Low-firing, temperature stable and improved microwave dielectric properties of ZnO-TiO2-Nb2O5 composite ceramics
This article presents low-firing, low-loss and temperature stable ZnOTiO2Nb2O5 microwave dielectric composite ceramics with the assistance of lithium borosilicate (LBS) and zinc borosilicate (ZBS) glass frits. There is a liquid phase (eutectic mixture) generated by LBS (ZBS) glass, and solid parti...
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| Vydáno v: | Journal of Materiomics Ročník 5; číslo 3; s. 471 - 479 |
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| Jazyk: | angličtina |
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Elsevier
01.09.2019
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| ISSN: | 2352-8478 |
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| Abstract | This article presents low-firing, low-loss and temperature stable ZnOTiO2Nb2O5 microwave dielectric composite ceramics with the assistance of lithium borosilicate (LBS) and zinc borosilicate (ZBS) glass frits. There is a liquid phase (eutectic mixture) generated by LBS (ZBS) glass, and solid particles could be wetted and dissolved. Therefore, the migrations and rearrangements of particles could be performed. Besides, compared with ceramics undoped with glass frits, lower activation energies (Ea) of ceramics doped with LBS and ZBS glass suggest that the low-temperature sintering behavior is easier to carry out. The results indicated that LBS and ZBS glass both are effective sintering aids to accelerate the sintering process and improve the microwave dielectric properties of composite ceramics by controlling the phase compositions under low temperature. Combination great properties of ZnOTiO2Nb2O5 ceramics were obtained when sintered at 900 °C for 4 h: εr = 36.7, Q × f = 20,000 GHz, τf = 7 ppm/oC. Keywords: ZnO-TiO2Nb2O5, Composite ceramics, Dielectric |
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| AbstractList | This article presents low-firing, low-loss and temperature stable ZnOTiO2Nb2O5 microwave dielectric composite ceramics with the assistance of lithium borosilicate (LBS) and zinc borosilicate (ZBS) glass frits. There is a liquid phase (eutectic mixture) generated by LBS (ZBS) glass, and solid particles could be wetted and dissolved. Therefore, the migrations and rearrangements of particles could be performed. Besides, compared with ceramics undoped with glass frits, lower activation energies (Ea) of ceramics doped with LBS and ZBS glass suggest that the low-temperature sintering behavior is easier to carry out. The results indicated that LBS and ZBS glass both are effective sintering aids to accelerate the sintering process and improve the microwave dielectric properties of composite ceramics by controlling the phase compositions under low temperature. Combination great properties of ZnOTiO2Nb2O5 ceramics were obtained when sintered at 900 °C for 4 h: εr = 36.7, Q × f = 20,000 GHz, τf = 7 ppm/oC. Keywords: ZnO-TiO2Nb2O5, Composite ceramics, Dielectric |
| Author | Fang, Zixuan Chen, Yawei Zhang, Shuren Li, Enzhu Yuan, Ying Yang, Hongyu Yang, Hongcheng |
| Author_xml | – sequence: 1 givenname: Hongyu surname: Yang fullname: Yang, Hongyu – sequence: 2 givenname: Shuren surname: Zhang fullname: Zhang, Shuren – sequence: 3 givenname: Yawei surname: Chen fullname: Chen, Yawei – sequence: 4 givenname: Hongcheng surname: Yang fullname: Yang, Hongcheng – sequence: 5 givenname: Zixuan surname: Fang fullname: Fang, Zixuan – sequence: 6 givenname: Ying surname: Yuan fullname: Yuan, Ying – sequence: 7 givenname: Enzhu surname: Li fullname: Li, Enzhu |
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