Light-triggered oxidative activity of chromate at neutral pH: A colorimetric system for accurate and on-site detection of Cr(VI) in natural water
Hexavalent chromium (Cr(VI)), a confirmed human respiratory carcinogen, has attracted widespread attention due to its high toxicity and mobility in natural water systems. However, the developed catalytic colorimetric probes for Cr(VI) detection remain challenging, such as various species of Cr(VI) c...
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| Published in: | Journal of hazardous materials Vol. 440; p. 129812 |
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| Main Authors: | , , , , , , , |
| Format: | Journal Article |
| Language: | English |
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Elsevier B.V
15.10.2022
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| ISSN: | 0304-3894, 1873-3336 |
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| Abstract | Hexavalent chromium (Cr(VI)), a confirmed human respiratory carcinogen, has attracted widespread attention due to its high toxicity and mobility in natural water systems. However, the developed catalytic colorimetric probes for Cr(VI) detection remain challenging, such as various species of Cr(VI) coexisting in water or acid buffer, the obvious interference from oxidizing ions at acidic pH, the synthesis of complex materials, and the consumption of hydrogen peroxide. In this work, a phenomenon of UV light-triggered chromate to produce singlet oxygen under neutral pH was found. An environmentally-friendly method based on the rapid oxidation of chromogenic substrates was thus developed for the highly specific and accurate detection of Cr(VI). Cr(VI) serves as both the active center and the target of this system, which ensures the rapidity, simplicity, and environmental protection of the proposed colorimetric strategy. Importantly, the neutral catalytic condition ensures that the predominant species CrO42- can be accurately quantified and avoids the interference of oxidizing ions. Subsequently, a portable analytical system integrating an array of LED lamps, a miniature color reading device, and a developed smartphone-based program was successfully developed to accomplish high-throughput and on-site analysis of Cr(VI) in natural water. The proposed method provides a rapid screening and water quality assessment tool for the faster, more cost-effective, and accurate detection of Cr(VI) in the water system.
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•The light-triggered oxidative activity of Cr(VI) at neutral pH was first proposed.•Cr(VI) is a green ionic photosensitizer that can generate singlet oxygen.•Accurate, selective, and environmentally-friendly analysis of Cr(VI) was obtained.•The portable colorimetric method is rapid, sensitive, and high throughput.•The developed colorimetric system can predict Cr(VI) pollution in natural water. |
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| AbstractList | Hexavalent chromium (Cr(VI)), a confirmed human respiratory carcinogen, has attracted widespread attention due to its high toxicity and mobility in natural water systems. However, the developed catalytic colorimetric probes for Cr(VI) detection remain challenging, such as various species of Cr(VI) coexisting in water or acid buffer, the obvious interference from oxidizing ions at acidic pH, the synthesis of complex materials, and the consumption of hydrogen peroxide. In this work, a phenomenon of UV light-triggered chromate to produce singlet oxygen under neutral pH was found. An environmentally-friendly method based on the rapid oxidation of chromogenic substrates was thus developed for the highly specific and accurate detection of Cr(VI). Cr(VI) serves as both the active center and the target of this system, which ensures the rapidity, simplicity, and environmental protection of the proposed colorimetric strategy. Importantly, the neutral catalytic condition ensures that the predominant species CrO₄²⁻ can be accurately quantified and avoids the interference of oxidizing ions. Subsequently, a portable analytical system integrating an array of LED lamps, a miniature color reading device, and a developed smartphone-based program was successfully developed to accomplish high-throughput and on-site analysis of Cr(VI) in natural water. The proposed method provides a rapid screening and water quality assessment tool for the faster, more cost-effective, and accurate detection of Cr(VI) in the water system. Hexavalent chromium (Cr(VI)), a confirmed human respiratory carcinogen, has attracted widespread attention due to its high toxicity and mobility in natural water systems. However, the developed catalytic colorimetric probes for Cr(VI) detection remain challenging, such as various species of Cr(VI) coexisting in water or acid buffer, the obvious interference from oxidizing ions at acidic pH, the synthesis of complex materials, and the consumption of hydrogen peroxide. In this work, a phenomenon of UV light-triggered chromate to produce singlet oxygen under neutral pH was found. An environmentally-friendly method based on the rapid oxidation of chromogenic substrates was thus developed for the highly specific and accurate detection of Cr(VI). Cr(VI) serves as both the active center and the target of this system, which ensures the rapidity, simplicity, and environmental protection of the proposed colorimetric strategy. Importantly, the neutral catalytic condition ensures that the predominant species CrO42- can be accurately quantified and avoids the interference of oxidizing ions. Subsequently, a portable analytical system integrating an array of LED lamps, a miniature color reading device, and a developed smartphone-based program was successfully developed to accomplish high-throughput and on-site analysis of Cr(VI) in natural water. The proposed method provides a rapid screening and water quality assessment tool for the faster, more cost-effective, and accurate detection of Cr(VI) in the water system. [Display omitted] •The light-triggered oxidative activity of Cr(VI) at neutral pH was first proposed.•Cr(VI) is a green ionic photosensitizer that can generate singlet oxygen.•Accurate, selective, and environmentally-friendly analysis of Cr(VI) was obtained.•The portable colorimetric method is rapid, sensitive, and high throughput.•The developed colorimetric system can predict Cr(VI) pollution in natural water. |
| ArticleNumber | 129812 |
| Author | Chen, Xueshan Huang, Ke Zheng, Chengbin Liao, Jing Wu, Yuke Lin, Yao Zhang, Jinyi Yu, Huimin |
| Author_xml | – sequence: 1 givenname: Jing surname: Liao fullname: Liao, Jing organization: College of Chemistry and Material Science, Sichuan Normal University, Chengdu, Sichuan 610068, China – sequence: 2 givenname: Yuke surname: Wu fullname: Wu, Yuke organization: Key Laboratory of Green Chemistry & Technology of MOE, College of Chemistry, Sichuan University, Chengdu, Sichuan 610065, China – sequence: 3 givenname: Xueshan surname: Chen fullname: Chen, Xueshan organization: Key Laboratory of Green Chemistry & Technology of MOE, College of Chemistry, Sichuan University, Chengdu, Sichuan 610065, China – sequence: 4 givenname: Huimin surname: Yu fullname: Yu, Huimin organization: College of Chemistry and Material Science, Sichuan Normal University, Chengdu, Sichuan 610068, China – sequence: 5 givenname: Yao surname: Lin fullname: Lin, Yao organization: West China School of Basic Medical Sciences & Forensic Medicine, Sichuan University, Chengdu 610041, China – sequence: 6 givenname: Ke surname: Huang fullname: Huang, Ke email: huangke@sicnu.edu.cn organization: College of Chemistry and Material Science, Sichuan Normal University, Chengdu, Sichuan 610068, China – sequence: 7 givenname: Jinyi surname: Zhang fullname: Zhang, Jinyi email: jinyizhang@scu.edu.cn organization: Key Laboratory of Green Chemistry & Technology of MOE, College of Chemistry, Sichuan University, Chengdu, Sichuan 610065, China – sequence: 8 givenname: Chengbin surname: Zheng fullname: Zheng, Chengbin email: abinscu@scu.edu.cn organization: Key Laboratory of Green Chemistry & Technology of MOE, College of Chemistry, Sichuan University, Chengdu, Sichuan 610065, China |
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| Keywords | Neutral pH Colorimetric sensor Cr(VI) detection Photocatalytic oxidation On-site analysis |
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| Title | Light-triggered oxidative activity of chromate at neutral pH: A colorimetric system for accurate and on-site detection of Cr(VI) in natural water |
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