Decane hydroconversion on bifunctional Zeogrid and nano-zeolite assembled from aluminosilicate nanoslabs of MFI framework type
Nanoslabs with MFI zeolite framework topology and having aluminosilicate composition were assembled into nanosize crystals and Zeogrid materials. The nanosize MFI zeolite had a particle size of ca. 200 nm. Micron sized Zeogrid spheres were assembled by precipitating a nanoslab suspension through cet...
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| Vydané v: | Applied catalysis. A, General Ročník 257; číslo 1; s. 7 - 17 |
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| Hlavní autori: | , , , , , , , , , , , |
| Médium: | Journal Article |
| Jazyk: | English |
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Amsterdam
Elsevier B.V
01.01.2004
Elsevier |
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| ISSN: | 0926-860X, 1873-3875 |
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| Abstract | Nanoslabs with MFI zeolite framework topology and having aluminosilicate composition were assembled into nanosize crystals and Zeogrid materials. The nanosize MFI zeolite had a particle size of ca. 200
nm. Micron sized Zeogrid spheres were assembled by precipitating a nanoslab suspension through cetyltrimethylammonium bromide (CTAB) addition and calcination of the precipitate. Zeogrid is a layered structure. Nitrogen adsorption isotherms on Zeogrid revealed the presence of two types of porosity: ultra-microporosity characteristic of MFI type framework and super-microporosity consisting of interlinked parallellopipedic voids occurring in between individual nanoslabs. The incorporation of aluminum in the tetrahedral framework was confirmed with
27
Al
MAS NMR. The materials were converted into bifunctional catalysts and evaluated in decane hydroconversion. Surprisingly, the nanosize MFI zeolite and the Zeogrids assembled from MFI type nanoslabs did not show the product selectivity observed with ZSM-5 zeolite prepared using hydrothermal gel method, but rather behaved like large pore zeolites. The unusual behavior is linked with the predominance of wide openings terminating zigzag pores on nanoslab surfaces. |
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| AbstractList | Nanoslabs with MFI zeolite framework topology and having aluminosilicate composition were assembled into nanosize crystals and Zeogrid materials. The nanosize MFI zeolite had a particle size of ca. 200
nm. Micron sized Zeogrid spheres were assembled by precipitating a nanoslab suspension through cetyltrimethylammonium bromide (CTAB) addition and calcination of the precipitate. Zeogrid is a layered structure. Nitrogen adsorption isotherms on Zeogrid revealed the presence of two types of porosity: ultra-microporosity characteristic of MFI type framework and super-microporosity consisting of interlinked parallellopipedic voids occurring in between individual nanoslabs. The incorporation of aluminum in the tetrahedral framework was confirmed with
27
Al
MAS NMR. The materials were converted into bifunctional catalysts and evaluated in decane hydroconversion. Surprisingly, the nanosize MFI zeolite and the Zeogrids assembled from MFI type nanoslabs did not show the product selectivity observed with ZSM-5 zeolite prepared using hydrothermal gel method, but rather behaved like large pore zeolites. The unusual behavior is linked with the predominance of wide openings terminating zigzag pores on nanoslab surfaces. |
| Author | Collignon, François Houthoofd, Kristof Baron, Gino V Denayer, Joeri F.M Huybrechts, Ward Isacker, Annabel van Kremer, Sebastien P.B Kirschhock, Christine E.A Marin, Guy B Jacobs, Pierre A Martens, Johan A Aerts, Alexander |
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| Cites_doi | 10.1016/S1387-1811(02)00558-9 10.1016/B978-044450701-3/50375-X 10.1016/S1387-1811(00)00215-8 10.1016/0166-9834(91)80009-L 10.1039/c39810000591 10.1016/0079-6565(84)80007-2 10.1016/0144-2449(87)90087-X 10.1039/dc9817200317 10.1016/0144-2449(94)90191-0 10.1016/S1387-1811(00)00190-6 10.1021/jp990297r 10.1016/0144-2449(94)90121-X 10.1021/jp992272y 10.1016/S1387-1811(98)00172-3 10.1021/j100002a047 10.1002/1616-3028(20020418)12:4<286::AID-ADFM286>3.0.CO;2-M 10.1016/0166-9834(83)80058-X 10.1016/S0926-860X(02)00536-7 10.1021/ja01228a038 10.1016/0144-2449(84)90013-7 10.1021/jp990296z 10.1023/A:1019061714047 10.1016/0144-2449(84)90044-7 10.1002/1521-3773(20010716)40:14<2637::AID-ANIE2637>3.0.CO;2-7 |
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| Keywords | Nano-zeolites Hydroconversion Super-micropores MFI zeolite Zeogrid ZSM-5 Mixed catalyst Catalytic reaction Hydrocarbon Isomerization Aluminosilicates Nanostructure Zeolite Hydrogenation Porous material Molecular sieve Heterogeneous catalysis Decane Microporosity Preparation Alkane |
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| Snippet | Nanoslabs with MFI zeolite framework topology and having aluminosilicate composition were assembled into nanosize crystals and Zeogrid materials. The nanosize... |
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| SubjectTerms | Catalysis Catalytic reactions Chemistry Exact sciences and technology General and physical chemistry Hydroconversion MFI zeolite Nano-zeolites Super-micropores Theory of reactions, general kinetics. Catalysis. Nomenclature, chemical documentation, computer chemistry Zeogrid ZSM-5 |
| Title | Decane hydroconversion on bifunctional Zeogrid and nano-zeolite assembled from aluminosilicate nanoslabs of MFI framework type |
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