Salts of amino acids with hexafluorosilicate anion
In this work we present our preliminary results on the systematic search for salts of amino acids with hexafluorosilicate (SiF62−) anion. Three types of simple salts have been obtained: 2A+·SiF62− (2Gly+·SiF62−, 2l-Phe+·SiF62−, 2l-Val+·SiF62−, 2l-Glu+·SiF62−, 2l-His+·SiF62−), A2+·SiF62− (l-His2+·SiF...
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| Published in: | Journal of crystal growth Vol. 362; pp. 162 - 166 |
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| Language: | English |
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Elsevier B.V
01.01.2013
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| Abstract | In this work we present our preliminary results on the systematic search for salts of amino acids with hexafluorosilicate (SiF62−) anion. Three types of simple salts have been obtained: 2A+·SiF62− (2Gly+·SiF62−, 2l-Phe+·SiF62−, 2l-Val+·SiF62−, 2l-Glu+·SiF62−, 2l-His+·SiF62−), A2+·SiF62− (l-His2+·SiF62−, l-Lys2+·SiF62−, l-Orn2+·SiF62−) and 2(A···A+)·SiF62− (2(Bet···Bet+)·SiF62−). Furthermore, one example of mixed salts with different anions, including SiF62−, viz. 2l-His2+·2BF4−·SiF62−·2H2O is presented. It was found that the salts of amino acids with SiF62− anion tend to form crystal hydrates and the SiF62− anion is often disordered within the structures.
► First report on a new class of amino acids salts with hexafluorosilicate anion. ► Crystals of three types of simple salts are reported. ► An example of mixed salts with different anions is presented. |
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| AbstractList | In this work we present our preliminary results on the systematic search for salts of amino acids with hexafluorosilicate (SiF62−) anion. Three types of simple salts have been obtained: 2A+·SiF62− (2Gly+·SiF62−, 2l-Phe+·SiF62−, 2l-Val+·SiF62−, 2l-Glu+·SiF62−, 2l-His+·SiF62−), A2+·SiF62− (l-His2+·SiF62−, l-Lys2+·SiF62−, l-Orn2+·SiF62−) and 2(A···A+)·SiF62− (2(Bet···Bet+)·SiF62−). Furthermore, one example of mixed salts with different anions, including SiF62−, viz. 2l-His2+·2BF4−·SiF62−·2H2O is presented. It was found that the salts of amino acids with SiF62− anion tend to form crystal hydrates and the SiF62− anion is often disordered within the structures.
► First report on a new class of amino acids salts with hexafluorosilicate anion. ► Crystals of three types of simple salts are reported. ► An example of mixed salts with different anions is presented. In this work we present our preliminary results on the systematic search for salts of amino acids with hexafluorosilicate (SiF62-) anion. Three types of simple salts have been obtained: 2A+ADTSiF62- (2Gly+ADTSiF62-, 2l-Phe+ADTSiF62-, 2l-Val+ADTSiF62-, 2l-Glu+ADTSiF62-, 2l-His+ADTSiF62-), A2+ADTSiF62- (l-His2+ADTSiF62-, l-Lys2+ADTSiF62-, l-Orn2+ADTSiF62-) and 2(AADTADTADTA+)ADTSiF62- (2(BetADTADTADTBet+)ADTSiF62-). Furthermore, one example of mixed salts with different anions, including SiF62-, viz. 2l-His2+ADT2BF4-ADTSiF62-ADT2H2O is presented. It was found that the salts of amino acids with SiF62- anion tend to form crystal hydrates and the SiF62- anion is often disordered within the structures. |
| Author | Ghazaryan, V.V. Fleck, M. Petrosyan, A.M. |
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| Cites_doi | 10.1524/zkri.2010.1269 10.1016/j.molstruc.2010.08.020 10.1016/j.molstruc.2010.05.022 10.1002/zaac.19885590103 10.1117/12.890269 10.1016/j.molstruc.2010.09.039 10.1016/j.molstruc.2010.09.010 10.1016/0022-2860(95)08981-0 |
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| Keywords | B1. Hexafluorosilicates A2. Growth from solution B1. Amino acids salts Crystal growth Salts Crystal form Organic conductors Amino acids Hexafluosilicates Growth from solution Hydrates |
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| References | Fleck, Ghazaryan, Petrosyan (bib10) 2011; 2 Petrosyan (bib12) 2010; 1 Ghazaryan, Fleck, Petrosyan (bib7) 2010; 982 Ghazaryan, Fleck, Petrosyan (bib5) 2011; 7998 Nakamoto (bib13) 2009 Ghazaryan, Fleck, Petrosyan (bib9) 2011; 2 Narayana, Rai, Dharmaprakash, Harrison (bib2) 2007; C63 Fleck, Ghazaryan, Petrosyan (bib3) 2010; 984 Ghazaryan, Fleck, Petrosyan (bib4) 2010; 977 Baran, Drozd, Lis, Ratajczak (bib11) 1995; 372 Petrosyan, Fleck, Ghazaryan (bib6) 2010; 225 Mootz, Oellers (bib1) 1988; 559 Ghazaryan, Fleck, Petrosyan (bib8) 2010; 984 Ghazaryan (10.1016/j.jcrysgro.2011.11.017_bib5) 2011; 7998 Mootz (10.1016/j.jcrysgro.2011.11.017_bib1) 1988; 559 Ghazaryan (10.1016/j.jcrysgro.2011.11.017_bib4) 2010; 977 Ghazaryan (10.1016/j.jcrysgro.2011.11.017_bib7) 2010; 982 Petrosyan (10.1016/j.jcrysgro.2011.11.017_bib12) 2010; 1 Nakamoto (10.1016/j.jcrysgro.2011.11.017_bib13) 2009 Narayana (10.1016/j.jcrysgro.2011.11.017_bib2) 2007; C63 Baran (10.1016/j.jcrysgro.2011.11.017_bib11) 1995; 372 Ghazaryan (10.1016/j.jcrysgro.2011.11.017_bib8) 2010; 984 Fleck (10.1016/j.jcrysgro.2011.11.017_bib3) 2010; 984 Ghazaryan (10.1016/j.jcrysgro.2011.11.017_bib9) 2011; 2 Petrosyan (10.1016/j.jcrysgro.2011.11.017_bib6) 2010; 225 Fleck (10.1016/j.jcrysgro.2011.11.017_bib10) 2011; 2 |
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| Snippet | In this work we present our preliminary results on the systematic search for salts of amino acids with hexafluorosilicate (SiF62−) anion. Three types of simple... In this work we present our preliminary results on the systematic search for salts of amino acids with hexafluorosilicate (SiF62-) anion. Three types of simple... |
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| SubjectTerms | A2. Growth from solution Amino acids Anions B1. Amino acids salts B1. Hexafluorosilicates Condensed matter: structure, mechanical and thermal properties Cross-disciplinary physics: materials science; rheology Crystal growth Crystal structure Exact sciences and technology Growth from solutions Hydrates Inorganic compounds Materials science Methods of crystal growth; physics of crystal growth Physics Searching Structure of solids and liquids; crystallography Structure of specific crystalline solids |
| Title | Salts of amino acids with hexafluorosilicate anion |
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