Effect of Long-Term Immersion on the Corrosion and Passivation Behavior of Lean Duplex Stainless Steel 2101 in 3.5 wt% NaCl Solution

The current study investigates the effect of long-term immersion on the corrosion response and the consequent passive film formation process of lean duplex stainless steel 2101 in 3.5 wt% NaCl solution. The corrosion behavior of the alloy has been monitored through long term immersion tests at diffe...

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Published in:	Metals and materials international Vol. 29; no. 7; pp. 1923 - 1939
Main Authors:	Bairi, Lipika Rani, Bairagi, Darothi, Duley, Partha, Mandal, Sumantra
Format:	Journal Article
Language:	English
Published:	Seoul The Korean Institute of Metals and Materials 01.07.2023 대한금속·재료학회
Subjects:	Characterization and Evaluation of Materials Chemistry and Materials Science Engineering Thermodynamics Heat and Mass Transfer Machines Magnetic Materials Magnetism Manufacturing Materials Science Metallic Materials Processes Solid Mechanics 재료공학 AFM Pitting Passive film Lean duplex stainless steel (LDSS) Immersion EIS
ISSN:	1598-9623, 2005-4149
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Abstract	The current study investigates the effect of long-term immersion on the corrosion response and the consequent passive film formation process of lean duplex stainless steel 2101 in 3.5 wt% NaCl solution. The corrosion behavior of the alloy has been monitored through long term immersion tests at different time intervals, viz . 0, 3, 5, 10, 20, 40, and 70 days. The electrochemical tests, such as potentiodynamic polarization and electrochemical impedance spectroscopy, have been performed after each immersion period to understand the change in corrosion rate and passivation behaviour, respectively, with respect to immersion duration. With the increase in immersion duration, the pitting potential ( E pit ) gradually shifts towards a nobler direction with a simultaneous reduction in corrosion rate ( r corr ). This has been attributed to the gradual increase in the thickness of the passive film with the increase in duration of immersion, as revealed through the EIS analysis. The passive film is found to become nearly stable after 40 days of immersion of the specimen in 3.5 wt% NaCl solution. Interestingly, the thickness and stability of the passive film obtained after 40 days of immersion in 3.5 wt% NaCl solution are comparable to the passive film that is formed in mildly passivating media, namely borate buffer solution. An investigation of post immersion surface morphology has also confirmed the gradual improvement in the uniformity and compactness of the oxide-rich passive layer with increase in immersion period, which eventually led to improved corrosion resistance of the alloy in the saline environment. Graphical Abstract
AbstractList	The current study investigates the effect of long-term immersion on the corrosion response and the consequent passive film formation process of lean duplex stainless steel 2101 in 3.5 wt% NaCl solution. The corrosion behavior of the alloy has been monitored through long term immersion tests at different time intervals, viz . 0, 3, 5, 10, 20, 40, and 70 days. The electrochemical tests, such as potentiodynamic polarization and electrochemical impedance spectroscopy, have been performed after each immersion period to understand the change in corrosion rate and passivation behaviour, respectively, with respect to immersion duration. With the increase in immersion duration, the pitting potential ( E pit ) gradually shifts towards a nobler direction with a simultaneous reduction in corrosion rate ( r corr ). This has been attributed to the gradual increase in the thickness of the passive film with the increase in duration of immersion, as revealed through the EIS analysis. The passive film is found to become nearly stable after 40 days of immersion of the specimen in 3.5 wt% NaCl solution. Interestingly, the thickness and stability of the passive film obtained after 40 days of immersion in 3.5 wt% NaCl solution are comparable to the passive film that is formed in mildly passivating media, namely borate buffer solution. An investigation of post immersion surface morphology has also confirmed the gradual improvement in the uniformity and compactness of the oxide-rich passive layer with increase in immersion period, which eventually led to improved corrosion resistance of the alloy in the saline environment. Graphical Abstract The current study investigates the effect of long-term immersion on the corrosion response and the consequent passive filmformation process of lean duplex stainless steel 2101 in 3.5 wt% NaCl solution. The corrosion behavior of the alloy has beenmonitored through long term immersion tests at different time intervals, viz. 0, 3, 5, 10, 20, 40, and 70 days. The electrochemicaltests, such as potentiodynamic polarization and electrochemical impedance spectroscopy, have been performedafter each immersion period to understand the change in corrosion rate and passivation behaviour, respectively, with respectto immersion duration. With the increase in immersion duration, the pitting potential (Epit) gradually shifts towards a noblerdirection with a simultaneous reduction in corrosion rate (rcorr). This has been attributed to the gradual increase in the thicknessof the passive film with the increase in duration of immersion, as revealed through the EIS analysis. The passive filmis found to become nearly stable after 40 days of immersion of the specimen in 3.5 wt% NaCl solution. Interestingly, thethickness and stability of the passive film obtained after 40 days of immersion in 3.5 wt% NaCl solution are comparable tothe passive film that is formed in mildly passivating media, namely borate buffer solution. An investigation of post immersionsurface morphology has also confirmed the gradual improvement in the uniformity and compactness of the oxide-richpassive layer with increase in immersion period, which eventually led to improved corrosion resistance of the alloy in thesaline environment. KCI Citation Count: 0
Author	Duley, Partha Mandal, Sumantra Bairi, Lipika Rani Bairagi, Darothi
Author_xml	– sequence: 1 givenname: Lipika Rani surname: Bairi fullname: Bairi, Lipika Rani email: lipikabairi@metal.iitkgp.ac.in, lrbairi@gmail.com organization: Department of Metallurgical and Materials Engineering, Indian Institute of Technology Kharagpur – sequence: 2 givenname: Darothi surname: Bairagi fullname: Bairagi, Darothi organization: Department of Metallurgical and Materials Engineering, Indian Institute of Technology Kharagpur – sequence: 3 givenname: Partha surname: Duley fullname: Duley, Partha organization: Department of Metallurgical and Materials Engineering, Indian Institute of Technology Kharagpur – sequence: 4 givenname: Sumantra surname: Mandal fullname: Mandal, Sumantra organization: Department of Metallurgical and Materials Engineering, Indian Institute of Technology Kharagpur
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Snippet	The current study investigates the effect of long-term immersion on the corrosion response and the consequent passive film formation process of lean duplex... The current study investigates the effect of long-term immersion on the corrosion response and the consequent passive filmformation process of lean duplex...
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Title	Effect of Long-Term Immersion on the Corrosion and Passivation Behavior of Lean Duplex Stainless Steel 2101 in 3.5 wt% NaCl Solution
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