A highly sensitive and selective fluorescent chemosensor for the sequential recognition of Zn2+ and S2− in living cells and aqueous media

A new highly selective chemosensor 1 (E)-5-((2-hydroxybenzylidene)amino)-1H-imidazole-4-carboxamide was designed and synthesized for the sequential recognition of Zn2+ and S2− in a near-perfect aqueous media. The sensor 1 exhibited a green color fluorescence in the presence of Zn2+. The detection li...

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Veröffentlicht in:Sensors and actuators. B, Chemical Jg. 255; S. 3108 - 3116
Hauptverfasser: Yun, Jin Yeong, Jo, Tae Geun, Han, Jiyeon, Jang, Hyo Jung, Lim, Mi Hee, Kim, Cheal
Format: Journal Article
Sprache:Englisch
Veröffentlicht: Elsevier B.V 01.02.2018
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ISSN:0925-4005, 1873-3077
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Abstract A new highly selective chemosensor 1 (E)-5-((2-hydroxybenzylidene)amino)-1H-imidazole-4-carboxamide was designed and synthesized for the sequential recognition of Zn2+ and S2− in a near-perfect aqueous media. The sensor 1 exhibited a green color fluorescence in the presence of Zn2+. The detection limit (1.18μM) of 1 for Zn2+ is much lower than World Health Organization guideline (76μM) in drinking water. 1 can detect and quantify Zn2+ in real water samples and the sensing mechanism of Zn2+ by 1 was explained by DFT calculations. Moreover, resulting 1-Zn2+ complex can detect hydrogen sulfide through turn-off fluorescent change, without any anion interference. The detection limit (2.60μM) of 1-Zn2+ complex for S2− was much lower than EPA guideline (7.8mM) by odor in drinking water. Furthermore, sensor 1 could detect sequentially Zn2+ and S2− in living cells.
AbstractList A new highly selective chemosensor 1 (E)-5-((2-hydroxybenzylidene)amino)-1H-imidazole-4-carboxamide was designed and synthesized for the sequential recognition of Zn2+ and S2− in a near-perfect aqueous media. The sensor 1 exhibited a green color fluorescence in the presence of Zn2+. The detection limit (1.18μM) of 1 for Zn2+ is much lower than World Health Organization guideline (76μM) in drinking water. 1 can detect and quantify Zn2+ in real water samples and the sensing mechanism of Zn2+ by 1 was explained by DFT calculations. Moreover, resulting 1-Zn2+ complex can detect hydrogen sulfide through turn-off fluorescent change, without any anion interference. The detection limit (2.60μM) of 1-Zn2+ complex for S2− was much lower than EPA guideline (7.8mM) by odor in drinking water. Furthermore, sensor 1 could detect sequentially Zn2+ and S2− in living cells.
Author Kim, Cheal
Jang, Hyo Jung
Han, Jiyeon
Yun, Jin Yeong
Jo, Tae Geun
Lim, Mi Hee
Author_xml – sequence: 1
  givenname: Jin Yeong
  surname: Yun
  fullname: Yun, Jin Yeong
  organization: Department of Fine Chemistry and Department of Interdisciplinary Bio IT Materials, Seoul National University of Science and Technology, Seoul 139-743, Republic of Korea
– sequence: 2
  givenname: Tae Geun
  surname: Jo
  fullname: Jo, Tae Geun
  organization: Department of Fine Chemistry and Department of Interdisciplinary Bio IT Materials, Seoul National University of Science and Technology, Seoul 139-743, Republic of Korea
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  givenname: Jiyeon
  surname: Han
  fullname: Han, Jiyeon
  organization: Department of Chemistry, Ulsan National Institute of Science and Technology (UNIST), Ulsan 44919, Republic of Korea
– sequence: 4
  givenname: Hyo Jung
  surname: Jang
  fullname: Jang, Hyo Jung
  organization: Department of Fine Chemistry and Department of Interdisciplinary Bio IT Materials, Seoul National University of Science and Technology, Seoul 139-743, Republic of Korea
– sequence: 5
  givenname: Mi Hee
  surname: Lim
  fullname: Lim, Mi Hee
  organization: Department of Chemistry, Ulsan National Institute of Science and Technology (UNIST), Ulsan 44919, Republic of Korea
– sequence: 6
  givenname: Cheal
  surname: Kim
  fullname: Kim, Cheal
  email: chealkim@seoultech.ac.kr
  organization: Department of Fine Chemistry and Department of Interdisciplinary Bio IT Materials, Seoul National University of Science and Technology, Seoul 139-743, Republic of Korea
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Keywords Sulfide
Fluorescence
Cell imaging
Theoretical calculations
Zinc
Sequential detection
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Snippet A new highly selective chemosensor 1 (E)-5-((2-hydroxybenzylidene)amino)-1H-imidazole-4-carboxamide was designed and synthesized for the sequential recognition...
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SubjectTerms Cell imaging
Fluorescence
Sequential detection
Sulfide
Theoretical calculations
Zinc
Title A highly sensitive and selective fluorescent chemosensor for the sequential recognition of Zn2+ and S2− in living cells and aqueous media
URI https://dx.doi.org/10.1016/j.snb.2017.09.136
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