High adsorption of methylene blue by activated carbon prepared from phosphoric acid treated eucalyptus residue

Activated carbon with large specific surface area (1545 m2·g−1) and total acid density (2.47 mmol·g−1) was prepared by thermal activation of phosphoric acid treated eucalyptus residue, and was successfully used for simulated dye wastewater treatment where it showed high methylene blue (MB) adsorptio...

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Vydáno v:	Powder technology Ročník 366; s. 239 - 248
Hlavní autoři:	Han, Qiaoning, Wang, Jing, Goodman, Bernard A., Xie, Junkang, Liu, Zuguang
Médium:	Journal Article
Jazyk:	angličtina
Vydáno:	Lausanne Elsevier B.V 15.04.2020 Elsevier BV
Témata:	Acids Activated carbon Activation Adsorption Carbon Computer simulation Dyes Eucalyptus Eucalyptus residue Functional groups Industrial wastewater Mass ratios Methylene blue moieties Particle diffusion Phosphoric acid powders Residues sorption isotherms surface area temperature texture wastewater Wastewater treatment Phosphoric acid Eucalyptus residue Adsorption Activated carbon Methylene blue
ISSN:	0032-5910, 1873-328X
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Abstract	Activated carbon with large specific surface area (1545 m2·g−1) and total acid density (2.47 mmol·g−1) was prepared by thermal activation of phosphoric acid treated eucalyptus residue, and was successfully used for simulated dye wastewater treatment where it showed high methylene blue (MB) adsorption capacity (977 mg·g−1). The textural properties and acidic functional groups of the activated carbon could be adjusted and controlled by phosphoric acid/eucalyptus residue mass ratios and activation temperature. Moreover, acidic functional groups could enhance MB adsorption by converting the adsorption pattern from planar to side adsorption with a decrease in activation temperature. The adsorption process was well described by the pseudo-second order kinetics and the Langmuir isotherm model, and it was demonstrated that intra-particle diffusion involved multi-linear stages. These findings provide important insights for the efficient treatment of dye wastewater on an industrial scale using waste eucalyptus residue. [Display omitted] •H3PO4 activated carbon was developed from waste eucalyptus residues.•The activated carbon has large specific surface area, high total acid density and yield.•The activated carbon has excellent adsorption performance to methylene blue.•The specific surface area and acidic functional groups play important role in adsorption capacity.•The adsorption pattern of methylene blue changed with the increase of acidic functional groups.
AbstractList	Activated carbon with large specific surface area (1545 m2·g−1) and total acid density (2.47 mmol·g−1) was prepared by thermal activation of phosphoric acid treated eucalyptus residue, and was successfully used for simulated dye wastewater treatment where it showed high methylene blue (MB) adsorption capacity (977 mg·g−1). The textural properties and acidic functional groups of the activated carbon could be adjusted and controlled by phosphoric acid/eucalyptus residue mass ratios and activation temperature. Moreover, acidic functional groups could enhance MB adsorption by converting the adsorption pattern from planar to side adsorption with a decrease in activation temperature. The adsorption process was well described by the pseudo-second order kinetics and the Langmuir isotherm model, and it was demonstrated that intra-particle diffusion involved multi-linear stages. These findings provide important insights for the efficient treatment of dye wastewater on an industrial scale using waste eucalyptus residue. [Display omitted] •H3PO4 activated carbon was developed from waste eucalyptus residues.•The activated carbon has large specific surface area, high total acid density and yield.•The activated carbon has excellent adsorption performance to methylene blue.•The specific surface area and acidic functional groups play important role in adsorption capacity.•The adsorption pattern of methylene blue changed with the increase of acidic functional groups. Activated carbon with large specific surface area (1545 m²·g⁻¹) and total acid density (2.47 mmol·g⁻¹) was prepared by thermal activation of phosphoric acid treated eucalyptus residue, and was successfully used for simulated dye wastewater treatment where it showed high methylene blue (MB) adsorption capacity (977 mg·g⁻¹). The textural properties and acidic functional groups of the activated carbon could be adjusted and controlled by phosphoric acid/eucalyptus residue mass ratios and activation temperature. Moreover, acidic functional groups could enhance MB adsorption by converting the adsorption pattern from planar to side adsorption with a decrease in activation temperature. The adsorption process was well described by the pseudo-second order kinetics and the Langmuir isotherm model, and it was demonstrated that intra-particle diffusion involved multi-linear stages. These findings provide important insights for the efficient treatment of dye wastewater on an industrial scale using waste eucalyptus residue. Activated carbon with large specific surface area (1545 m2·g−1) and total acid density (2.47 mmol·g−1) was prepared by thermal activation of phosphoric acid treated eucalyptus residue, and was successfully used for simulated dye wastewater treatment where it showed high methylene blue (MB) adsorption capacity (977 mg·g−1). The textural properties and acidic functional groups of the activated carbon could be adjusted and controlled by phosphoric acid/eucalyptus residue mass ratios and activation temperature. Moreover, acidic functional groups could enhance MB adsorption by converting the adsorption pattern from planar to side adsorption with a decrease in activation temperature. The adsorption process was well described by the pseudo-second order kinetics and the Langmuir isotherm model, and it was demonstrated that intra-particle diffusion involved multi-linear stages. These findings provide important insights for the efficient treatment of dye wastewater on an industrial scale using waste eucalyptus residue.
Author	Goodman, Bernard A. Liu, Zuguang Han, Qiaoning Wang, Jing Xie, Junkang
Author_xml	– sequence: 1 givenname: Qiaoning surname: Han fullname: Han, Qiaoning organization: School of Chemistry and Chemical Engineering, Guangxi University for Nationalities, Guangxi Key Laboratory of Chemistry and Engineering of Forest Products, Nanning, Guangxi 530008, China – sequence: 2 givenname: Jing surname: Wang fullname: Wang, Jing organization: School of Chemistry and Chemical Engineering, Guangxi University for Nationalities, Guangxi Key Laboratory of Chemistry and Engineering of Forest Products, Nanning, Guangxi 530008, China – sequence: 3 givenname: Bernard A. surname: Goodman fullname: Goodman, Bernard A. organization: College of Physical Sciences and Engineering, Guangxi University, Nanning, Guangxi 530004, China – sequence: 4 givenname: Junkang surname: Xie fullname: Xie, Junkang organization: School of Chemistry and Chemical Engineering, Guangxi University for Nationalities, Guangxi Key Laboratory of Chemistry and Engineering of Forest Products, Nanning, Guangxi 530008, China – sequence: 5 givenname: Zuguang orcidid: 0000-0003-4652-8540 surname: Liu fullname: Liu, Zuguang email: gxmd311lab@163.com organization: School of Chemistry and Chemical Engineering, Guangxi University for Nationalities, Guangxi Key Laboratory of Chemistry and Engineering of Forest Products, Nanning, Guangxi 530008, China
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Snippet	Activated carbon with large specific surface area (1545 m2·g−1) and total acid density (2.47 mmol·g−1) was prepared by thermal activation of phosphoric acid... Activated carbon with large specific surface area (1545 m2·g−1) and total acid density (2.47 mmol·g−1) was prepared by thermal activation of phosphoric acid... Activated carbon with large specific surface area (1545 m²·g⁻¹) and total acid density (2.47 mmol·g⁻¹) was prepared by thermal activation of phosphoric acid...
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SubjectTerms	Acids Activated carbon Activation Adsorption Carbon Computer simulation Dyes Eucalyptus Eucalyptus residue Functional groups Industrial wastewater Mass ratios Methylene blue moieties Particle diffusion Phosphoric acid powders Residues sorption isotherms surface area temperature texture wastewater Wastewater treatment
Title	High adsorption of methylene blue by activated carbon prepared from phosphoric acid treated eucalyptus residue
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