Al rich PVD protective coatings: A promising approach to prevent T91 steel corrosion in stagnant liquid lead

In order to investigate a protective coating approach for nuclear applications, two different aluminum rich layers were deposited on T91 steel coupons: Ti-Al-N films were grown via High Power Impulse Magnetron Sputtering and AlO coatings were produced by Radio Frequency Magnetron Sputtering. In this...

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Published in:	Surface & coatings technology Vol. 377; p. 124890
Main Authors:	Miorin, Enrico, Montagner, Francesco, Zin, Valentina, Giuranno, Donatella, Ricci, Enrica, Pedroni, Matteo, Spampinato, Valentina, Vassallo, Espedito, Deambrosis, Silvia Maria
Format:	Journal Article
Language:	English
Published:	Lausanne Elsevier B.V 15.11.2019 Elsevier BV
Subjects:	Aluminum Aluminum oxide Corrosion tests Heat resistant steels Heavy liquid metals corrosion protection High power impulse magnetron sputtering (HiPIMS) Liquid lead Magnetron sputtering Martensitic stainless steels Oxide coatings Protective coatings Radio frequency magnetron sputtering (RFMS) Sputtered films Substrates Titanium Titanium aluminum nitride Titanium aluminum nitride Sputtered films High power impulse magnetron sputtering (HiPIMS) Radio frequency magnetron sputtering (RFMS) Heavy liquid metals corrosion protection Aluminum oxide
ISSN:	0257-8972, 1879-3347
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Abstract	In order to investigate a protective coating approach for nuclear applications, two different aluminum rich layers were deposited on T91 steel coupons: Ti-Al-N films were grown via High Power Impulse Magnetron Sputtering and AlO coatings were produced by Radio Frequency Magnetron Sputtering. In this exploratory work, coated specimens were corrosion tested in stagnant Pb at 550 °C for 1200 h and both types of coatings proved to be effective in protecting the substrate from the harsh environment. Due to the severe experimental conditions, the Al oxide film underwent some mechanical changes, while, the nitride coating demonstrated its noteworthy stability. [Display omitted] •Assessment of Al-rich coatings potentiality against liquid lead corrosion of steel•Aluminum Oxide and Titanium Aluminum Nitride coatings by magnetron sputtering•Coated and bare samples are exposed to severe liquid lead corrosive attack.•Aluminum-rich coatings are effective in protecting steel from corrosion.•Nitride coatings maintain their excellent mechanical properties unchanged.
AbstractList	In order to investigate a protective coating approach for nuclear applications, two different aluminum rich layers were deposited on T91 steel coupons: Ti-Al-N films were grown via High Power Impulse Magnetron Sputtering and AlO coatings were produced by Radio Frequency Magnetron Sputtering. In this exploratory work, coated specimens were corrosion tested in stagnant Pb at 550 °C for 1200 h and both types of coatings proved to be effective in protecting the substrate from the harsh environment. Due to the severe experimental conditions, the Al oxide film underwent some mechanical changes, while, the nitride coating demonstrated its noteworthy stability. [Display omitted] •Assessment of Al-rich coatings potentiality against liquid lead corrosion of steel•Aluminum Oxide and Titanium Aluminum Nitride coatings by magnetron sputtering•Coated and bare samples are exposed to severe liquid lead corrosive attack.•Aluminum-rich coatings are effective in protecting steel from corrosion.•Nitride coatings maintain their excellent mechanical properties unchanged. In order to investigate a protective coating approach for nuclear applications, two different aluminum rich layers were deposited on T91 steel coupons: Ti-Al-N films were grown via High Power Impulse Magnetron Sputtering and Al-O coatings were produced by Radio Frequency Magnetron Sputtering. In this exploratory work, coated specimens were corrosion tested in stagnant Pb at 550 °C for 1200 h and both types of coatings proved to be effective in protecting the substrate from the harsh environment. Due to the severe experimental conditions, the Al oxide film underwent some mechanical changes, while, the nitride coating demonstrated its noteworthy stability.
ArticleNumber	124890
Author	Miorin, Enrico Deambrosis, Silvia Maria Giuranno, Donatella Spampinato, Valentina Zin, Valentina Montagner, Francesco Pedroni, Matteo Vassallo, Espedito Ricci, Enrica
Author_xml	– sequence: 1 givenname: Enrico surname: Miorin fullname: Miorin, Enrico email: enrico.miorin@cnr.it organization: National Research Council - CNR, Institute of Condensed Matter Chemistry and Technologies for Energy – ICMATE, Corso Stati Uniti, 4 - 35127 Padova, Italy – sequence: 2 givenname: Francesco surname: Montagner fullname: Montagner, Francesco email: francesco.montagner@cnr.it organization: National Research Council - CNR, Institute of Condensed Matter Chemistry and Technologies for Energy – ICMATE, Corso Stati Uniti, 4 - 35127 Padova, Italy – sequence: 3 givenname: Valentina surname: Zin fullname: Zin, Valentina email: valentina.zin@cnr.it organization: National Research Council - CNR, Institute of Condensed Matter Chemistry and Technologies for Energy – ICMATE, Corso Stati Uniti, 4 - 35127 Padova, Italy – sequence: 4 givenname: Donatella surname: Giuranno fullname: Giuranno, Donatella email: donatella.giuranno@ge.icmate.cnr.it organization: National Research Council - CNR, Institute of Condensed Matter Chemistry and Technologies for Energy – ICMATE – via De Marini, 6 - 16149 Genova, Italy – sequence: 5 givenname: Enrica orcidid: 0000-0002-7054-5271 surname: Ricci fullname: Ricci, Enrica email: enrica.ricci@ge.icmate.cnr.it organization: National Research Council - CNR, Institute of Condensed Matter Chemistry and Technologies for Energy – ICMATE – via De Marini, 6 - 16149 Genova, Italy – sequence: 6 givenname: Matteo surname: Pedroni fullname: Pedroni, Matteo email: pedroni@ifp.cnr.it organization: National Research Council - CNR, Institute of Plasma Physics “Piero Caldirola” - via R. Cozzi, 53 - 20125 Milano, Italy – sequence: 7 givenname: Valentina surname: Spampinato fullname: Spampinato, Valentina email: spampinato@ifp.cnr.it organization: National Research Council - CNR, Institute of Plasma Physics “Piero Caldirola” - via R. Cozzi, 53 - 20125 Milano, Italy – sequence: 8 givenname: Espedito orcidid: 0000-0001-8435-4196 surname: Vassallo fullname: Vassallo, Espedito email: vassallo@ifp.cnr.it organization: National Research Council - CNR, Institute of Plasma Physics “Piero Caldirola” - via R. Cozzi, 53 - 20125 Milano, Italy – sequence: 9 givenname: Silvia Maria surname: Deambrosis fullname: Deambrosis, Silvia Maria email: silviamaria.deambrosis@cnr.it organization: National Research Council - CNR, Institute of Condensed Matter Chemistry and Technologies for Energy – ICMATE, Corso Stati Uniti, 4 - 35127 Padova, Italy
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Keywords	Titanium aluminum nitride Sputtered films High power impulse magnetron sputtering (HiPIMS) Radio frequency magnetron sputtering (RFMS) Heavy liquid metals corrosion protection Aluminum oxide
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Snippet	In order to investigate a protective coating approach for nuclear applications, two different aluminum rich layers were deposited on T91 steel coupons: Ti-Al-N...
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SubjectTerms	Aluminum Aluminum oxide Corrosion tests Heat resistant steels Heavy liquid metals corrosion protection High power impulse magnetron sputtering (HiPIMS) Liquid lead Magnetron sputtering Martensitic stainless steels Oxide coatings Protective coatings Radio frequency magnetron sputtering (RFMS) Sputtered films Substrates Titanium Titanium aluminum nitride
Title	Al rich PVD protective coatings: A promising approach to prevent T91 steel corrosion in stagnant liquid lead
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