Theophylline-regulated pyrolysis synthesis of nitrogen-doped carbon nanotubes with iron-cobalt nanoparticles for greatly boosting oxygen reduction reaction
[Display omitted] At present, construction of economical, efficient and stable electrocatalysts for oxygen reduction reaction (ORR) is critical to alleviate the energy shortage. Theophylline (THP) can be easily extracted from natural plants, whose nitrogen atoms can chelate with metal ions. With ass...
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| Veröffentlicht in: | Journal of colloid and interface science Jg. 626; S. 653 - 661 |
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| Format: | Journal Article |
| Sprache: | Englisch |
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Elsevier Inc
15.11.2022
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| ISSN: | 0021-9797, 1095-7103, 1095-7103 |
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| Abstract | [Display omitted]
At present, construction of economical, efficient and stable electrocatalysts for oxygen reduction reaction (ORR) is critical to alleviate the energy shortage. Theophylline (THP) can be easily extracted from natural plants, whose nitrogen atoms can chelate with metal ions. With assistance of THP, FeCo alloy was confined in N-doped carbon nanotubes (FeCo/NCNTs-800) by one-step pyrolysis of a mixture of the metal precursors, g-C3N4 and THP. The resulting FeCo/NCNTs-800 showed a better ORR performance (onset potential, Eonset = 1.09 V; half-wave potential, E1/2 = 0.87 V) than commercial Pt/C (50 wt%) in a 0.1 M KOH solution, with a limiting current density as high as –5.54 mA cm−2. This work offers a feasible strategy for developing transitional bimetal-based carbon catalysts in alkaline fuel cells. |
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| AbstractList | At present, construction of economical, efficient and stable electrocatalysts for oxygen reduction reaction (ORR) is critical to alleviate the energy shortage. Theophylline (THP) can be easily extracted from natural plants, whose nitrogen atoms can chelate with metal ions. With assistance of THP, FeCo alloy was confined in N-doped carbon nanotubes (FeCo/NCNTs-800) by one-step pyrolysis of a mixture of the metal precursors, g-C₃N₄ and THP. The resulting FeCo/NCNTs-800 showed a better ORR performance (onset potential, Eₒₙₛₑₜ = 1.09 V; half-wave potential, E₁/₂ = 0.87 V) than commercial Pt/C (50 wt%) in a 0.1 M KOH solution, with a limiting current density as high as –5.54 mA cm⁻². This work offers a feasible strategy for developing transitional bimetal-based carbon catalysts in alkaline fuel cells. [Display omitted] At present, construction of economical, efficient and stable electrocatalysts for oxygen reduction reaction (ORR) is critical to alleviate the energy shortage. Theophylline (THP) can be easily extracted from natural plants, whose nitrogen atoms can chelate with metal ions. With assistance of THP, FeCo alloy was confined in N-doped carbon nanotubes (FeCo/NCNTs-800) by one-step pyrolysis of a mixture of the metal precursors, g-C3N4 and THP. The resulting FeCo/NCNTs-800 showed a better ORR performance (onset potential, Eonset = 1.09 V; half-wave potential, E1/2 = 0.87 V) than commercial Pt/C (50 wt%) in a 0.1 M KOH solution, with a limiting current density as high as –5.54 mA cm−2. This work offers a feasible strategy for developing transitional bimetal-based carbon catalysts in alkaline fuel cells. At present, construction of economical, efficient and stable electrocatalysts for oxygen reduction reaction (ORR) is critical to alleviate the energy shortage. Theophylline (THP) can be easily extracted from natural plants, whose nitrogen atoms can chelate with metal ions. With assistance of THP, FeCo alloy was confined in N-doped carbon nanotubes (FeCo/NCNTs-800) by one-step pyrolysis of a mixture of the metal precursors, g-C3N4 and THP. The resulting FeCo/NCNTs-800 showed a better ORR performance (onset potential, Eonset = 1.09 V; half-wave potential, E1/2 = 0.87 V) than commercial Pt/C (50 wt%) in a 0.1 M KOH solution, with a limiting current density as high as -5.54 mA cm-2. This work offers a feasible strategy for developing transitional bimetal-based carbon catalysts in alkaline fuel cells.At present, construction of economical, efficient and stable electrocatalysts for oxygen reduction reaction (ORR) is critical to alleviate the energy shortage. Theophylline (THP) can be easily extracted from natural plants, whose nitrogen atoms can chelate with metal ions. With assistance of THP, FeCo alloy was confined in N-doped carbon nanotubes (FeCo/NCNTs-800) by one-step pyrolysis of a mixture of the metal precursors, g-C3N4 and THP. The resulting FeCo/NCNTs-800 showed a better ORR performance (onset potential, Eonset = 1.09 V; half-wave potential, E1/2 = 0.87 V) than commercial Pt/C (50 wt%) in a 0.1 M KOH solution, with a limiting current density as high as -5.54 mA cm-2. This work offers a feasible strategy for developing transitional bimetal-based carbon catalysts in alkaline fuel cells. |
| Author | Chen, Yu-Ping Feng, Jiu-Ju Zhang, Lu Li, Xin-Sheng Wang, Ai-Jun Zhang, Wei |
| Author_xml | – sequence: 1 givenname: Wei surname: Zhang fullname: Zhang, Wei – sequence: 2 givenname: Yu-Ping surname: Chen fullname: Chen, Yu-Ping – sequence: 3 givenname: Lu surname: Zhang fullname: Zhang, Lu – sequence: 4 givenname: Jiu-Ju surname: Feng fullname: Feng, Jiu-Ju email: jjfeng@zjnu.cn – sequence: 5 givenname: Xin-Sheng surname: Li fullname: Li, Xin-Sheng – sequence: 6 givenname: Ai-Jun surname: Wang fullname: Wang, Ai-Jun email: ajwang@zjnu.cn |
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| Keywords | Pyrolysis Electrocatalyst Iron-cobalt alloyed nanoparticles Nitrogen-doped carbon nanotubes Oxygen reduction reaction Theophylline |
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At present, construction of economical, efficient and stable electrocatalysts for oxygen reduction reaction (ORR) is critical to alleviate... At present, construction of economical, efficient and stable electrocatalysts for oxygen reduction reaction (ORR) is critical to alleviate the energy shortage.... |
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| SubjectTerms | alloys carbon carbon nanotubes Electrocatalyst electrochemistry energy Iron-cobalt alloyed nanoparticles nitrogen Nitrogen-doped carbon nanotubes Oxygen reduction reaction Pyrolysis Theophylline |
| Title | Theophylline-regulated pyrolysis synthesis of nitrogen-doped carbon nanotubes with iron-cobalt nanoparticles for greatly boosting oxygen reduction reaction |
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