Effects of neutron–gamma radiation on the free radical contents in epoxy resin: upconversion luminescence and structural stabilization

The purpose of this work is to study the effect of mixed neutron–gamma radiation (MNGR) on structural, optical and paramagnetic properties on epoxy resin nanostructure thin films [ER] NSTF . These films were prepared and irradiated in the nuclear reactor with dose range between 100 and 900 Gy. After...

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Vydáno v:	Applied physics. A, Materials science & processing Ročník 125; číslo 11; s. 1 - 9
Hlavní autoři:	Kacem, I., Daoudi, M., Dridi, W., Sellemi, H., Harzli, K., De Izzara, G., Geslot, B., Guermazi, H., Blaise, P., Hosni, F., Al-Hossainy, Ahmed F., Bourezgui, A., Chtourou, R.
Médium:	Journal Article
Jazyk:	angličtina
Vydáno:	Berlin/Heidelberg Springer Berlin Heidelberg 01.11.2019 Springer Nature B.V
Témata:	Applied physics C band Chain scission Characterization and Evaluation of Materials Cleavage Condensed Matter Physics Crosslinking Crystal defects Crystal structure Crystallinity Epoxy resins Free radicals Gamma rays Luminescence Machines Manufacturing Materials science Nanotechnology Nuclear reactors Optical and Electronic Materials Optical properties Physics Physics and Astronomy Processes Radiation dosage Surfaces and Interfaces Thin Films Upconversion
ISSN:	0947-8396, 1432-0630
On-line přístup:	Získat plný text
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Abstract	The purpose of this work is to study the effect of mixed neutron–gamma radiation (MNGR) on structural, optical and paramagnetic properties on epoxy resin nanostructure thin films [ER] NSTF . These films were prepared and irradiated in the nuclear reactor with dose range between 100 and 900 Gy. After exposure to MNGR, FT-IR results demonstrated the broad ν (OH) and ν (C=O) band to increase with increase in radiation dose, while the ν (C–H) band decreased with increase in radiation dose. This is due to the formation of chain stretch, bending and scission/cross-linking through MNGR that lead to a decrease in the crystallinity region contained within the [ER] NSTF . XRD data confirm these results and show that the crystalline phase was destroyed by MNGR irradiation. PL is used to determine the fundamental transition and defects transitions in [ER] NSTF at 300 K. It was found that MNGR leads to significant enhancement of the luminescence properties. Samples of [ER] NSTF irradiated with 600 Gy dose presented the highest response. Therefore, EPR results confirmed that MNGR induces the paramagnetic center’s formation of the [ER] NSTF whose concentration varies differently.
AbstractList	The purpose of this work is to study the effect of mixed neutron–gamma radiation (MNGR) on structural, optical and paramagnetic properties on epoxy resin nanostructure thin films [ER] NSTF . These films were prepared and irradiated in the nuclear reactor with dose range between 100 and 900 Gy. After exposure to MNGR, FT-IR results demonstrated the broad ν (OH) and ν (C=O) band to increase with increase in radiation dose, while the ν (C–H) band decreased with increase in radiation dose. This is due to the formation of chain stretch, bending and scission/cross-linking through MNGR that lead to a decrease in the crystallinity region contained within the [ER] NSTF . XRD data confirm these results and show that the crystalline phase was destroyed by MNGR irradiation. PL is used to determine the fundamental transition and defects transitions in [ER] NSTF at 300 K. It was found that MNGR leads to significant enhancement of the luminescence properties. Samples of [ER] NSTF irradiated with 600 Gy dose presented the highest response. Therefore, EPR results confirmed that MNGR induces the paramagnetic center’s formation of the [ER] NSTF whose concentration varies differently. The purpose of this work is to study the effect of mixed neutron–gamma radiation (MNGR) on structural, optical and paramagnetic properties on epoxy resin nanostructure thin films [ER]NSTF. These films were prepared and irradiated in the nuclear reactor with dose range between 100 and 900 Gy. After exposure to MNGR, FT-IR results demonstrated the broad ν(OH) and ν(C=O) band to increase with increase in radiation dose, while the ν(C–H) band decreased with increase in radiation dose. This is due to the formation of chain stretch, bending and scission/cross-linking through MNGR that lead to a decrease in the crystallinity region contained within the [ER]NSTF. XRD data confirm these results and show that the crystalline phase was destroyed by MNGR irradiation. PL is used to determine the fundamental transition and defects transitions in [ER]NSTF at 300 K. It was found that MNGR leads to significant enhancement of the luminescence properties. Samples of [ER]NSTF irradiated with 600 Gy dose presented the highest response. Therefore, EPR results confirmed that MNGR induces the paramagnetic center’s formation of the [ER]NSTF whose concentration varies differently.
ArticleNumber	758
Author	Bourezgui, A. Sellemi, H. Dridi, W. De Izzara, G. Chtourou, R. Harzli, K. Daoudi, M. Blaise, P. Al-Hossainy, Ahmed F. Kacem, I. Geslot, B. Hosni, F. Guermazi, H.
Author_xml	– sequence: 1 givenname: I. surname: Kacem fullname: Kacem, I. organization: Faculty of Mathematical, Physical and Natural Sciences of Tunis, University of Tunis El Manar, Nanomaterials and Systems for Renewable Energy Laboratory, Research and Technology Center of Energy, Faculty of Science, Northern Border University – sequence: 2 givenname: M. surname: Daoudi fullname: Daoudi, M. organization: Energy and Matter Research Laboratory (LR16CNSTN02), National Centre for Nuclear Sciences and Technology – sequence: 3 givenname: W. surname: Dridi fullname: Dridi, W. organization: Energy and Matter Research Laboratory (LR16CNSTN02), National Centre for Nuclear Sciences and Technology – sequence: 4 givenname: H. surname: Sellemi fullname: Sellemi, H. organization: Energy and Matter Research Laboratory (LR16CNSTN02), National Centre for Nuclear Sciences and Technology – sequence: 5 givenname: K. surname: Harzli fullname: Harzli, K. organization: Energy and Matter Research Laboratory (LR16CNSTN02), National Centre for Nuclear Sciences and Technology – sequence: 6 givenname: G. surname: De Izzara fullname: De Izzara, G. organization: Experimental Programs Laboratory (LPE) – sequence: 7 givenname: B. surname: Geslot fullname: Geslot, B. organization: Experimental Programs Laboratory (LPE) – sequence: 8 givenname: H. surname: Guermazi fullname: Guermazi, H. organization: Research Unit, Physics of Insulating and Semi-insulating Materials, University of Sfax – sequence: 9 givenname: P. surname: Blaise fullname: Blaise, P. organization: Experimental Programs Laboratory (LPE) – sequence: 10 givenname: F. surname: Hosni fullname: Hosni, F. organization: Energy and Matter Research Laboratory (LR16CNSTN02), National Centre for Nuclear Sciences and Technology, Faculty of Sciences, University of Bisha – sequence: 11 givenname: Ahmed F. orcidid: 0000-0001-5531-6940 surname: Al-Hossainy fullname: Al-Hossainy, Ahmed F. email: ahmed73chem@scinv.au.edu.eg organization: Faculty of Science, Northern Border University, Faculty of Science, Chemistry Department, New Valley University – sequence: 12 givenname: A. surname: Bourezgui fullname: Bourezgui, A. organization: Faculty of Mathematical, Physical and Natural Sciences of Tunis, University of Tunis El Manar, Nanomaterials and Systems for Renewable Energy Laboratory, Research and Technology Center of Energy, Faculty of Science, Northern Border University – sequence: 13 givenname: R. surname: Chtourou fullname: Chtourou, R. organization: Nanomaterials and Systems for Renewable Energy Laboratory, Research and Technology Center of Energy
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Snippet	The purpose of this work is to study the effect of mixed neutron–gamma radiation (MNGR) on structural, optical and paramagnetic properties on epoxy resin...
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SubjectTerms	Applied physics C band Chain scission Characterization and Evaluation of Materials Cleavage Condensed Matter Physics Crosslinking Crystal defects Crystal structure Crystallinity Epoxy resins Free radicals Gamma rays Luminescence Machines Manufacturing Materials science Nanotechnology Nuclear reactors Optical and Electronic Materials Optical properties Physics Physics and Astronomy Processes Radiation dosage Surfaces and Interfaces Thin Films Upconversion
Title	Effects of neutron–gamma radiation on the free radical contents in epoxy resin: upconversion luminescence and structural stabilization
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