Molecular Engineering of Metal Complexes for Electrocatalytic Carbon Dioxide Reduction: From Adjustment of Intrinsic Activity to Molecular Immobilization

The electrocatalytic CO2 reduction reaction (ECO2RR) is one promising method for storing intermittent clean energy in chemical bonds and producing fuels. Among various kinds of catalysts for ECO2RR, molecular metal complexes with well‐defined structures are convenient for studies of their rational d...

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Veröffentlicht in:	Angewandte Chemie International Edition Jg. 61; H. 44; S. e202205301 - n/a
Hauptverfasser:	Yang, Zhi‐Wen, Chen, Jin‐Mei, Qiu, Li‐Qi, Xie, Wen‐Jun, He, Liang‐Nian
Format:	Journal Article
Sprache:	Englisch
Veröffentlicht:	Weinheim Wiley Subscription Services, Inc 02.11.2022
Ausgabe:	International ed. in English
Schlagworte:	Carbon Dioxide Catalysts Chemical bonds Chemical reduction Clean energy Coordination compounds Electrocatalytic Reduction Immobilization Ligand Modification Metal Complex Catalysts Metal complexes Molecular Immobilization Organic chemistry
ISSN:	1433-7851, 1521-3773, 1521-3773
Online-Zugang:	Volltext
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Abstract	The electrocatalytic CO2 reduction reaction (ECO2RR) is one promising method for storing intermittent clean energy in chemical bonds and producing fuels. Among various kinds of catalysts for ECO2RR, molecular metal complexes with well‐defined structures are convenient for studies of their rational design, structure–reactivity relationships, and mechanisms. In this Review, we summarize the molecular engineering of several N‐based metal complexes including Re/Mn bipyridine compounds and metal macrocycles, concluding with general modification strategies to devise novel molecular catalysts with high intrinsic activity. Through physical adsorption, covalent linking, and formation of a periodic backbone, these active molecules can be heterogenized into immobilized catalysts with more practical prospects. Finally, significant challenges and opportunities based on molecular catalysts are discussed. This Review focuses on molecular catalysts for the electrocatalytic CO2 reduction reaction (ECO2RR) including metal bipyridines and macrocycle complexes, and summarizes the molecular engineering strategies developed to regulate the intrinsic catalytic efficiency and modify the electrode. Guidelines are provided for the rational design of ECO2RR catalytic systems.
AbstractList	The electrocatalytic CO 2 reduction reaction (ECO 2 RR) is one promising method for storing intermittent clean energy in chemical bonds and producing fuels. Among various kinds of catalysts for ECO 2 RR, molecular metal complexes with well‐defined structures are convenient for studies of their rational design, structure–reactivity relationships, and mechanisms. In this Review, we summarize the molecular engineering of several N‐based metal complexes including Re/Mn bipyridine compounds and metal macrocycles, concluding with general modification strategies to devise novel molecular catalysts with high intrinsic activity. Through physical adsorption, covalent linking, and formation of a periodic backbone, these active molecules can be heterogenized into immobilized catalysts with more practical prospects. Finally, significant challenges and opportunities based on molecular catalysts are discussed. The electrocatalytic CO2 reduction reaction (ECO2RR) is one promising method for storing intermittent clean energy in chemical bonds and producing fuels. Among various kinds of catalysts for ECO2RR, molecular metal complexes with well‐defined structures are convenient for studies of their rational design, structure–reactivity relationships, and mechanisms. In this Review, we summarize the molecular engineering of several N‐based metal complexes including Re/Mn bipyridine compounds and metal macrocycles, concluding with general modification strategies to devise novel molecular catalysts with high intrinsic activity. Through physical adsorption, covalent linking, and formation of a periodic backbone, these active molecules can be heterogenized into immobilized catalysts with more practical prospects. Finally, significant challenges and opportunities based on molecular catalysts are discussed. This Review focuses on molecular catalysts for the electrocatalytic CO2 reduction reaction (ECO2RR) including metal bipyridines and macrocycle complexes, and summarizes the molecular engineering strategies developed to regulate the intrinsic catalytic efficiency and modify the electrode. Guidelines are provided for the rational design of ECO2RR catalytic systems. The electrocatalytic CO2 reduction reaction (ECO2RR) is one promising method for storing intermittent clean energy in chemical bonds and producing fuels. Among various kinds of catalysts for ECO2RR, molecular metal complexes with well‐defined structures are convenient for studies of their rational design, structure–reactivity relationships, and mechanisms. In this Review, we summarize the molecular engineering of several N‐based metal complexes including Re/Mn bipyridine compounds and metal macrocycles, concluding with general modification strategies to devise novel molecular catalysts with high intrinsic activity. Through physical adsorption, covalent linking, and formation of a periodic backbone, these active molecules can be heterogenized into immobilized catalysts with more practical prospects. Finally, significant challenges and opportunities based on molecular catalysts are discussed.Dedicated to the 60th anniversary of Institute of Elemento-Organic Chemistry, Nankai University. The electrocatalytic CO2 reduction reaction (ECO2 RR) is one promising method for storing intermittent clean energy in chemical bonds and producing fuels. Among various kinds of catalysts for ECO2 RR, molecular metal complexes with well-defined structures are convenient for studies of their rational design, structure-reactivity relationships, and mechanisms. In this Review, we summarize the molecular engineering of several N-based metal complexes including Re/Mn bipyridine compounds and metal macrocycles, concluding with general modification strategies to devise novel molecular catalysts with high intrinsic activity. Through physical adsorption, covalent linking, and formation of a periodic backbone, these active molecules can be heterogenized into immobilized catalysts with more practical prospects. Finally, significant challenges and opportunities based on molecular catalysts are discussed.The electrocatalytic CO2 reduction reaction (ECO2 RR) is one promising method for storing intermittent clean energy in chemical bonds and producing fuels. Among various kinds of catalysts for ECO2 RR, molecular metal complexes with well-defined structures are convenient for studies of their rational design, structure-reactivity relationships, and mechanisms. In this Review, we summarize the molecular engineering of several N-based metal complexes including Re/Mn bipyridine compounds and metal macrocycles, concluding with general modification strategies to devise novel molecular catalysts with high intrinsic activity. Through physical adsorption, covalent linking, and formation of a periodic backbone, these active molecules can be heterogenized into immobilized catalysts with more practical prospects. Finally, significant challenges and opportunities based on molecular catalysts are discussed.
Author	Xie, Wen‐Jun Chen, Jin‐Mei He, Liang‐Nian Yang, Zhi‐Wen Qiu, Li‐Qi
Author_xml	– sequence: 1 givenname: Zhi‐Wen surname: Yang fullname: Yang, Zhi‐Wen organization: Nankai University – sequence: 2 givenname: Jin‐Mei surname: Chen fullname: Chen, Jin‐Mei organization: Nankai University – sequence: 3 givenname: Li‐Qi surname: Qiu fullname: Qiu, Li‐Qi organization: Nankai University – sequence: 4 givenname: Wen‐Jun surname: Xie fullname: Xie, Wen‐Jun organization: Nankai University – sequence: 5 givenname: Liang‐Nian orcidid: 0000-0002-6067-5937 surname: He fullname: He, Liang‐Nian email: heln@nankai.edu.cn organization: Nankai University
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Snippet	The electrocatalytic CO2 reduction reaction (ECO2RR) is one promising method for storing intermittent clean energy in chemical bonds and producing fuels. Among... The electrocatalytic CO 2 reduction reaction (ECO 2 RR) is one promising method for storing intermittent clean energy in chemical bonds and producing fuels.... The electrocatalytic CO2 reduction reaction (ECO2 RR) is one promising method for storing intermittent clean energy in chemical bonds and producing fuels....
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SubjectTerms	Carbon Dioxide Catalysts Chemical bonds Chemical reduction Clean energy Coordination compounds Electrocatalytic Reduction Immobilization Ligand Modification Metal Complex Catalysts Metal complexes Molecular Immobilization Organic chemistry
Title	Molecular Engineering of Metal Complexes for Electrocatalytic Carbon Dioxide Reduction: From Adjustment of Intrinsic Activity to Molecular Immobilization
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