Bi26Mo10O69–based solid solution with nonmetal dopants: Synthesis and properties

A series of S- and P- doped Bi26Mo10O69 was synthesized by conventional solid state method and studied. Chemical analysis detected closeness of experimental and theoretical ratios of bismuth, molybdenum and dopant for P-doped samples and 50% deficiency of sulfur for S-doped samples. The solid soluti...

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Vydáno v:	Solid state ionics Ročník 331; s. 30 - 36
Hlavní autoři:	Mikhaylovskaya, Zoya A., Petrova, Sofia A., Buyanova, Elena S., Morozova, Maria V.
Médium:	Journal Article
Jazyk:	angličtina
Vydáno:	Amsterdam Elsevier B.V 01.03.2019 Elsevier BV
Témata:	Bismuth Bismuth molybdates Bismuth oxide Chemical analysis Chemical synthesis Dopants Infrared spectroscopy Ion currents Molybdenum Organic chemistry Oxygen ion conductors Particle size Phosphor doping Solid solutions Solids Spectrum analysis Sulfur doping X-ray diffraction Oxygen ion conductors Bismuth oxide Phosphor doping Sulfur doping Bismuth molybdates
ISSN:	0167-2738, 1872-7689
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Abstract	A series of S- and P- doped Bi26Mo10O69 was synthesized by conventional solid state method and studied. Chemical analysis detected closeness of experimental and theoretical ratios of bismuth, molybdenum and dopant for P-doped samples and 50% deficiency of sulfur for S-doped samples. The solid solutions ranges were determined to be x = 0–0.7 for Bi26Mo10−2xP2xO69−d and x = 0–0.6 for Bi26Mo10−2xSxO69−d. Stabilization of the monoclinic form is observed when x > 0.1 for P and x > 0.4 for S doping. The IR FT spectroscopy and Rietveld whole profile structure refinement at X-Ray diffraction data showed substitution of Mo by S and P forming SO4 and PO4 groups. The geometrical sizes of particles were determined to be in the range of 1–20 μm. Materials under study are characterized with total ionic conductivity of the 1 × 10−4 − 9 × 10−3 S cm−1 at 273–1073 K. •S and doped Bi26Mo10O69−d solid solutions were synthesized by solid sate method.•Chemical analysis gave Bi26Mo10−2xP2xO69−d and Bi26Mo10−2xSxO69−d formulae.•Infrared spectroscopy detected SO4 and PO4 groups.•Impedance spectroscopy showed a modest increase in conductivity.
AbstractList	A series of S- and P- doped Bi26Mo10O69 was synthesized by conventional solid state method and studied. Chemical analysis detected closeness of experimental and theoretical ratios of bismuth, molybdenum and dopant for P-doped samples and 50% deficiency of sulfur for S-doped samples. The solid solutions ranges were determined to be x = 0-0.7 for Bi26Mo10-2xP2xO69-d and x = 0-0.6 for Bi26Mo10-2xSxO69-d. Stabilization of the monoclinic form is observed when x> 0.1 for P and x> 0.4 for S doping. The IR FT spectroscopy and Rietveld whole profile structure refinement at X-Ray diffraction data showed substitution of Mo by S and P forming SO4 and PO4 groups. The geometrical sizes of particles were determined to be in the range of 1-20 μm. Materials under study are characterized with total ionic conductivity of the 1 x 10-4 - 9 x 10-3 S cm-1 at 273-1073 K. A series of S- and P- doped Bi26Mo10O69 was synthesized by conventional solid state method and studied. Chemical analysis detected closeness of experimental and theoretical ratios of bismuth, molybdenum and dopant for P-doped samples and 50% deficiency of sulfur for S-doped samples. The solid solutions ranges were determined to be x = 0–0.7 for Bi26Mo10−2xP2xO69−d and x = 0–0.6 for Bi26Mo10−2xSxO69−d. Stabilization of the monoclinic form is observed when x > 0.1 for P and x > 0.4 for S doping. The IR FT spectroscopy and Rietveld whole profile structure refinement at X-Ray diffraction data showed substitution of Mo by S and P forming SO4 and PO4 groups. The geometrical sizes of particles were determined to be in the range of 1–20 μm. Materials under study are characterized with total ionic conductivity of the 1 × 10−4 − 9 × 10−3 S cm−1 at 273–1073 K. •S and doped Bi26Mo10O69−d solid solutions were synthesized by solid sate method.•Chemical analysis gave Bi26Mo10−2xP2xO69−d and Bi26Mo10−2xSxO69−d formulae.•Infrared spectroscopy detected SO4 and PO4 groups.•Impedance spectroscopy showed a modest increase in conductivity.
Author	Buyanova, Elena S. Morozova, Maria V. Mikhaylovskaya, Zoya A. Petrova, Sofia A.
Author_xml	– sequence: 1 givenname: Zoya A. orcidid: 0000-0002-0050-9216 surname: Mikhaylovskaya fullname: Mikhaylovskaya, Zoya A. email: zoya.mihaylovskaya@urfu.ru organization: Ural Federal University, Ekaterinburg 620000, Russia – sequence: 2 givenname: Sofia A. surname: Petrova fullname: Petrova, Sofia A. organization: Institute for Metallurgy, Ural Branch of the Russian Academy of Sciences, Ekaterinburg 620016, Russia – sequence: 3 givenname: Elena S. surname: Buyanova fullname: Buyanova, Elena S. email: elena.buyanova@urfu.ru organization: Ural Federal University, Ekaterinburg 620000, Russia – sequence: 4 givenname: Maria V. surname: Morozova fullname: Morozova, Maria V. organization: Ural Federal University, Ekaterinburg 620000, Russia
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Keywords	Oxygen ion conductors Bismuth oxide Phosphor doping Sulfur doping Bismuth molybdates
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Snippet	A series of S- and P- doped Bi26Mo10O69 was synthesized by conventional solid state method and studied. Chemical analysis detected closeness of experimental...
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SubjectTerms	Bismuth Bismuth molybdates Bismuth oxide Chemical analysis Chemical synthesis Dopants Infrared spectroscopy Ion currents Molybdenum Organic chemistry Oxygen ion conductors Particle size Phosphor doping Solid solutions Solids Spectrum analysis Sulfur doping X-ray diffraction
Title	Bi26Mo10O69–based solid solution with nonmetal dopants: Synthesis and properties
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