Synthesis of large crystals of all-silica zeolite ferrierite

In this paper, the non-aqueous organothermal synthesis of large crystals of zeolite ferrierite is described. The influence of unbranched monoalkyl C 3–C 5 amines, different gel compositions and crystallization conditions is studied. These parameters have a significant impact on crystal form. The lar...

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Vydáno v:	Microporous and mesoporous materials Ročník 104; číslo 1; s. 179 - 184
Hlavní autoři:	Rakoczy, Rainer A., Traa, Yvonne, Kortunov, Pavel, Vasenkov, Sergey, Kärger, Jörg, Weitkamp, Jens
Médium:	Journal Article
Jazyk:	angličtina
Vydáno:	Amsterdam Elsevier Inc 23.08.2007 Elsevier
Témata:	Chemistry Colloidal state and disperse state Exact sciences and technology General and physical chemistry Interference microscopy Ion-exchange Large crystals Mono-alkyl amines Non-aqueous synthesis Porous materials Pyridine Surface physical chemistry Zeolite ferrierite Zeolites: preparations and properties Non-aqueous synthesis Mono-alkyl amines Interference microscopy Zeolite ferrierite Pyridine Large crystals Nitrogen heterocycle Crystals Alkylamine Zeolite Silica Molecular sieve Amine Synthesis Alkyl Six membered ring
ISSN:	1387-1811, 1873-3093
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Abstract	In this paper, the non-aqueous organothermal synthesis of large crystals of zeolite ferrierite is described. The influence of unbranched monoalkyl C 3–C 5 amines, different gel compositions and crystallization conditions is studied. These parameters have a significant impact on crystal form. The large crystals obtained show adsorption properties similar to conventionally synthesized zeolite ferrierite and allowed the observation of the evolution of intracrystalline concentration profiles by interference microscopy.
AbstractList	In this paper, the non-aqueous organothermal synthesis of large crystals of zeolite ferrierite is described. The influence of unbranched monoalkyl C 3–C 5 amines, different gel compositions and crystallization conditions is studied. These parameters have a significant impact on crystal form. The large crystals obtained show adsorption properties similar to conventionally synthesized zeolite ferrierite and allowed the observation of the evolution of intracrystalline concentration profiles by interference microscopy.
Author	Rakoczy, Rainer A. Kärger, Jörg Weitkamp, Jens Traa, Yvonne Kortunov, Pavel Vasenkov, Sergey
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Keywords	Non-aqueous synthesis Mono-alkyl amines Interference microscopy Zeolite ferrierite Pyridine Large crystals Nitrogen heterocycle Crystals Alkylamine Zeolite Silica Molecular sieve Amine Synthesis Alkyl Six membered ring
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SubjectTerms	Chemistry Colloidal state and disperse state Exact sciences and technology General and physical chemistry Interference microscopy Ion-exchange Large crystals Mono-alkyl amines Non-aqueous synthesis Porous materials Pyridine Surface physical chemistry Zeolite ferrierite Zeolites: preparations and properties
Title	Synthesis of large crystals of all-silica zeolite ferrierite
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