Catalytic surface development of novel nickel plate catalyst with combined thermally annealed platinum and alumina coatings for steam methane reforming

Catalytically active surface of small nickel (min 99 wt%) plates for steam methane reforming was enhanced by successive temperature programmed oxidation−reduction (TPO−TPR) pretreatment and combined physical vapor deposition of Pt and Al2O3. The effect of annealing time, temperature, order and numbe...

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Vydané v:	International journal of hydrogen energy Ročník 38; číslo 3; s. 1419 - 1429
Hlavní autori:	Obradović, Ana, Likozar, Blaž, Levec, Janez
Médium:	Journal Article
Jazyk:	English
Vydavateľské údaje:	Kidlington Elsevier Ltd 06.02.2013 Elsevier
Predmet:	Activity Aluminum oxide Applied sciences Catalysis Catalysts: preparations and properties Chemistry Energy Exact sciences and technology Fuels Gas industry General and physical chemistry Ni/Pt/Al2O3 Physical vapor deposition Spillover Steam methane reforming Structured plate catalyst Theory of reactions, general kinetics. Catalysis. Nomenclature, chemical documentation, computer chemistry Physical vapor deposition Activity Spillover Ni/Pt/Al2O3 Structured plate catalyst Steam methane reforming Methane Aluminium oxide Coated material O Platinum Ni/Pt/Al Nickel Steam reforming Catalyst activity Catalyst
ISSN:	0360-3199, 1879-3487
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Abstract	Catalytically active surface of small nickel (min 99 wt%) plates for steam methane reforming was enhanced by successive temperature programmed oxidation−reduction (TPO−TPR) pretreatment and combined physical vapor deposition of Pt and Al2O3. The effect of annealing time, temperature, order and number of coatings on the catalytic activity was investigated by means of a pulse technique at the reaction temperature of 760 °C. The most active and stable surface phases resulted after the successively deposited layers of Pt, Al2O3, and Pt had been annealed for 12 h onto 2-cycle TPO−TPR pretreated nickel plate at the temperature of 700 °C in a circulating atmosphere of N2. The durability performance of the so-prepared surface phases on a specifically structured plate catalyst element (diameter 43 mm and length 42 mm) was tested in a tubular reactor for some 70 h in temperature range 500−650 °C. Deactivation was mainly caused by carbon surface deposition. Structured nickel (Ni) plate catalyst for steam methane reforming (SMR) with enhanced activity by platinum (Pt) and alumina (Al2O3) coating. [Display omitted] ► Catalytic enhancement of structured Ni-plate reforming catalyst was investigated. ► Oxidation–reduction process and deposition of Pt and Al2O3 were done on Ni plates. ► Catalytic activity of enhanced Ni-plate samples was tested by pulse technique. ► Structured Ni-plate catalyst was examined in continuous differential reactor. ► Catalyst deactivation at conditions chosen was caused mainly by carbon deposition.
AbstractList	Catalytically active surface of small nickel (min 99 wt%) plates for steam methane reforming was enhanced by successive temperature programmed oxidation−reduction (TPO−TPR) pretreatment and combined physical vapor deposition of Pt and Al2O3. The effect of annealing time, temperature, order and number of coatings on the catalytic activity was investigated by means of a pulse technique at the reaction temperature of 760 °C. The most active and stable surface phases resulted after the successively deposited layers of Pt, Al2O3, and Pt had been annealed for 12 h onto 2-cycle TPO−TPR pretreated nickel plate at the temperature of 700 °C in a circulating atmosphere of N2. The durability performance of the so-prepared surface phases on a specifically structured plate catalyst element (diameter 43 mm and length 42 mm) was tested in a tubular reactor for some 70 h in temperature range 500−650 °C. Deactivation was mainly caused by carbon surface deposition. Structured nickel (Ni) plate catalyst for steam methane reforming (SMR) with enhanced activity by platinum (Pt) and alumina (Al2O3) coating. [Display omitted] ► Catalytic enhancement of structured Ni-plate reforming catalyst was investigated. ► Oxidation–reduction process and deposition of Pt and Al2O3 were done on Ni plates. ► Catalytic activity of enhanced Ni-plate samples was tested by pulse technique. ► Structured Ni-plate catalyst was examined in continuous differential reactor. ► Catalyst deactivation at conditions chosen was caused mainly by carbon deposition. Catalytically active surface of small nickel (min 99 wt%) plates for steam methane reforming was enhanced by successive temperature programmed oxidation-reduction (TPO-TPR) pretreatment and combined physical vapor deposition of Pt and Al2O3. The effect of annealing time, temperature, order and number of coatings on the catalytic activity was investigated by means of a pulse technique at the reaction temperature of 760 degree C. The most active and stable surface phases resulted after the successively deposited layers of Pt, Al2O3, and Pt had been annealed for 12 h onto 2-cycle TPO-TPR pretreated nickel plate at the temperature of 700 degree C in a circulating atmosphere of N2. The durability performance of the so-prepared surface phases on a specifically structured plate catalyst element (diameter 43 mm and length 42 mm) was tested in a tubular reactor for some 70 h in temperature range 500-650 degree C. Deactivation was mainly caused by carbon surface deposition.
Author	Obradović, Ana Levec, Janez Likozar, Blaž
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Keywords	Physical vapor deposition Activity Spillover Ni/Pt/Al2O3 Structured plate catalyst Steam methane reforming Methane Aluminium oxide Coated material O Platinum Ni/Pt/Al Nickel Steam reforming Catalyst activity Catalyst
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Snippet	Catalytically active surface of small nickel (min 99 wt%) plates for steam methane reforming was enhanced by successive temperature programmed... Catalytically active surface of small nickel (min 99 wt%) plates for steam methane reforming was enhanced by successive temperature programmed...
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SubjectTerms	Activity Aluminum oxide Applied sciences Catalysis Catalysts: preparations and properties Chemistry Energy Exact sciences and technology Fuels Gas industry General and physical chemistry Ni/Pt/Al2O3 Physical vapor deposition Spillover Steam methane reforming Structured plate catalyst Theory of reactions, general kinetics. Catalysis. Nomenclature, chemical documentation, computer chemistry
Title	Catalytic surface development of novel nickel plate catalyst with combined thermally annealed platinum and alumina coatings for steam methane reforming
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