High-temperature radiation resistance of NiCoFe medium-entropy alloy enabled by stable nanostructures and defect evolution mechanisms

The study innovatively examined a nano oxide dispersion-strengthened (ODS) NiCoFe medium-entropy alloy with nanosized grains to address the challenge of discovering structural materials for high-temperature irradiation applications, such as in advanced nuclear reactors. The ODS-NiCoFe alloy exhibite...

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Veröffentlicht in:Journal of materials research and technology Jg. 37; S. 5448 - 5464
Hauptverfasser: Nori, Sri Tapaswi, Esfandiarpour, Amin, Kalita, Damian, Zieliński, Maciej, Mulewska, Katarzyna, Bjørge, Ruben, Vullum, Per Erik, Ferreirós, Pedro A., Chrominski, Witold, Li, Mingyang, Chang, Yongqin, Zhang, Yanwen, Diduszko, Ryszard, Macha, Nagini, Malladi, Sai Rama Krishna, Mason, Daniel R., Holmestad, Randi, Alava, Mikko, Kurpaska, Lukasz
Format: Journal Article
Sprache:Englisch
Veröffentlicht: Elsevier B.V 01.07.2025
Elsevier
Schlagworte:
High-temperature irradiation
Irradiation-hardening resistance
Irradiation-swelling resistance
Molecular dynamics damage cascade simulations
Oxide dispersion-strengthened NiCoFe medium-entropy alloy
Physical stability of nanostructures
Oxide dispersion-strengthened NiCoFe medium-entropy alloy
Physical stability of nanostructures
Irradiation-swelling resistance
Irradiation-hardening resistance
Molecular dynamics damage cascade simulations
High-temperature irradiation
ISSN:2238-7854
Online-Zugang:Volltext
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Abstract The study innovatively examined a nano oxide dispersion-strengthened (ODS) NiCoFe medium-entropy alloy with nanosized grains to address the challenge of discovering structural materials for high-temperature irradiation applications, such as in advanced nuclear reactors. The ODS-NiCoFe alloy exhibited a nanoindentation hardness of 4.3 ± 0.9 GPa, representing a two-fold enhancement over the 2.0 ± 0.1 GPa of single-crystal NiCoFe. Dislocations were identified as the primary defect structures. Following irradiation (Ni2+, 580 °C), the average dislocation length density increased from ∼2.6 × 1013 m−2 to ∼6.1 × 1013 m−2, while the mean dislocation length decreased from 249 nm to 104 nm, contributing to a relative irradiation hardening of 25 %. Additionally, the study demonstrated the stability of various nanostructures, with only minor changes in the average sizes of nanoprecipitates and grains—from 6.7 ± 1.7 nm to 6.4 ± 1.7 nm, and from 73 ± 2 nm to 76 ± 2 nm, respectively, upon irradiation, suggesting effective defect annihilation at interfaces and grain boundaries. The alloy exhibited no observable irradiation-induced voids. Molecular dynamics simulations revealed irradiation resistance of the alloy through the absorption of vacancy clusters at grain boundaries and Shockley-dominant-dislocation chains and the absorption of interstitial clusters at grain boundaries, aided by the high mobility and three-dimensional motion of interstitial clusters. Thus, the findings demonstrate the high-temperature radiation resistance of the novel ODS-NiCoFe alloy, surpassing that of well-known ODS steels, using a correlative approach that combines experiments and simulations.
AbstractList The study innovatively examined a nano oxide dispersion-strengthened (ODS) NiCoFe medium-entropy alloy with nanosized grains to address the challenge of discovering structural materials for high-temperature irradiation applications, such as in advanced nuclear reactors. The ODS-NiCoFe alloy exhibited a nanoindentation hardness of 4.3 ± 0.9 GPa, representing a two-fold enhancement over the 2.0 ± 0.1 GPa of single-crystal NiCoFe. Dislocations were identified as the primary defect structures. Following irradiation (Ni2+, 580 °C), the average dislocation length density increased from ∼2.6 × 1013 m−2 to ∼6.1 × 1013 m−2, while the mean dislocation length decreased from 249 nm to 104 nm, contributing to a relative irradiation hardening of 25 %. Additionally, the study demonstrated the stability of various nanostructures, with only minor changes in the average sizes of nanoprecipitates and grains—from 6.7 ± 1.7 nm to 6.4 ± 1.7 nm, and from 73 ± 2 nm to 76 ± 2 nm, respectively, upon irradiation, suggesting effective defect annihilation at interfaces and grain boundaries. The alloy exhibited no observable irradiation-induced voids. Molecular dynamics simulations revealed irradiation resistance of the alloy through the absorption of vacancy clusters at grain boundaries and Shockley-dominant-dislocation chains and the absorption of interstitial clusters at grain boundaries, aided by the high mobility and three-dimensional motion of interstitial clusters. Thus, the findings demonstrate the high-temperature radiation resistance of the novel ODS-NiCoFe alloy, surpassing that of well-known ODS steels, using a correlative approach that combines experiments and simulations.
Author Vullum, Per Erik
Chrominski, Witold
Malladi, Sai Rama Krishna
Zhang, Yanwen
Macha, Nagini
Nori, Sri Tapaswi
Bjørge, Ruben
Mason, Daniel R.
Holmestad, Randi
Esfandiarpour, Amin
Mulewska, Katarzyna
Zieliński, Maciej
Kalita, Damian
Diduszko, Ryszard
Chang, Yongqin
Alava, Mikko
Li, Mingyang
Kurpaska, Lukasz
Ferreirós, Pedro A.
Author_xml – sequence: 1
  givenname: Sri Tapaswi
  orcidid: 0000-0002-7164-1118
  surname: Nori
  fullname: Nori, Sri Tapaswi
  email: Sri_tapaswi.Nori@ncbj.gov.pl, sritapaswi2007@gmail.com
  organization: NOMATEN Centre of Excellence, National Centre for Nuclear Research, Andrzeja Soltana 7, Otwock, 05-400, Poland
– sequence: 2
  givenname: Amin
  orcidid: 0000-0003-2507-0796
  surname: Esfandiarpour
  fullname: Esfandiarpour, Amin
  email: Amin.Esfandiarpour@ncbj.gov.pl
  organization: NOMATEN Centre of Excellence, National Centre for Nuclear Research, Andrzeja Soltana 7, Otwock, 05-400, Poland
– sequence: 3
  givenname: Damian
  orcidid: 0000-0003-1135-6873
  surname: Kalita
  fullname: Kalita, Damian
  organization: NOMATEN Centre of Excellence, National Centre for Nuclear Research, Andrzeja Soltana 7, Otwock, 05-400, Poland
– sequence: 4
  givenname: Maciej
  orcidid: 0000-0003-0760-1004
  surname: Zieliński
  fullname: Zieliński, Maciej
  organization: NOMATEN Centre of Excellence, National Centre for Nuclear Research, Andrzeja Soltana 7, Otwock, 05-400, Poland
– sequence: 5
  givenname: Katarzyna
  orcidid: 0000-0001-6863-9431
  surname: Mulewska
  fullname: Mulewska, Katarzyna
  organization: NOMATEN Centre of Excellence, National Centre for Nuclear Research, Andrzeja Soltana 7, Otwock, 05-400, Poland
– sequence: 6
  givenname: Ruben
  orcidid: 0000-0002-6310-7820
  surname: Bjørge
  fullname: Bjørge, Ruben
  organization: Norwegian University of Science and Technology, Trondheim, NO-7491, Norway
– sequence: 7
  givenname: Per Erik
  orcidid: 0000-0001-7968-4879
  surname: Vullum
  fullname: Vullum, Per Erik
  organization: Norwegian University of Science and Technology, Trondheim, NO-7491, Norway
– sequence: 8
  givenname: Pedro A.
  orcidid: 0000-0003-1782-9520
  surname: Ferreirós
  fullname: Ferreirós, Pedro A.
  organization: Centre for Nuclear Safety, VTT Technical Research Centre of Finland Limited, Espoo, FI-02044, Finland
– sequence: 9
  givenname: Witold
  orcidid: 0000-0002-5345-7667
  surname: Chrominski
  fullname: Chrominski, Witold
  organization: NOMATEN Centre of Excellence, National Centre for Nuclear Research, Andrzeja Soltana 7, Otwock, 05-400, Poland
– sequence: 10
  givenname: Mingyang
  surname: Li
  fullname: Li, Mingyang
  organization: School of Materials Science and Engineering, University of Science and Technology Beijing, Beijing, 100083, China
– sequence: 11
  givenname: Yongqin
  surname: Chang
  fullname: Chang, Yongqin
  organization: School of Materials Science and Engineering, University of Science and Technology Beijing, Beijing, 100083, China
– sequence: 12
  givenname: Yanwen
  surname: Zhang
  fullname: Zhang, Yanwen
  organization: Department of Mechanical and Materials Engineering, Queen's University, Kingston, Ontario, K7L 3N6, Canada
– sequence: 13
  givenname: Ryszard
  orcidid: 0000-0003-0590-6824
  surname: Diduszko
  fullname: Diduszko, Ryszard
  organization: NOMATEN Centre of Excellence, National Centre for Nuclear Research, Andrzeja Soltana 7, Otwock, 05-400, Poland
– sequence: 14
  givenname: Nagini
  surname: Macha
  fullname: Macha, Nagini
  organization: Department of Materials Science & Metallurgical Engineering, Indian Institute of Technology Hyderabad, Kandi, Telangana, 502285, India
– sequence: 15
  givenname: Sai Rama Krishna
  surname: Malladi
  fullname: Malladi, Sai Rama Krishna
  organization: Department of Materials Science & Metallurgical Engineering, Indian Institute of Technology Hyderabad, Kandi, Telangana, 502285, India
– sequence: 16
  givenname: Daniel R.
  surname: Mason
  fullname: Mason, Daniel R.
  organization: United Kingdom Atomic Energy Authority, Culham Science Centre, Abingdon, Oxfordshire, OX14 3DB, United Kingdom
– sequence: 17
  givenname: Randi
  surname: Holmestad
  fullname: Holmestad, Randi
  organization: Norwegian University of Science and Technology, Trondheim, NO-7491, Norway
– sequence: 18
  givenname: Mikko
  surname: Alava
  fullname: Alava, Mikko
  organization: NOMATEN Centre of Excellence, National Centre for Nuclear Research, Andrzeja Soltana 7, Otwock, 05-400, Poland
– sequence: 19
  givenname: Lukasz
  orcidid: 0000-0002-2970-4090
  surname: Kurpaska
  fullname: Kurpaska, Lukasz
  organization: NOMATEN Centre of Excellence, National Centre for Nuclear Research, Andrzeja Soltana 7, Otwock, 05-400, Poland
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Keywords Oxide dispersion-strengthened NiCoFe medium-entropy alloy
Physical stability of nanostructures
Irradiation-swelling resistance
Irradiation-hardening resistance
Molecular dynamics damage cascade simulations
High-temperature irradiation
Language English
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Snippet The study innovatively examined a nano oxide dispersion-strengthened (ODS) NiCoFe medium-entropy alloy with nanosized grains to address the challenge of...
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SubjectTerms High-temperature irradiation
Irradiation-hardening resistance
Irradiation-swelling resistance
Molecular dynamics damage cascade simulations
Oxide dispersion-strengthened NiCoFe medium-entropy alloy
Physical stability of nanostructures
Title High-temperature radiation resistance of NiCoFe medium-entropy alloy enabled by stable nanostructures and defect evolution mechanisms
URI https://dx.doi.org/10.1016/j.jmrt.2025.07.079
https://doaj.org/article/cdf2c6b02eff4f63b9512305cd0a3c38
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