Adjusting Al location in the framework of ITH zeolites for catalytic conversion of methanol to olefins

Adjusting location and distribution of Al sites in the zeolite framework is critical for catalysis, and typical strategies include using zeolites as starting Al source. However, this approach is still challenging for aluminosilicate ITH zeolite. Herein, the distribution of Al species in the framewor...

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Vydané v:	Chinese journal of catalysis Ročník 56; s. 114 - 121
Hlavní autori:	Fan, Kai, Wu, Qinming, Liu, Shuo, Kong, Haiyu, Wang, Sen, Kunkes, Eduard, Baerdemaeker, Trees De, Parvulescu, Andrei-Nicolae, Bottke, Nils, Yokoi, Toshiyuki, Vos, Dirk E. De, Meng, Xiangju, Zhang, Weiping, Xiao, Feng-Shou
Médium:	Journal Article
Jazyk:	English
Vydavateľské údaje:	Elsevier B.V 01.01.2024
Predmet:	27Al MAS NMR spectroscopy Al location in the framework Aluminosilicate ITH zeolite Methanol to olefins Al location in the framework Methanol to olefins 27Al MAS NMR spectroscopy Aluminosilicate ITH zeolite
ISSN:	1872-2067, 1872-2067
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Abstract	Adjusting location and distribution of Al sites in the zeolite framework is critical for catalysis, and typical strategies include using zeolites as starting Al source. However, this approach is still challenging for aluminosilicate ITH zeolite. Herein, the distribution of Al species in the framework of ITH was efficiently regulated by implementing LTA zeolite as the aluminum source added in the starting gels (LTA-ITH). The obtained LTA-ITH zeolites have similar nanosheet morphology, textual parameters, and acidic properties to those of conventional ITH synthesized from boehmite (C-ITH), while the results of 27Al MAS NMR spectra and 1-hexene cracking indicate that they have a different Al distribution. The use of LTA zeolite in starting gel is favorable for the formation of more Al species in sinusoidal and straight channels, compared with the C-ITH. Catalytic tests in the conversion of methanol to light olefin showed that LTA-ITH exhibited enhanced catalyst lifetime and propene selectivity compared with the C-ITH, which is reasonably attributed to the different locations of Al species in their respective ITH frameworks. [Display omitted]
AbstractList	Adjusting location and distribution of Al sites in the zeolite framework is critical for catalysis, and typical strategies include using zeolites as starting Al source. However, this approach is still challenging for aluminosilicate ITH zeolite. Herein, the distribution of Al species in the framework of ITH was efficiently regulated by implementing LTA zeolite as the aluminum source added in the starting gels (LTA-ITH). The obtained LTA-ITH zeolites have similar nanosheet morphology, textual parameters, and acidic properties to those of conventional ITH synthesized from boehmite (C-ITH), while the results of 27Al MAS NMR spectra and 1-hexene cracking indicate that they have a different Al distribution. The use of LTA zeolite in starting gel is favorable for the formation of more Al species in sinusoidal and straight channels, compared with the C-ITH. Catalytic tests in the conversion of methanol to light olefin showed that LTA-ITH exhibited enhanced catalyst lifetime and propene selectivity compared with the C-ITH, which is reasonably attributed to the different locations of Al species in their respective ITH frameworks. [Display omitted]
Author	Wu, Qinming Yokoi, Toshiyuki Wang, Sen Bottke, Nils Vos, Dirk E. De Kong, Haiyu Xiao, Feng-Shou Fan, Kai Parvulescu, Andrei-Nicolae Kunkes, Eduard Baerdemaeker, Trees De Meng, Xiangju Zhang, Weiping Liu, Shuo
Author_xml	– sequence: 1 givenname: Kai surname: Fan fullname: Fan, Kai organization: Key Lab of Applied Chemistry of Zhejiang Province, Department of Chemistry, Zhejiang University, Hangzhou 310028, Zhejiang, China – sequence: 2 givenname: Qinming surname: Wu fullname: Wu, Qinming organization: College of Chemical and Biological Engineering, Zhejiang University, Hangzhou 310028, Zhejiang, China – sequence: 3 givenname: Shuo surname: Liu fullname: Liu, Shuo organization: State Key Laboratory of Fine Chemicals, Dalian University of Technology, Dalian 116012, Liaoning, China – sequence: 4 givenname: Haiyu surname: Kong fullname: Kong, Haiyu organization: State Key Laboratory of Fine Chemicals, Dalian University of Technology, Dalian 116012, Liaoning, China – sequence: 5 givenname: Sen surname: Wang fullname: Wang, Sen organization: State Key Laboratory of Coal Conversion, Institute of Coal Chemistry, Chinese Academy of Sciences, Taiyuan 030001, Shanxi, China – sequence: 6 givenname: Eduard surname: Kunkes fullname: Kunkes, Eduard organization: BASF SE, Ludwigshafen 67056, Germany – sequence: 7 givenname: Trees De surname: Baerdemaeker fullname: Baerdemaeker, Trees De organization: BASF SE, Ludwigshafen 67056, Germany – sequence: 8 givenname: Andrei-Nicolae surname: Parvulescu fullname: Parvulescu, Andrei-Nicolae organization: BASF SE, Ludwigshafen 67056, Germany – sequence: 9 givenname: Nils surname: Bottke fullname: Bottke, Nils organization: BASF SE, Ludwigshafen 67056, Germany – sequence: 10 givenname: Toshiyuki surname: Yokoi fullname: Yokoi, Toshiyuki organization: Chemical Resources Laboratory, Tokyo Institute of Technology, Yokohama 226-8503, Japan – sequence: 11 givenname: Dirk E. De surname: Vos fullname: Vos, Dirk E. De organization: Centre for Surface Chemistry and Catalysis, KU Leuven, Kasteelpark Arenberg 23, Leuven 3001, Belgium – sequence: 12 givenname: Xiangju surname: Meng fullname: Meng, Xiangju email: mengxj@zju.edu.cn organization: Key Lab of Applied Chemistry of Zhejiang Province, Department of Chemistry, Zhejiang University, Hangzhou 310028, Zhejiang, China – sequence: 13 givenname: Weiping surname: Zhang fullname: Zhang, Weiping email: wpzhang@dlut.edu.cn organization: State Key Laboratory of Fine Chemicals, Dalian University of Technology, Dalian 116012, Liaoning, China – sequence: 14 givenname: Feng-Shou surname: Xiao fullname: Xiao, Feng-Shou email: fsxiao@zju.edu.cn organization: College of Chemical and Biological Engineering, Zhejiang University, Hangzhou 310028, Zhejiang, China
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Keywords	Al location in the framework Methanol to olefins 27Al MAS NMR spectroscopy Aluminosilicate ITH zeolite
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Snippet	Adjusting location and distribution of Al sites in the zeolite framework is critical for catalysis, and typical strategies include using zeolites as starting...
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SubjectTerms	27Al MAS NMR spectroscopy Al location in the framework Aluminosilicate ITH zeolite Methanol to olefins
Title	Adjusting Al location in the framework of ITH zeolites for catalytic conversion of methanol to olefins
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