Thermoplastic polyurethane-carbon black nanocomposite coating: Fabrication and solid particle erosion resistance

Carbon black (CB)/thermoplastic polyurethane (TPU) nanocomposites with a range of nanoparticle loadings were prepared successfully by using a joint co-coagulation technique and hot pressing. The presence of hydrogen bonding interactions between the CB particles and TPU chains was identified from the...

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Veröffentlicht in:	Polymer (Guilford) Jg. 158; S. 381 - 390
Hauptverfasser:	Dong, Mengyao, Li, Qiang, Liu, Hu, Liu, Chuntai, Wujcik, Evan K., Shao, Qian, Ding, Tao, Mai, Xianmin, Shen, Changyu, Guo, Zhanhu
Format:	Journal Article
Sprache:	Englisch
Veröffentlicht:	Kidlington Elsevier Ltd 05.12.2018 Elsevier BV
Schlagworte:	Black carbon Bonded joints Calorimetry Carbon Carbon black Coagulation Differential scanning calorimetry Ductile erosion Erosion rates Erosion resistance Fabrication Fourier transforms Heat conductivity Hot pressing Hydrogen bonding Impact velocity Infrared spectroscopy Mechanical properties Nanocomposites Nanoparticles Polyurethane Polyurethane resins Protective coatings Solid particle erosion Tensile strength Thermal conductivity Thermal stability Thermoplastic polyurethane Urethane thermoplastic elastomers Thermoplastic polyurethane Solid particle erosion Carbon black
ISSN:	0032-3861, 1873-2291
Online-Zugang:	Volltext
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Abstract	Carbon black (CB)/thermoplastic polyurethane (TPU) nanocomposites with a range of nanoparticle loadings were prepared successfully by using a joint co-coagulation technique and hot pressing. The presence of hydrogen bonding interactions between the CB particles and TPU chains was identified from the results of Fourier transform infrared (FT-IR) spectroscopy and differential scanning calorimetry (DSC). Uniform dispersion of CB particles throughout the TPU matrix improved the overall mechanical properties of the TPU nanocomposites, as compared with the neat TPU. The thermal conductivity and thermal stability of the CB/TPU nanocomposites were also found to be enhanced with increasing the CB loading. All samples exhibited a rapid increase of erosion rate with the impact velocity between 20 and 30 m/s. The largest and smallest erosion rates (ER) were observed at 30° and 90° impact angle, respectively, for all CB/TPU nanocomposites. This shows a typical ductile erosion behavior in this material. In addition, the ER (TPU-2CB > TPU-12CB > TPU > TPU-6CB) under all test conditions showed an opposite trend to the tensile strength. These results indicate that the CB/TPU nanocomposites are suitable for protective coatings. [Display omitted] •Thermoplastic polyurethane nanocomposites were fabricated using co-coagulation plus compression molding technique.•Uniform dispersion of CB nanoparticles effectively enhanced the tensile strength of the nanocomposites.•The solid particle erosion behavior was characterized by different impact angles, velocities and time.•The erosion rate showed an opposite trend to the tensile strength.
AbstractList	Carbon black (CB)/thermoplastic polyurethane (TPU) nanocomposites with a range of nanoparticle loadings were prepared successfully by using a joint co-coagulation technique and hot pressing. The presence of hydrogen bonding interactions between the CB particles and TPU chains was identified from the results of Fourier transform infrared (FT-IR) spectroscopy and differential scanning calorimetry (DSC). Uniform dispersion of CB particles throughout the TPU matrix improved the overall mechanical properties of the TPU nanocomposites, as compared with the neat TPU. The thermal conductivity and thermal stability of the CB/TPU nanocomposites were also found to be enhanced with increasing the CB loading. All samples exhibited a rapid increase of erosion rate with the impact velocity between 20 and 30 m/s. The largest and smallest erosion rates (ER) were observed at 30° and 90° impact angle, respectively, for all CB/TPU nanocomposites. This shows a typical ductile erosion behavior in this material. In addition, the ER (TPU-2CB > TPU-12CB > TPU > TPU-6CB) under all test conditions showed an opposite trend to the tensile strength. These results indicate that the CB/TPU nanocomposites are suitable for protective coatings. Carbon black (CB)/thermoplastic polyurethane (TPU) nanocomposites with a range of nanoparticle loadings were prepared successfully by using a joint co-coagulation technique and hot pressing. The presence of hydrogen bonding interactions between the CB particles and TPU chains was identified from the results of Fourier transform infrared (FT-IR) spectroscopy and differential scanning calorimetry (DSC). Uniform dispersion of CB particles throughout the TPU matrix improved the overall mechanical properties of the TPU nanocomposites, as compared with the neat TPU. The thermal conductivity and thermal stability of the CB/TPU nanocomposites were also found to be enhanced with increasing the CB loading. All samples exhibited a rapid increase of erosion rate with the impact velocity between 20 and 30 m/s. The largest and smallest erosion rates (ER) were observed at 30° and 90° impact angle, respectively, for all CB/TPU nanocomposites. This shows a typical ductile erosion behavior in this material. In addition, the ER (TPU-2CB > TPU-12CB > TPU > TPU-6CB) under all test conditions showed an opposite trend to the tensile strength. These results indicate that the CB/TPU nanocomposites are suitable for protective coatings. [Display omitted] •Thermoplastic polyurethane nanocomposites were fabricated using co-coagulation plus compression molding technique.•Uniform dispersion of CB nanoparticles effectively enhanced the tensile strength of the nanocomposites.•The solid particle erosion behavior was characterized by different impact angles, velocities and time.•The erosion rate showed an opposite trend to the tensile strength.
Author	Li, Qiang Mai, Xianmin Liu, Hu Liu, Chuntai Shen, Changyu Wujcik, Evan K. Ding, Tao Dong, Mengyao Shao, Qian Guo, Zhanhu
Author_xml	– sequence: 1 givenname: Mengyao surname: Dong fullname: Dong, Mengyao organization: School of Materials Science and Engineering, Key Laboratory of Materials Processing and Mold (Zhengzhou University), Ministry of Education, National Engineering Research Center for Advanced Polymer Processing Technology, Zhengzhou University, Zhengzhou, 450002, Henan, China – sequence: 2 givenname: Qiang surname: Li fullname: Li, Qiang organization: School of Materials Science and Engineering, Key Laboratory of Materials Processing and Mold (Zhengzhou University), Ministry of Education, National Engineering Research Center for Advanced Polymer Processing Technology, Zhengzhou University, Zhengzhou, 450002, Henan, China – sequence: 3 givenname: Hu orcidid: 0000-0003-3840-8135 surname: Liu fullname: Liu, Hu email: liuhu@zzu.edu.cn organization: School of Materials Science and Engineering, Key Laboratory of Materials Processing and Mold (Zhengzhou University), Ministry of Education, National Engineering Research Center for Advanced Polymer Processing Technology, Zhengzhou University, Zhengzhou, 450002, Henan, China – sequence: 4 givenname: Chuntai surname: Liu fullname: Liu, Chuntai email: ctliu@zzu.edu.cn organization: School of Materials Science and Engineering, Key Laboratory of Materials Processing and Mold (Zhengzhou University), Ministry of Education, National Engineering Research Center for Advanced Polymer Processing Technology, Zhengzhou University, Zhengzhou, 450002, Henan, China – sequence: 5 givenname: Evan K. orcidid: 0000-0002-4966-863X surname: Wujcik fullname: Wujcik, Evan K. organization: Materials Engineering and Nanosensors [MEAN] Laboratory, Department of Chemical and Biological Engineering, The University of Alabama, Tuscaloosa, AL, 35487, USA – sequence: 6 givenname: Qian surname: Shao fullname: Shao, Qian organization: College of Materials Science and Engineering, Shandong University of Science and Technology, Qingdao, 266590, China – sequence: 7 givenname: Tao surname: Ding fullname: Ding, Tao email: dingtao@henu.edu.cn organization: College of Chemistry and Chemical Engineering, Henan University, Kaifeng, 475004, China – sequence: 8 givenname: Xianmin surname: Mai fullname: Mai, Xianmin email: maixianmin@foxmail.com organization: School of Urban Planning and Architecture, Southwest Minzu University, Chengdu, 610041, China – sequence: 9 givenname: Changyu surname: Shen fullname: Shen, Changyu organization: School of Materials Science and Engineering, Key Laboratory of Materials Processing and Mold (Zhengzhou University), Ministry of Education, National Engineering Research Center for Advanced Polymer Processing Technology, Zhengzhou University, Zhengzhou, 450002, Henan, China – sequence: 10 givenname: Zhanhu orcidid: 0000-0003-0134-0210 surname: Guo fullname: Guo, Zhanhu email: zguo10@utk.edu organization: Integrated Composites Laboratory (ICL), Department of Chemical & Biomolecular Engineering, University of Tennessee, Knoxville, TN, 37996, USA
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PublicationYear	2018
Publisher	Elsevier Ltd Elsevier BV
Publisher_xml	– name: Elsevier Ltd – name: Elsevier BV
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SubjectTerms	Black carbon Bonded joints Calorimetry Carbon Carbon black Coagulation Differential scanning calorimetry Ductile erosion Erosion rates Erosion resistance Fabrication Fourier transforms Heat conductivity Hot pressing Hydrogen bonding Impact velocity Infrared spectroscopy Mechanical properties Nanocomposites Nanoparticles Polyurethane Polyurethane resins Protective coatings Solid particle erosion Tensile strength Thermal conductivity Thermal stability Thermoplastic polyurethane Urethane thermoplastic elastomers
Title	Thermoplastic polyurethane-carbon black nanocomposite coating: Fabrication and solid particle erosion resistance
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