Ultrafast Porous Carbon Activation Promises High‐Energy Density Supercapacitors

Activated porous carbons (APCs) are traditionally produced by heat treatment and KOH activation, where the production time can be as long as 2 h, and the produced activated porous carbons suffer from relatively low specific surface area and porosity. In this study, the fast high‐temperature shock (H...

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Published in:	Small (Weinheim an der Bergstrasse, Germany) Vol. 18; no. 23; pp. e2200954 - n/a
Main Authors:	Liu, Zhedong, Duan, Cunpeng, Dou, Shuming, Yuan, Qunyao, Xu, Jie, Liu, Wei‐Di, Chen, Yanan
Format:	Journal Article
Language:	English
Published:	Germany Wiley Subscription Services, Inc 01.06.2022
Subjects:	Activated carbon activated porous carbons Energy storage Heat treatment High temperature high‐temperature shock Ionic liquids Nanotechnology Ohmic dissipation Porosity Rapid quenching (metallurgy) Resistance heating Specific surface supercapacitor Supercapacitors Surface area ultrafast synthesis activated porous carbons high-temperature shock ultrafast synthesis supercapacitor
ISSN:	1613-6810, 1613-6829, 1613-6829
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Abstract	Activated porous carbons (APCs) are traditionally produced by heat treatment and KOH activation, where the production time can be as long as 2 h, and the produced activated porous carbons suffer from relatively low specific surface area and porosity. In this study, the fast high‐temperature shock (HTS) carbonization and HTS‐KOH activation method to synthesize activated porous carbons with high specific surface area of ≈843 m2 g‐1, is proposed. During the HTS process, the instant Joule heating (at a heating speed of ≈1100 K s‐1) with high temperature and rapid quenching can effectively produce abundant pores with homogeneous size‐distribution due to the instant melt of KOH into small droplets, which facilitates the interaction between carbon and KOH to form controllable, dense, and small pores. The as‐prepared HTS‐APC‐based supercapacitors deliver a high energy density of 25 Wh kg‐1 at a power density of 582 W kg‐1 in the EMIMBF4 ionic liquid. It is believed that the proposed HTS technique has created a new pathway for manufacturing activated porous carbons with largely enhanced energy density of supercapacitors, which can inspire the development of energy storage materials. The coconut shell, characterized by loose structure and high carbon content, is employed to synthesize activated porous carbon by high‐temperature shock (HTS) progress. The instant Joule heating (at a heating speed of ≈1100 K s–1) with high temperature and rapid quenching facilitates the interaction between carbon and KOH to form controllable, dense, and small pores.
AbstractList	Activated porous carbons (APCs) are traditionally produced by heat treatment and KOH activation, where the production time can be as long as 2 h, and the produced activated porous carbons suffer from relatively low specific surface area and porosity. In this study, the fast high‐temperature shock (HTS) carbonization and HTS‐KOH activation method to synthesize activated porous carbons with high specific surface area of ≈843 m2 g‐1, is proposed. During the HTS process, the instant Joule heating (at a heating speed of ≈1100 K s‐1) with high temperature and rapid quenching can effectively produce abundant pores with homogeneous size‐distribution due to the instant melt of KOH into small droplets, which facilitates the interaction between carbon and KOH to form controllable, dense, and small pores. The as‐prepared HTS‐APC‐based supercapacitors deliver a high energy density of 25 Wh kg‐1 at a power density of 582 W kg‐1 in the EMIMBF4 ionic liquid. It is believed that the proposed HTS technique has created a new pathway for manufacturing activated porous carbons with largely enhanced energy density of supercapacitors, which can inspire the development of energy storage materials. Activated porous carbons (APCs) are traditionally produced by heat treatment and KOH activation, where the production time can be as long as 2 h, and the produced activated porous carbons suffer from relatively low specific surface area and porosity. In this study, the fast high‐temperature shock (HTS) carbonization and HTS‐KOH activation method to synthesize activated porous carbons with high specific surface area of ≈843 m 2 g ‐1 , is proposed. During the HTS process, the instant Joule heating (at a heating speed of ≈1100 K s ‐1 ) with high temperature and rapid quenching can effectively produce abundant pores with homogeneous size‐distribution due to the instant melt of KOH into small droplets, which facilitates the interaction between carbon and KOH to form controllable, dense, and small pores. The as‐prepared HTS‐APC‐based supercapacitors deliver a high energy density of 25 Wh kg ‐1 at a power density of 582 W kg ‐1 in the EMIMBF 4 ionic liquid. It is believed that the proposed HTS technique has created a new pathway for manufacturing activated porous carbons with largely enhanced energy density of supercapacitors, which can inspire the development of energy storage materials. Activated porous carbons (APCs) are traditionally produced by heat treatment and KOH activation, where the production time can be as long as 2 h, and the produced activated porous carbons suffer from relatively low specific surface area and porosity. In this study, the fast high-temperature shock (HTS) carbonization and HTS-KOH activation method to synthesize activated porous carbons with high specific surface area of ≈843 m2 g-1 , is proposed. During the HTS process, the instant Joule heating (at a heating speed of ≈1100 K s-1 ) with high temperature and rapid quenching can effectively produce abundant pores with homogeneous size-distribution due to the instant melt of KOH into small droplets, which facilitates the interaction between carbon and KOH to form controllable, dense, and small pores. The as-prepared HTS-APC-based supercapacitors deliver a high energy density of 25 Wh kg-1 at a power density of 582 W kg-1 in the EMIMBF4 ionic liquid. It is believed that the proposed HTS technique has created a new pathway for manufacturing activated porous carbons with largely enhanced energy density of supercapacitors, which can inspire the development of energy storage materials.Activated porous carbons (APCs) are traditionally produced by heat treatment and KOH activation, where the production time can be as long as 2 h, and the produced activated porous carbons suffer from relatively low specific surface area and porosity. In this study, the fast high-temperature shock (HTS) carbonization and HTS-KOH activation method to synthesize activated porous carbons with high specific surface area of ≈843 m2 g-1 , is proposed. During the HTS process, the instant Joule heating (at a heating speed of ≈1100 K s-1 ) with high temperature and rapid quenching can effectively produce abundant pores with homogeneous size-distribution due to the instant melt of KOH into small droplets, which facilitates the interaction between carbon and KOH to form controllable, dense, and small pores. The as-prepared HTS-APC-based supercapacitors deliver a high energy density of 25 Wh kg-1 at a power density of 582 W kg-1 in the EMIMBF4 ionic liquid. It is believed that the proposed HTS technique has created a new pathway for manufacturing activated porous carbons with largely enhanced energy density of supercapacitors, which can inspire the development of energy storage materials. Activated porous carbons (APCs) are traditionally produced by heat treatment and KOH activation, where the production time can be as long as 2 h, and the produced activated porous carbons suffer from relatively low specific surface area and porosity. In this study, the fast high-temperature shock (HTS) carbonization and HTS-KOH activation method to synthesize activated porous carbons with high specific surface area of ≈843 m g , is proposed. During the HTS process, the instant Joule heating (at a heating speed of ≈1100 K s ) with high temperature and rapid quenching can effectively produce abundant pores with homogeneous size-distribution due to the instant melt of KOH into small droplets, which facilitates the interaction between carbon and KOH to form controllable, dense, and small pores. The as-prepared HTS-APC-based supercapacitors deliver a high energy density of 25 Wh kg at a power density of 582 W kg in the EMIMBF ionic liquid. It is believed that the proposed HTS technique has created a new pathway for manufacturing activated porous carbons with largely enhanced energy density of supercapacitors, which can inspire the development of energy storage materials. Activated porous carbons (APCs) are traditionally produced by heat treatment and KOH activation, where the production time can be as long as 2 h, and the produced activated porous carbons suffer from relatively low specific surface area and porosity. In this study, the fast high‐temperature shock (HTS) carbonization and HTS‐KOH activation method to synthesize activated porous carbons with high specific surface area of ≈843 m2 g‐1, is proposed. During the HTS process, the instant Joule heating (at a heating speed of ≈1100 K s‐1) with high temperature and rapid quenching can effectively produce abundant pores with homogeneous size‐distribution due to the instant melt of KOH into small droplets, which facilitates the interaction between carbon and KOH to form controllable, dense, and small pores. The as‐prepared HTS‐APC‐based supercapacitors deliver a high energy density of 25 Wh kg‐1 at a power density of 582 W kg‐1 in the EMIMBF4 ionic liquid. It is believed that the proposed HTS technique has created a new pathway for manufacturing activated porous carbons with largely enhanced energy density of supercapacitors, which can inspire the development of energy storage materials. The coconut shell, characterized by loose structure and high carbon content, is employed to synthesize activated porous carbon by high‐temperature shock (HTS) progress. The instant Joule heating (at a heating speed of ≈1100 K s–1) with high temperature and rapid quenching facilitates the interaction between carbon and KOH to form controllable, dense, and small pores.
Author	Duan, Cunpeng Yuan, Qunyao Xu, Jie Chen, Yanan Liu, Zhedong Dou, Shuming Liu, Wei‐Di
Author_xml	– sequence: 1 givenname: Zhedong surname: Liu fullname: Liu, Zhedong organization: Tianjin University – sequence: 2 givenname: Cunpeng surname: Duan fullname: Duan, Cunpeng email: cunpengduantju@gmail.com organization: Tianjin University – sequence: 3 givenname: Shuming surname: Dou fullname: Dou, Shuming organization: Tianjin University – sequence: 4 givenname: Qunyao surname: Yuan fullname: Yuan, Qunyao organization: Tianjin University – sequence: 5 givenname: Jie surname: Xu fullname: Xu, Jie organization: Tianjin University – sequence: 6 givenname: Wei‐Di surname: Liu fullname: Liu, Wei‐Di organization: The University of Queensland – sequence: 7 givenname: Yanan orcidid: 0000-0002-6346-6372 surname: Chen fullname: Chen, Yanan email: yananchen@tju.edu.cn organization: Tianjin University
BackLink	https://www.ncbi.nlm.nih.gov/pubmed/35557492$$D View this record in MEDLINE/PubMed
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Snippet	Activated porous carbons (APCs) are traditionally produced by heat treatment and KOH activation, where the production time can be as long as 2 h, and the...
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SubjectTerms	Activated carbon activated porous carbons Energy storage Heat treatment High temperature high‐temperature shock Ionic liquids Nanotechnology Ohmic dissipation Porosity Rapid quenching (metallurgy) Resistance heating Specific surface supercapacitor Supercapacitors Surface area ultrafast synthesis
Title	Ultrafast Porous Carbon Activation Promises High‐Energy Density Supercapacitors
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