products has gradually increased in recent years, resulting food safety and human health has become a global issue. An innovative design of a magnetic molecularly imprinted polymer (Fe3O4@UiO-66-NH2@MIP) for efficient, fast, and selective determination of sunset yellow (SY) from different food products was described in this study. The absorption properties of Fe3O4@UiO-66-NH2@MIP were elucidated by adsorption kinetics, isotherms, reusability, and selectivity experiments. Because of the incorporation of porous Fe3O4@UiO-66-NH2nanocomposite into molecularly imprinted polymer an efficient nanosorbent with a short equilibrium time, a high adsorption capacity, and a good imprinting factor was finally obtained. The porous Fe3O4@UiO-66-NH2@MIP are also used for quantification of the SY. Under optimal conditions, good linearity (R2 0.9964) in the range of 1.0-120 mg L-1 and a low limit of detection (0.41 mg L-1) was observed with satisfactory recoveries (92.50-106.1%) and excellent reusability (RSD ≤ 6.6% after 12 cycles).The overuse of synthetic dyes in food products has gradually increased in recent years, resulting food safety and human health has become a global issue. An innovative design of a magnetic molecularly imprinted polymer (Fe3O4@UiO-66-NH2@MIP) for efficient, fast, and selective determination of sunset yellow (SY) from different food products was described in this study. The absorption properties of Fe3O4@UiO-66-NH2@MIP were elucidated by adsorption kinetics, isotherms, reusability, and selectivity experiments. Because of the incorporation of porous Fe3O4@UiO-66-NH2nanocomposite into molecularly imprinted polymer an efficient nanosorbent with a short equilibrium time, a high adsorption capacity, and a good imprinting factor was finally obtained. The porous Fe3O4@UiO-66-NH2@MIP are also used for quantification of the SY. Under optimal conditions, good linearity (R2 0.9964) in the range of 1.0-120 mg L-1 and a low limit of detection (0.41 mg L-1) was observed with satisfactory recoveries (92.50-106.1%) and excellent reusability (RSD ≤ 6.6% after 12 cycles). The overuse of synthetic dyes in food products has gradually increased in recent years, resulting food safety and human health has become a global issue. An innovative design of a magnetic molecularly imprinted polymer (Fe₃O₄@UiO-66-NH₂@MIP) for efficient, fast, and selective determination of sunset yellow (SY) from different food products was described in this study. The absorption properties of Fe₃O₄@UiO-66-NH₂@MIP were elucidated by adsorption kinetics, isotherms, reusability, and selectivity experiments. Because of the incorporation of porous Fe₃O₄@UiO-66-NH₂nanocomposite into molecularly imprinted polymer an efficient nanosorbent with a short equilibrium time, a high adsorption capacity, and a good imprinting factor was finally obtained. The porous Fe₃O₄@UiO-66-NH₂@MIP are also used for quantification of the SY. Under optimal conditions, good linearity (R² 0.9964) in the range of 1.0–120 mg L⁻¹ and a low limit of detection (0.41 mg L⁻¹) was observed with satisfactory recoveries (92.50–106.1%) and excellent reusability (RSD ≤ 6.6% after 12 cycles). |
| ArticleNumber | 129782 |
| Author | Sadeghian, Reihaneh Hatamluyi, Behnaz Malek, Farhad Boroushaki, Mohammad Taher |
| Author_xml | – sequence: 1 givenname: Behnaz surname: Hatamluyi fullname: Hatamluyi, Behnaz organization: Department of Pharmacology, Faculty of Medicine, Mashhad University of Medical Sciences, Mashhad, Iran – sequence: 2 givenname: Reihaneh surname: Sadeghian fullname: Sadeghian, Reihaneh organization: Medical Plants Research Center, Basic Health Sciences Institute, Shahrekord University of Medical Sciences, Shahrekord, Iran – sequence: 3 givenname: Farhad surname: Malek fullname: Malek, Farhad organization: Department of Internal Medicine, Kosar Hospital, Semnan University of Medical Sciences, Semnan, Iran – sequence: 4 givenname: Mohammad Taher surname: Boroushaki fullname: Boroushaki, Mohammad Taher email: BoroushakiMT@mums.ac.ir organization: Department of Pharmacology, Faculty of Medicine, Mashhad University of Medical Sciences, Mashhad, Iran |
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| Keywords | Metal organic framework Magnetic molecularly imprinted polymer Sunset yellow Adsorption |
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| Snippet | •Successful preparation of a novel molecularly imprinted polymer reinforced by Fe3O4@UIO-66-NH2 nanocomposite was presented.•Combination of Fe3O4@UIO-66-NH2... The overuse of synthetic dyes in food products has gradually increased in recent years, resulting food safety and human health has become a global issue. An... |
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| SubjectTerms | absorption Adsorption design detection limit food chemistry food safety human health Magnetic molecularly imprinted polymer magnetism Metal organic framework molecular imprinting polymers solid phase extraction Sunset yellow |
| Title | Improved solid phase extraction for selective and efficient quantification of sunset yellow in different food samples using a novel molecularly imprinted polymer reinforced by Fe3O4@UiO-66-NH2 |
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