The Effect of Molecular Weight on the (Re)-Processability and Material Properties of Bio-Based, Thermoreversibly Cross-Linked Polyesters

A (partially) bio-based short-chain polyester is prepared through interfacial polycondensation of furan-functionalized diphenolic acid with terephthalic chloride. The furan groups along the backbone of the obtained polyester are able to form a covalent network (PE-fur/Bism) with various ratios of 1,...

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Vydané v:	Applied sciences Ročník 12; číslo 14; s. 7287
Hlavní autori:	Beljaars, Martijn, Kamphuis, Arjen J., Heeres, Hero J., Broekhuis, Antonius A., Picchioni, Francesco
Médium:	Journal Article
Jazyk:	English
Vydavateľské údaje:	Basel MDPI AG 01.07.2022
Predmet:	Acids bio-based bismaleimide Bisphenol A Bond strength Chemistry Chloride furan Mechanical properties Molecular weight Phenols polyester Polymer melts polymers Resins short-chain United States > US
ISSN:	2076-3417, 2076-3417
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Abstract	A (partially) bio-based short-chain polyester is prepared through interfacial polycondensation of furan-functionalized diphenolic acid with terephthalic chloride. The furan groups along the backbone of the obtained polyester are able to form a covalent network (PE-fur/Bism) with various ratios of 1,1′-(methylenedi-4,1-phenylene)bismaleimide via the thermoreversible Diels–Alder (DA) reaction. Several techniques have been employed to characterize the polyester network, including 1H-NMR, gel permeation chromatography (GPC), thermogravimetric analysis (TGA), differential scanning calorimetry (DSC), and dynamic mechanical thermal analysis (DMTA). The polyester base polymer displays a glass transition temperature of 115 °C, whereas the temperatures at which the retro-Diels–Alder (rDA) reaction takes place lie above 130 °C for the various polyester/bismaleimide networks. Excellent thermoreversibility and recyclability of the polyester resin have been shown through DSC and DMTA measurements.
AbstractList	A (partially) bio-based short-chain polyester is prepared through interfacial polycondensation of furan-functionalized diphenolic acid with terephthalic chloride. The furan groups along the backbone of the obtained polyester are able to form a covalent network (PE-fur/Bism) with various ratios of 1,1′-(methylenedi-4,1-phenylene)bismaleimide via the thermoreversible Diels–Alder (DA) reaction. Several techniques have been employed to characterize the polyester network, including 1H-NMR, gel permeation chromatography (GPC), thermogravimetric analysis (TGA), differential scanning calorimetry (DSC), and dynamic mechanical thermal analysis (DMTA). The polyester base polymer displays a glass transition temperature of 115 °C, whereas the temperatures at which the retro-Diels–Alder (rDA) reaction takes place lie above 130 °C for the various polyester/bismaleimide networks. Excellent thermoreversibility and recyclability of the polyester resin have been shown through DSC and DMTA measurements.
Author	Picchioni, Francesco Kamphuis, Arjen J. Broekhuis, Antonius A. Beljaars, Martijn Heeres, Hero J.
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SubjectTerms	Acids bio-based bismaleimide Bisphenol A Bond strength Chemistry Chloride furan Mechanical properties Molecular weight Phenols polyester Polymer melts polymers Resins short-chain
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Title	The Effect of Molecular Weight on the (Re)-Processability and Material Properties of Bio-Based, Thermoreversibly Cross-Linked Polyesters
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