Effect of cation insertion on the stability of gliding arc plasma-precipitated mesoporous MnO2 dye bleaching catalysts

α-MnO 2 and γ-MnO 2 polymorphs were, respectively, obtained from the plasma precipitation of KMnO 4 and Mn(CH 3 COO) 3 ⋅2H 2 O precursors. The obtained powders were calcined at 150 °C, 210 °C and 400 °C, and characterized by X-ray diffraction, Raman spectroscopy, Fourier transform infrared spectrosc...

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Published in:	Journal of materials research Vol. 38; no. 17; pp. 4144 - 4156
Main Authors:	Boyom-Tatchemo, Franck W., Devred, François, Acayanka, Elie, Kamgang-Youbi, Georges, Nzali, Serge, Laminsi, Samuel, Gaigneaux, Eric M.
Format:	Journal Article
Language:	English
Published:	Cham Springer International Publishing 14.09.2023 Springer Nature B.V
Subjects:	Applied and Technical Physics Biomaterials Bleaching Catalysis Cations Chemistry and Materials Science Crystal structure Crystallinity Decomposition Dyes Fourier transforms Infrared analysis Inorganic Chemistry Insertion Manganese dioxide Materials Engineering Materials Science Metal oxides Nanomaterials Nanotechnology Oxidation Photoelectrons Plasma Potassium permanganate Raman spectroscopy Roasting Temperature Thermal stability Thermogravimetric analysis Vibration X ray photoelectron spectroscopy Calcination Plasma-precipitated MnO Catalytic stability Cation insertion
ISSN:	0884-2914, 2044-5326
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Abstract	α-MnO 2 and γ-MnO 2 polymorphs were, respectively, obtained from the plasma precipitation of KMnO 4 and Mn(CH 3 COO) 3 ⋅2H 2 O precursors. The obtained powders were calcined at 150 °C, 210 °C and 400 °C, and characterized by X-ray diffraction, Raman spectroscopy, Fourier transform infrared spectroscopy (FTIR), Thermogravimetric analysis (TGA), X-ray photoelectron spectroscopy (XPS), nitrogen physisorption and Scanning electron microscopy (SEM). As a result, the calcination does not significantly affect textural properties and crystalline structure of the α-MnO 2 , while γ-MnO 2 is transformed into β-MnO 2 for temperatures above 400 °C. The thermal stability α-MnO 2 is due to the K + ions insertion in its 4.6 Å × 4.6 Å tunnels and corroborated the catalytic performance of 100, 98, 98 and 97% compared to 71, 54, 52 and 48% for γ-MnO 2 after four successive reuse cycles on Tartrazine Yellow dye. The insertion of cationic species (K + , Na + , Mg 2+ ) into the structure of MnO 2 reinforces its crystalline structure and promotes the formation of powerful oxidizing species through oxygen vacant sites. Graphical Abstract
AbstractList	α-MnO 2 and γ-MnO 2 polymorphs were, respectively, obtained from the plasma precipitation of KMnO 4 and Mn(CH 3 COO) 3 ⋅2H 2 O precursors. The obtained powders were calcined at 150 °C, 210 °C and 400 °C, and characterized by X-ray diffraction, Raman spectroscopy, Fourier transform infrared spectroscopy (FTIR), Thermogravimetric analysis (TGA), X-ray photoelectron spectroscopy (XPS), nitrogen physisorption and Scanning electron microscopy (SEM). As a result, the calcination does not significantly affect textural properties and crystalline structure of the α-MnO 2 , while γ-MnO 2 is transformed into β-MnO 2 for temperatures above 400 °C. The thermal stability α-MnO 2 is due to the K + ions insertion in its 4.6 Å × 4.6 Å tunnels and corroborated the catalytic performance of 100, 98, 98 and 97% compared to 71, 54, 52 and 48% for γ-MnO 2 after four successive reuse cycles on Tartrazine Yellow dye. The insertion of cationic species (K + , Na + , Mg 2+ ) into the structure of MnO 2 reinforces its crystalline structure and promotes the formation of powerful oxidizing species through oxygen vacant sites. Graphical Abstract α-MnO2 and γ-MnO2 polymorphs were, respectively, obtained from the plasma precipitation of KMnO4 and Mn(CH3COO)3⋅2H2O precursors. The obtained powders were calcined at 150 °C, 210 °C and 400 °C, and characterized by X-ray diffraction, Raman spectroscopy, Fourier transform infrared spectroscopy (FTIR), Thermogravimetric analysis (TGA), X-ray photoelectron spectroscopy (XPS), nitrogen physisorption and Scanning electron microscopy (SEM). As a result, the calcination does not significantly affect textural properties and crystalline structure of the α-MnO2, while γ-MnO2 is transformed into β-MnO2 for temperatures above 400 °C. The thermal stability α-MnO2 is due to the K+ ions insertion in its 4.6 Å × 4.6 Å tunnels and corroborated the catalytic performance of 100, 98, 98 and 97% compared to 71, 54, 52 and 48% for γ-MnO2 after four successive reuse cycles on Tartrazine Yellow dye. The insertion of cationic species (K+, Na+, Mg2+) into the structure of MnO2 reinforces its crystalline structure and promotes the formation of powerful oxidizing species through oxygen vacant sites.
Author	Boyom-Tatchemo, Franck W. Nzali, Serge Gaigneaux, Eric M. Acayanka, Elie Laminsi, Samuel Kamgang-Youbi, Georges Devred, François
Author_xml	– sequence: 1 givenname: Franck W. orcidid: 0009-0003-6814-1192 surname: Boyom-Tatchemo fullname: Boyom-Tatchemo, Franck W. email: boyom.william@yahoo.com organization: Institute of Condensed Matter and Nanosciences (IMCN), Université Catholique de Louvain, Department of Inorganic Chemistry, University of Yaoundé I – sequence: 2 givenname: François surname: Devred fullname: Devred, François organization: Institute of Condensed Matter and Nanosciences (IMCN), Université Catholique de Louvain – sequence: 3 givenname: Elie surname: Acayanka fullname: Acayanka, Elie organization: Department of Inorganic Chemistry, University of Yaoundé I – sequence: 4 givenname: Georges surname: Kamgang-Youbi fullname: Kamgang-Youbi, Georges organization: Department of Inorganic Chemistry, University of Yaoundé I – sequence: 5 givenname: Serge surname: Nzali fullname: Nzali, Serge organization: School of Wood, Water and Natural Resources, Faculty of Agronomy and Agricultural Sciences, University of Dschang – sequence: 6 givenname: Samuel surname: Laminsi fullname: Laminsi, Samuel organization: Department of Inorganic Chemistry, University of Yaoundé I – sequence: 7 givenname: Eric M. surname: Gaigneaux fullname: Gaigneaux, Eric M. email: eric.gaigneaux@uclouvain.be organization: Institute of Condensed Matter and Nanosciences (IMCN), Université Catholique de Louvain
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Snippet	α-MnO 2 and γ-MnO 2 polymorphs were, respectively, obtained from the plasma precipitation of KMnO 4 and Mn(CH 3 COO) 3 ⋅2H 2 O precursors. The obtained powders... α-MnO2 and γ-MnO2 polymorphs were, respectively, obtained from the plasma precipitation of KMnO4 and Mn(CH3COO)3⋅2H2O precursors. The obtained powders were...
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SubjectTerms	Applied and Technical Physics Biomaterials Bleaching Catalysis Cations Chemistry and Materials Science Crystal structure Crystallinity Decomposition Dyes Fourier transforms Infrared analysis Inorganic Chemistry Insertion Manganese dioxide Materials Engineering Materials Science Metal oxides Nanomaterials Nanotechnology Oxidation Photoelectrons Plasma Potassium permanganate Raman spectroscopy Roasting Temperature Thermal stability Thermogravimetric analysis Vibration X ray photoelectron spectroscopy
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Title	Effect of cation insertion on the stability of gliding arc plasma-precipitated mesoporous MnO2 dye bleaching catalysts
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