Kinetic Characteristics of Nitriding of Zr–1% Nb Alloy

We study the kinetic characteristics of nitriding of thin-sheet (~ 1 mm) samples of Zr–1% Nb alloy treated in a nitrogen atmosphere ( ) in broad temperature ( T = 550; 650; 750; 850 and 950°С) and time ( τ = 1; 5 and 10 h) ranges. It is shown that the process of nitriding of the analyzed alloy obeys...

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Vydané v:	Materials science (New York, N.Y.) Ročník 58; číslo 3; s. 408 - 416
Hlavní autori:	Trush, V. S., Pohrelyuk, I. M., Kravchyshyn, T. M., Luk’yanenko, A. G., Stoev, P. I., Fedirko, V. M., Kovalchuk, I. V.
Médium:	Journal Article
Jazyk:	English
Vydavateľské údaje:	New York Springer US 01.11.2022 Springer Springer Nature B.V
Predmet:	Alloys Characterization and Evaluation of Materials Chemistry and Materials Science Materials Science Microhardness Niobium base alloys Nitriding Nitrogen Reflexes Solid Mechanics Specialty metals industry Structural Materials Zirconium base alloys Zr–1% Nb alloy microstructure surface layer parameters of the crystal lattice kinetics of mass changes microhardness nitriding
ISSN:	1068-820X, 1573-885X
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Abstract	We study the kinetic characteristics of nitriding of thin-sheet (~ 1 mm) samples of Zr–1% Nb alloy treated in a nitrogen atmosphere ( ) in broad temperature ( T = 550; 650; 750; 850 and 950°С) and time ( τ = 1; 5 and 10 h) ranges. It is shown that the process of nitriding of the analyzed alloy obeys a law close to a parabolic dependence ( n ≈ 2). It is discovered that the activation energy of nitriding of the alloy within the temperature range 550–950°C is equal to 131.8 kJ/mole. The microstructure of the subsurface layer of the alloy after nitriding is analyzed. The distribution of the surface microhardness of Zr–1% Nb alloy is determined. The diagrams of intensity of the phase reflexes of α -Zr and ZrN on the surface of alloy after treatment in a nitrogen atmosphere are constructed.
AbstractList	We study the kinetic characteristics of nitriding of thin-sheet (~ 1 mm) samples of Zr–1% Nb alloy treated in a nitrogen atmosphere () in broad temperature (T = 550; 650; 750; 850 and 950°С) and time (τ = 1; 5 and 10 h) ranges. It is shown that the process of nitriding of the analyzed alloy obeys a law close to a parabolic dependence (n ≈ 2). It is discovered that the activation energy of nitriding of the alloy within the temperature range 550–950°C is equal to 131.8 kJ/mole. The microstructure of the subsurface layer of the alloy after nitriding is analyzed. The distribution of the surface microhardness of Zr–1% Nb alloy is determined. The diagrams of intensity of the phase reflexes of α-Zr and ZrN on the surface of alloy after treatment in a nitrogen atmosphere are constructed. We study the kinetic characteristics of nitriding of thin-sheet (~ 1 mm) samples of Zr-1% Nb alloy treated in a nitrogen atmosphere ( [Formula omitted]) in broad temperature (T = 550; 650; 750; 850 and 950°Ð¡) and time ([tau] = 1; 5 and 10 h) ranges. It is shown that the process of nitriding of the analyzed alloy obeys a law close to a parabolic dependence (n [almost equal to] 2). It is discovered that the activation energy of nitriding of the alloy within the temperature range 550-950°C is equal to 131.8 kJ/mole. The microstructure of the subsurface layer of the alloy after nitriding is analyzed. The distribution of the surface microhardness of Zr-1% Nb alloy is determined. The diagrams of intensity of the phase reflexes of [alpha]-Zr and ZrN on the surface of alloy after treatment in a nitrogen atmosphere are constructed. We study the kinetic characteristics of nitriding of thin-sheet (~ 1 mm) samples of Zr–1% Nb alloy treated in a nitrogen atmosphere ( ) in broad temperature ( T = 550; 650; 750; 850 and 950°С) and time ( τ = 1; 5 and 10 h) ranges. It is shown that the process of nitriding of the analyzed alloy obeys a law close to a parabolic dependence ( n ≈ 2). It is discovered that the activation energy of nitriding of the alloy within the temperature range 550–950°C is equal to 131.8 kJ/mole. The microstructure of the subsurface layer of the alloy after nitriding is analyzed. The distribution of the surface microhardness of Zr–1% Nb alloy is determined. The diagrams of intensity of the phase reflexes of α -Zr and ZrN on the surface of alloy after treatment in a nitrogen atmosphere are constructed.
Audience	Academic
Author	Luk’yanenko, A. G. Stoev, P. I. Kovalchuk, I. V. Pohrelyuk, I. M. Trush, V. S. Fedirko, V. M. Kravchyshyn, T. M.
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References_xml	– reference: I. M. Pohrelyuk, J. Padgurskas, S. M. Lavrys, A. G. Luk’yanenko, V. S. Trush, and R. Kreivaitis, “Topography, hardness, elastic modulus and wear resistance of nitride on titanium,” in: Proc. of the 9th Internat. Conf. BALTTRIB’2017, (November, 16–17, 2017), A. Stulginskis Univ., Kaunas (2017), pp. 41–46; DOI:10.15544/balttrib.2017.09. – reference: О. М. Ivasishin, V. N. Voevodin, А. I. Dekhtyar, P. E. Markovsky, M. M. Pylypenko, S. D. Lavrinenko, and R. G. Gontareva, “Features of the mechanical behavior of fuel elements tubes of Zr–1%Nb under conditions simulating breakdown of cooling,” Probl. Atomic Sci. Technol., No. 5 (99), 53–60 (2015). – reference: S. Banerjee and M. K. Banerjee, “Nuclear applications: zirconium alloys,” Reference Module Mater. Sci. Mater. Eng., 1–15 (2016); DOI:https://doi.org/10.1016/В978-0-12-803581-8.02576-5. – reference: Z. Z. Tang, “Effect of nitrogen concentration to the structural, chemical and electrical properties of tantalum zirconium nitride films,” Ceramics Int., No. 38 (4), 2997–3000 (2012); DOI:https://doi.org/10.1016/j.ceramint.2011.11.07. – reference: AzarenkovNАBulavinLАZalyubovskiiIIKirichenkoVGNeklyudovIМShilyaevBАNuclear Power Engineering: A Textbook2012KharkovKarazin Kharkov National University[in Russian] – reference: V. M. Voyevodin, V. M. Fedirko, V. S. Trush, O. H. Luk’yanenko, P. I. Stoev, V. A. Panov, M. А. Tykhonovsky, “Influence of thermochemical treatment on the oxidation of fuel cladding tubes made of Zr–1%Nb alloy,” Mater. Sci.,56, No. 4, 509–515 (2021); DOI:https://doi.org/10.1007/s11003-021-00457-x. – reference: TrushVSLukianenkoОHStoevPІInfluence of modification of the surface layer by penetrating impurities on the long-term strength of Zr–1% Nb alloyMater. Sci.20205545855891:CAS:528:DC%2BB3cXpt1yktrc%3D10.1007/s11003-020-00342-z – reference: V. M. Fedirko, O. H. Luk’yanenko, V. S. Trush, P. I. Stoev, and M. A. Tykhonovs’kyi, “Effect of thermochemical treatment in regulated gas media on the thermal resistance of Zr–1%Nb alloy,” Mater. Sci.,52, No. 2, 209–215 (2016); DOI: https://doi.org/10.1007/s11003-016-9945-x. – reference: ChossonRGourgues-LorenzonAFVandenbergheVBrachetJCCrépinJCreep flow and fracture behavior of the oxygen-enriched alpha phase in zirconium alloysScripta Mater.201611720231:CAS:528:DC%2BC28XksFCrtbs%3D10.1016/j.scriptamat.2016.02.021 – reference: L. Gribaudo, D. Arias, and J. Abriata, “The N–Zr (Nitrogen–Zirconium) system,” J. Phase Equilibria,15, No. 4, 441–449 (1994). – reference: DubeyPAryaVSrivastavaSSinghDChandraREffect of nitrogen flow rate on structural and mechanical properties of zirconium tungsten nitride (Zr–W–N) coatings deposited by magnetron sputteringSurf. Coat. Technol.20132361821871:CAS:528:DC%2BC3sXhs1Wiu7zF10.1016/j.surfcoat.2013.09.04 – reference: J. Zhang, A. R. Oganov, X. Li, H. Dong, and Q. 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Snippet	We study the kinetic characteristics of nitriding of thin-sheet (~ 1 mm) samples of Zr–1% Nb alloy treated in a nitrogen atmosphere ( ) in broad temperature (... We study the kinetic characteristics of nitriding of thin-sheet (~ 1 mm) samples of Zr-1% Nb alloy treated in a nitrogen atmosphere ( [Formula omitted]) in... We study the kinetic characteristics of nitriding of thin-sheet (~ 1 mm) samples of Zr–1% Nb alloy treated in a nitrogen atmosphere () in broad temperature (T...
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SubjectTerms	Alloys Characterization and Evaluation of Materials Chemistry and Materials Science Materials Science Microhardness Niobium base alloys Nitriding Nitrogen Reflexes Solid Mechanics Specialty metals industry Structural Materials Zirconium base alloys
Title	Kinetic Characteristics of Nitriding of Zr–1% Nb Alloy
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