From liquid to thin film: colloidal suspensions for tungsten oxide as an electrode material for Li-ion batteries
Using a colloidal suspension, tungsten oxide thin films (150 nm) have been prepared via ultrasonic spray deposition using two different current collectors, namely TiN and Pt. First, the precursor chemistry was studied, revealing that the tungsten present is reduced due to the formation of chlorine g...
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| Vydáno v: | RSC advances Ročník 6; číslo 57; s. 51747 - 51756 |
|---|---|
| Hlavní autoři: | , , , , , , , , , |
| Médium: | Journal Article |
| Jazyk: | angličtina |
| Vydáno: |
01.01.2016
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| Témata: | |
| ISSN: | 2046-2069, 2046-2069 |
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| Abstract | Using a colloidal suspension, tungsten oxide thin films (150 nm) have been prepared
via
ultrasonic spray deposition using two different current collectors, namely TiN and Pt. First, the precursor chemistry was studied, revealing that the tungsten present is reduced due to the formation of chlorine gas. Due to a dehydrogenation 1,1-diethoxyethane (DEE) and hydrogen chloride (HCl) evolve from the precursor, reducing the chloride content of the precursor. The thin films were annealed at 400 and 500 C, yielding tetragonal tungsten oxide without the presence of chlorides. Electrochemical analysis indicated that the TiN current collector has a pronounced positive effect on cycling behavior of the WO
3
thin film. A higher annealing temperature yields an improved performance, but annealing at temperatures as low as 400 C also yielded electrochemically active WO
3
. The current study presents a versatile method to produce electrochemically active tungsten oxide thin films with a high volumetric capacity (640 mA h cm
3
) at relatively low temperature to be applied in all-solid-state Li-ion batteries.
Using a colloidal suspension, electrochemically active tungsten oxide thin films (150 nm) have been prepared
via
ultrasonic spray deposition using two different current collectors, namely TiN and Pt. |
|---|---|
| AbstractList | Using a colloidal suspension, tungsten oxide thin films (150 nm) have been prepared via ultrasonic spray deposition using two different current collectors, namely TiN and Pt. First, the precursor chemistry was studied, revealing that the tungsten present is reduced due to the formation of chlorine gas. Due to a dehydrogenation 1,1-diethoxyethane (DEE) and hydrogen chloride (HCl) evolve from the precursor, reducing the chloride content of the precursor. The thin films were annealed at 400 and 500 °C, yielding tetragonal tungsten oxide without the presence of chlorides. Electrochemical analysis indicated that the TiN current collector has a pronounced positive effect on cycling behavior of the WO₃ thin film. A higher annealing temperature yields an improved performance, but annealing at temperatures as low as 400 °C also yielded electrochemically active WO₃. The current study presents a versatile method to produce electrochemically active tungsten oxide thin films with a high volumetric capacity (640 mA h cm⁻³) at relatively low temperature to be applied in all-solid-state Li-ion batteries. Using a colloidal suspension, tungsten oxide thin films (150 nm) have been prepared via ultrasonic spray deposition using two different current collectors, namely TiN and Pt. First, the precursor chemistry was studied, revealing that the tungsten present is reduced due to the formation of chlorine gas. Due to a dehydrogenation 1,1-diethoxyethane (DEE) and hydrogen chloride (HCl) evolve from the precursor, reducing the chloride content of the precursor. The thin films were annealed at 400 and 500 C, yielding tetragonal tungsten oxide without the presence of chlorides. Electrochemical analysis indicated that the TiN current collector has a pronounced positive effect on cycling behavior of the WO 3 thin film. A higher annealing temperature yields an improved performance, but annealing at temperatures as low as 400 C also yielded electrochemically active WO 3 . The current study presents a versatile method to produce electrochemically active tungsten oxide thin films with a high volumetric capacity (640 mA h cm 3 ) at relatively low temperature to be applied in all-solid-state Li-ion batteries. Using a colloidal suspension, electrochemically active tungsten oxide thin films (150 nm) have been prepared via ultrasonic spray deposition using two different current collectors, namely TiN and Pt. Using a colloidal suspension, tungsten oxide thin films (150 nm) have been prepared via ultrasonic spray deposition using two different current collectors, namely TiN and Pt. First, the precursor chemistry was studied, revealing that the tungsten present is reduced due to the formation of chlorine gas. Due to a dehydrogenation 1,1-diethoxyethane (DEE) and hydrogen chloride (HCl) evolve from the precursor, reducing the chloride content of the precursor. The thin films were annealed at 400 and 500 °C, yielding tetragonal tungsten oxide without the presence of chlorides. Electrochemical analysis indicated that the TiN current collector has a pronounced positive effect on cycling behavior of the WO 3 thin film. A higher annealing temperature yields an improved performance, but annealing at temperatures as low as 400 °C also yielded electrochemically active WO 3 . The current study presents a versatile method to produce electrochemically active tungsten oxide thin films with a high volumetric capacity (640 mA h cm −3 ) at relatively low temperature to be applied in all-solid-state Li-ion batteries. |
| Author | Van Bael, M. K van den Ham, E. J Peys, N Marchal, W Bonneux, G Yaci, B Ulu, F Kokal, I Elen, K Hardy, A |
| AuthorAffiliation | Hasselt University Inorganic and Physical Chemistry and IMEC, Division IMOMEC Institute for Materials Research Ko University Surface Science and Technology Center (KUYTAM) Pavezyum Chemicals |
| AuthorAffiliation_xml | – sequence: 0 name: Ko University Surface Science and Technology Center (KUYTAM) – sequence: 0 name: Institute for Materials Research – sequence: 0 name: Inorganic and Physical Chemistry and IMEC, Division IMOMEC – sequence: 0 name: Hasselt University – sequence: 0 name: Pavezyum Chemicals |
| Author_xml | – sequence: 1 givenname: E. J surname: van den Ham fullname: van den Ham, E. J – sequence: 2 givenname: K surname: Elen fullname: Elen, K – sequence: 3 givenname: I surname: Kokal fullname: Kokal, I – sequence: 4 givenname: B surname: Yaci fullname: Yaci, B – sequence: 5 givenname: N surname: Peys fullname: Peys, N – sequence: 6 givenname: G surname: Bonneux fullname: Bonneux, G – sequence: 7 givenname: F surname: Ulu fullname: Ulu, F – sequence: 8 givenname: W surname: Marchal fullname: Marchal, W – sequence: 9 givenname: M. K surname: Van Bael fullname: Van Bael, M. K – sequence: 10 givenname: A surname: Hardy fullname: Hardy, A |
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| Snippet | Using a colloidal suspension, tungsten oxide thin films (150 nm) have been prepared
via
ultrasonic spray deposition using two different current collectors,... Using a colloidal suspension, tungsten oxide thin films (150 nm) have been prepared via ultrasonic spray deposition using two different current collectors,... |
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| SubjectTerms | annealing chlorides chlorine collectors colloids dehydrogenation electrochemistry electrodes hydrochloric acid liquids lithium batteries spray deposition temperature tungsten oxide ultrasonics |
| Title | From liquid to thin film: colloidal suspensions for tungsten oxide as an electrode material for Li-ion batteries |
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