Effect of mechanical recycling and virgin PBR addition on the properties of ABS recovered from WEEE: A multi-technique characterization
•Extrusion raises T10% by ∼30 °C and improves ABS particle size homogeneity.•Virgin PBR improves matrix cohesion and induces fibrous recyclate morphology.•Multi-technique approach enables complete characterization of recycled ABS.•Findings support tuning recyclate quality by extrusion and additive s...
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| Veröffentlicht in: | Waste Management Bulletin Jg. 3; H. 3; S. 100238 |
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| Format: | Journal Article |
| Sprache: | Englisch |
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Elsevier B.V
01.09.2025
Elsevier |
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| ISSN: | 2949-7507, 2949-7507 |
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| Abstract | •Extrusion raises T10% by ∼30 °C and improves ABS particle size homogeneity.•Virgin PBR improves matrix cohesion and induces fibrous recyclate morphology.•Multi-technique approach enables complete characterization of recycled ABS.•Findings support tuning recyclate quality by extrusion and additive strategy.
With the growing use of electrical and electronic devices, the volume of waste electrical and electronic equipment (WEEE) continues to increase, posing a major environmental and recycling challenge. Acrylonitrile-butadiene-styrene (ABS) is one of the most common thermoplastics found in WEEE, its recovery is complicated by contamination, heterogeneity, and degradation. While mechanical recycling of ABS is widely practiced, the impact of specific processing steps on the chemical and physical properties of the recyclate remains insufficiently explored. This study investigates the effect of shredding and extrusion, as well as the integration of virgin polybutadiene rubber (PBR), on the morphology, chemical structure, and thermal stability of ABS-rich WEEE recyclates. A multi-analytical approach, combining Fourier transform infrared spectroscopy (FT-IR), transmission electron microscopy (TEM), scanning electron microscopy (SEM), energy dispersive X-ray analysis (EDX), inductively coupled plasma optical emission spectroscopy (ICP-OES) and thermal analysis − was employed to fully characterize the materials. Our findings show that extrusion improves sample homogeneity and removes some contaminants (e.g., Ba, Cl), leading to a significant increase in thermal stability (T10% +30 °C). The addition of virgin PBR contributes to enhanced internal cohesion and a fibrous morphology. This work provides a robust methodology for distinguishing processing-related changes from compositional variability in real-world recycled plastics. The approach can support the development of advanced processing strategies for polymer waste streams. |
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| AbstractList | With the growing use of electrical and electronic devices, the volume of waste electrical and electronic equipment (WEEE) continues to increase, posing a major environmental and recycling challenge. Acrylonitrile-butadiene-styrene (ABS) is one of the most common thermoplastics found in WEEE, its recovery is complicated by contamination, heterogeneity, and degradation. While mechanical recycling of ABS is widely practiced, the impact of specific processing steps on the chemical and physical properties of the recyclate remains insufficiently explored. This study investigates the effect of shredding and extrusion, as well as the integration of virgin polybutadiene rubber (PBR), on the morphology, chemical structure, and thermal stability of ABS-rich WEEE recyclates. A multi-analytical approach, combining Fourier transform infrared spectroscopy (FT-IR), transmission electron microscopy (TEM), scanning electron microscopy (SEM), energy dispersive X-ray analysis (EDX), inductively coupled plasma optical emission spectroscopy (ICP-OES) and thermal analysis − was employed to fully characterize the materials. Our findings show that extrusion improves sample homogeneity and removes some contaminants (e.g., Ba, Cl), leading to a significant increase in thermal stability (T10% +30 °C). The addition of virgin PBR contributes to enhanced internal cohesion and a fibrous morphology. This work provides a robust methodology for distinguishing processing-related changes from compositional variability in real-world recycled plastics. The approach can support the development of advanced processing strategies for polymer waste streams. •Extrusion raises T10% by ∼30 °C and improves ABS particle size homogeneity.•Virgin PBR improves matrix cohesion and induces fibrous recyclate morphology.•Multi-technique approach enables complete characterization of recycled ABS.•Findings support tuning recyclate quality by extrusion and additive strategy. With the growing use of electrical and electronic devices, the volume of waste electrical and electronic equipment (WEEE) continues to increase, posing a major environmental and recycling challenge. Acrylonitrile-butadiene-styrene (ABS) is one of the most common thermoplastics found in WEEE, its recovery is complicated by contamination, heterogeneity, and degradation. While mechanical recycling of ABS is widely practiced, the impact of specific processing steps on the chemical and physical properties of the recyclate remains insufficiently explored. This study investigates the effect of shredding and extrusion, as well as the integration of virgin polybutadiene rubber (PBR), on the morphology, chemical structure, and thermal stability of ABS-rich WEEE recyclates. A multi-analytical approach, combining Fourier transform infrared spectroscopy (FT-IR), transmission electron microscopy (TEM), scanning electron microscopy (SEM), energy dispersive X-ray analysis (EDX), inductively coupled plasma optical emission spectroscopy (ICP-OES) and thermal analysis − was employed to fully characterize the materials. Our findings show that extrusion improves sample homogeneity and removes some contaminants (e.g., Ba, Cl), leading to a significant increase in thermal stability (T10% +30 °C). The addition of virgin PBR contributes to enhanced internal cohesion and a fibrous morphology. This work provides a robust methodology for distinguishing processing-related changes from compositional variability in real-world recycled plastics. The approach can support the development of advanced processing strategies for polymer waste streams. |
| ArticleNumber | 100238 |
| Author | Vincent, Luc Pagnotta, Sophie Sbirrazzuoli, Nicolas Schollaert, Joost Lesiak, Anna Safou, Lamiae Orange, Francois Guigo, Nathanael |
| Author_xml | – sequence: 1 givenname: Anna surname: Lesiak fullname: Lesiak, Anna organization: Université Côte d’Azur, Institut de Chimie de Nice (ICN) UMR CNRS 7272, Parc Valrose, Nice 06108, France – sequence: 2 givenname: Luc surname: Vincent fullname: Vincent, Luc organization: Université Côte d’Azur, Institut de Chimie de Nice (ICN) UMR CNRS 7272, Parc Valrose, Nice 06108, France – sequence: 3 givenname: Joost surname: Schollaert fullname: Schollaert, Joost organization: Galloo Plastics, Av. Port Fluvial, 59250 Halluin, France – sequence: 4 givenname: Lamiae surname: Safou fullname: Safou, Lamiae organization: Galloo Plastics, Av. Port Fluvial, 59250 Halluin, France – sequence: 5 givenname: Francois surname: Orange fullname: Orange, Francois organization: Université Côte d’Azur, Centre Commun de Microscopie Appliquée, 06108 Nice, France – sequence: 6 givenname: Sophie surname: Pagnotta fullname: Pagnotta, Sophie organization: Université Côte d’Azur, Centre Commun de Microscopie Appliquée, 06108 Nice, France – sequence: 7 givenname: Nicolas surname: Sbirrazzuoli fullname: Sbirrazzuoli, Nicolas organization: Université Côte d’Azur, Institut de Chimie de Nice (ICN) UMR CNRS 7272, Parc Valrose, Nice 06108, France – sequence: 8 givenname: Nathanael orcidid: 0000-0002-0858-4093 surname: Guigo fullname: Guigo, Nathanael email: nathanael.guigo@univ-cotedazur.fr organization: Université Côte d’Azur, Institut de Chimie de Nice (ICN) UMR CNRS 7272, Parc Valrose, Nice 06108, France |
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| Keywords | Extrusion ABS Polybutadiene Recycling Contaminants |
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| Snippet | •Extrusion raises T10% by ∼30 °C and improves ABS particle size homogeneity.•Virgin PBR improves matrix cohesion and induces fibrous recyclate... With the growing use of electrical and electronic devices, the volume of waste electrical and electronic equipment (WEEE) continues to increase, posing a major... |
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| SubjectTerms | ABS Contaminants Extrusion Polybutadiene Recycling |
| Title | Effect of mechanical recycling and virgin PBR addition on the properties of ABS recovered from WEEE: A multi-technique characterization |
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