Tuning the properties of nickel nanoparticles inside SBA-15 mesopores for enhanced stability in methane reforming
[Display omitted] •Calcination rate affects pore plugging and dispersion of nickel.•Optimum calcination rate enhances nickel stability in dry reforming of methane.•Coke is absent on confined particles of nickel inside the mesopores of SBA-15. The properties of nickel nanoparticles inside the mesopor...
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| Vydané v: | Journal of CO2 utilization Ročník 17; s. 119 - 124 |
|---|---|
| Hlavní autori: | , , , |
| Médium: | Journal Article |
| Jazyk: | English |
| Vydavateľské údaje: |
Elsevier Ltd
01.01.2017
Elsevier |
| Edícia: | Lecture Notes in Electrical Engineering |
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| ISSN: | 2212-9820, 2212-9839 |
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| Abstract | [Display omitted]
•Calcination rate affects pore plugging and dispersion of nickel.•Optimum calcination rate enhances nickel stability in dry reforming of methane.•Coke is absent on confined particles of nickel inside the mesopores of SBA-15.
The properties of nickel nanoparticles inside the mesopores of SBA-15 support were tuned by a careful control of the calcination rate. Ni/SBA-15 catalysts containing 5wt% nickel were prepared following three different calcination rate values (0.25 −0.5 −4.5°Cmin−1). Their properties were characterized by N2-sorption, X-ray diffraction (low and wide angles), temperature programed reduction and transmission electron microscopy. These catalysts were then tested in dry reforming of methane (DRM). As a result, the catalyst calcined at 0.5°Cmin−1 resulted in the formation of strong interaction between the active phase and the SBA-15 support, high nickel dispersion and accessibility that greatly enhanced its stability in dry reforming of methane. |
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| AbstractList | [Display omitted]
•Calcination rate affects pore plugging and dispersion of nickel.•Optimum calcination rate enhances nickel stability in dry reforming of methane.•Coke is absent on confined particles of nickel inside the mesopores of SBA-15.
The properties of nickel nanoparticles inside the mesopores of SBA-15 support were tuned by a careful control of the calcination rate. Ni/SBA-15 catalysts containing 5wt% nickel were prepared following three different calcination rate values (0.25 −0.5 −4.5°Cmin−1). Their properties were characterized by N2-sorption, X-ray diffraction (low and wide angles), temperature programed reduction and transmission electron microscopy. These catalysts were then tested in dry reforming of methane (DRM). As a result, the catalyst calcined at 0.5°Cmin−1 resulted in the formation of strong interaction between the active phase and the SBA-15 support, high nickel dispersion and accessibility that greatly enhanced its stability in dry reforming of methane. |
| Author | Karam, Leila El Hassan, Nissrine Casale, Sandra El Zakhem, Henri |
| Author_xml | – sequence: 1 givenname: Leila surname: Karam fullname: Karam, Leila organization: Department of Chemical Engineering, Faculty of Engineering, University of Balamand, P.O. Box 33, Amioun, El Koura, Lebanon – sequence: 2 givenname: Sandra surname: Casale fullname: Casale, Sandra organization: Sorbonne Universités, UPMC Université Paris 06, Laboratoire de Réactivité de Surface, 4 Place Jussieu, 75005 Paris, France – sequence: 3 givenname: Henri surname: El Zakhem fullname: El Zakhem, Henri organization: Department of Chemical Engineering, Faculty of Engineering, University of Balamand, P.O. Box 33, Amioun, El Koura, Lebanon – sequence: 4 givenname: Nissrine surname: El Hassan fullname: El Hassan, Nissrine email: nissrine.hassan@balamand.edu.lb organization: Department of Chemical Engineering, Faculty of Engineering, University of Balamand, P.O. Box 33, Amioun, El Koura, Lebanon |
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| Keywords | Particle size Metal-support interaction Accessibility Dry reforming of methane Nickel nanoparticles |
| Language | English |
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