Synthesis of Fe3O4-PVP nanocomposite functionalized with sulfonic group as an effective catalyst for one-pot synthesis of xanthene derivatives

An effective and environmentally friendly Fe 3 O 4 -PVP nanocomposite functionalized with sulfonic group, Fe 3 O 4 -PVP-SO 3 H, was synthesized and characterized as the heterogeneous nanocatalyst for one-pot synthesis of xanthene derivatives via condensation reaction of various aldehydes and dimedon...

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Veröffentlicht in:	Research on chemical intermediates Jg. 47; H. 11; S. 4537 - 4555
Hauptverfasser:	Karegar, Mohsen, Khodaei, Mohammad Mehdi
Format:	Journal Article
Sprache:	Englisch
Veröffentlicht:	Dordrecht Springer Netherlands 01.11.2021 Springer Nature B.V
Schlagworte:	Aldehydes Catalysis Catalysts Chemical synthesis Chemistry Chemistry and Materials Science Condensates Ethanol Inorganic Chemistry Iron oxides Nanocomposites Physical Chemistry Sulfonic acid Polyvinylpyrrolidone Solid acid nanocatalyst Magnetic nanoparticles Xanthene
ISSN:	0922-6168, 1568-5675
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Abstract	An effective and environmentally friendly Fe 3 O 4 -PVP nanocomposite functionalized with sulfonic group, Fe 3 O 4 -PVP-SO 3 H, was synthesized and characterized as the heterogeneous nanocatalyst for one-pot synthesis of xanthene derivatives via condensation reaction of various aldehydes and dimedone in ethanol media. The catalyst was efficient, and can be separated easily from the reaction mixture and recovered rapidly by an external magnetic field. It can be used five times without significant loss of its activity. Physicochemical properties were characterized using different techniques including FT-IR, XRD, FE-SEM, EDS, TGA, and VSM to illustrate the structure of the catalyst. The presence of sulfonic group on the surface of the catalyst was confirmed by these analyses. Large number of the acidic groups on the surface of the PVP layer led to the more activity of the catalyst and consequently, the yield of xanthene increases. The products were obtained in high yields with short reaction times.
AbstractList	An effective and environmentally friendly Fe3O4-PVP nanocomposite functionalized with sulfonic group, Fe3O4-PVP-SO3H, was synthesized and characterized as the heterogeneous nanocatalyst for one-pot synthesis of xanthene derivatives via condensation reaction of various aldehydes and dimedone in ethanol media. The catalyst was efficient, and can be separated easily from the reaction mixture and recovered rapidly by an external magnetic field. It can be used five times without significant loss of its activity. Physicochemical properties were characterized using different techniques including FT-IR, XRD, FE-SEM, EDS, TGA, and VSM to illustrate the structure of the catalyst. The presence of sulfonic group on the surface of the catalyst was confirmed by these analyses. Large number of the acidic groups on the surface of the PVP layer led to the more activity of the catalyst and consequently, the yield of xanthene increases. The products were obtained in high yields with short reaction times. An effective and environmentally friendly Fe 3 O 4 -PVP nanocomposite functionalized with sulfonic group, Fe 3 O 4 -PVP-SO 3 H, was synthesized and characterized as the heterogeneous nanocatalyst for one-pot synthesis of xanthene derivatives via condensation reaction of various aldehydes and dimedone in ethanol media. The catalyst was efficient, and can be separated easily from the reaction mixture and recovered rapidly by an external magnetic field. It can be used five times without significant loss of its activity. Physicochemical properties were characterized using different techniques including FT-IR, XRD, FE-SEM, EDS, TGA, and VSM to illustrate the structure of the catalyst. The presence of sulfonic group on the surface of the catalyst was confirmed by these analyses. Large number of the acidic groups on the surface of the PVP layer led to the more activity of the catalyst and consequently, the yield of xanthene increases. The products were obtained in high yields with short reaction times.
Author	Khodaei, Mohammad Mehdi Karegar, Mohsen
Author_xml	– sequence: 1 givenname: Mohsen surname: Karegar fullname: Karegar, Mohsen organization: Department of Organic Chemistry, Razi University – sequence: 2 givenname: Mohammad Mehdi orcidid: 0000-0002-0385-9203 surname: Khodaei fullname: Khodaei, Mohammad Mehdi email: mmkhoda@razi.ac.ir organization: Department of Organic Chemistry, Razi University, Nanoscience & Nanotechnology Research Center (NNRC), Razi University
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Snippet	An effective and environmentally friendly Fe 3 O 4 -PVP nanocomposite functionalized with sulfonic group, Fe 3 O 4 -PVP-SO 3 H, was synthesized and... An effective and environmentally friendly Fe3O4-PVP nanocomposite functionalized with sulfonic group, Fe3O4-PVP-SO3H, was synthesized and characterized as the...
SourceID	proquest crossref springer
SourceType	Aggregation Database Enrichment Source Index Database Publisher
StartPage	4537
SubjectTerms	Aldehydes Catalysis Catalysts Chemical synthesis Chemistry Chemistry and Materials Science Condensates Ethanol Inorganic Chemistry Iron oxides Nanocomposites Physical Chemistry Sulfonic acid
Title	Synthesis of Fe3O4-PVP nanocomposite functionalized with sulfonic group as an effective catalyst for one-pot synthesis of xanthene derivatives
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