Kinetics and mechanism of nonisothermal crystallization of biobased poly(hexamethylene 2,5-furan dicarboxylate)
Biobased poly(hexamethylene 2,5-furan dicarboxylate) (PHF) was synthesized by the two-stage melt polycondensation method (transesterification and polycondensation) in a glass batch reactor. The nonisothermal crystallization from the melt and from the glass was studied by means of Differential Scanni...
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| Published in: | Polymer (Guilford) Vol. 285; p. 126366 |
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| Main Authors: | , , , , |
| Format: | Journal Article |
| Language: | English |
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Elsevier Ltd
20.10.2023
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| ISSN: | 0032-3861, 1873-2291 |
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| Abstract | Biobased poly(hexamethylene 2,5-furan dicarboxylate) (PHF) was synthesized by the two-stage melt polycondensation method (transesterification and polycondensation) in a glass batch reactor. The nonisothermal crystallization from the melt and from the glass was studied by means of Differential Scanning Calorimetry, Fast Scanning Calorimetry and advanced kinetic analysis. It is shown that changes in the crystallization regime occurs at certain temperatures and that the end of the crystallization presents some deviation from what is predicted by the Hoffman-Lauritzen's theory of growth rate. A method is presented that allows the determination of the equilibrium melting temperature, the infinite glass transition temperature, the temperature at maximum of the growth rate, and accurate simulation of crystallization rate curves. An equation is proposed for modelling the crystallization process using a methodology that avoid the problem of local minima occurring when too many parameters must be determined simultaneously.
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•Nonisothermal crystallization of a new biobased polyester.•Changes in the crystallization regime occurs at certain temperatures.•A new method allows the determination of key parameters of crystallization processes.•Accurate simulation of crystallization rate curves are obtained.•The method can be extended to modelling crystallization of polymers in processing applications. |
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| AbstractList | Biobased poly(hexamethylene 2,5-furan dicarboxylate) (PHF) was synthesized by the two-stage melt polycondensation method (transesterification and polycondensation) in a glass batch reactor. The nonisothermal crystallization from the melt and from the glass was studied by means of Differential Scanning Calorimetry, Fast Scanning Calorimetry and advanced kinetic analysis. It is shown that changes in the crystallization regime occurs at certain temperatures and that the end of the crystallization presents some deviation from what is predicted by the Hoffman-Lauritzen's theory of growth rate. A method is presented that allows the determination of the equilibrium melting temperature, the infinite glass transition temperature, the temperature at maximum of the growth rate, and accurate simulation of crystallization rate curves. An equation is proposed for modelling the crystallization process using a methodology that avoid the problem of local minima occurring when too many parameters must be determined simultaneously.
[Display omitted]
•Nonisothermal crystallization of a new biobased polyester.•Changes in the crystallization regime occurs at certain temperatures.•A new method allows the determination of key parameters of crystallization processes.•Accurate simulation of crystallization rate curves are obtained.•The method can be extended to modelling crystallization of polymers in processing applications. |
| ArticleNumber | 126366 |
| Author | Poulopoulou, Nikki Sbirrazzuoli, Nicolas Papageorgiou, George Z. Bikiaris, Dimitrios N. Guigo, Nathanaël |
| Author_xml | – sequence: 1 givenname: Nathanaël surname: Guigo fullname: Guigo, Nathanaël organization: Université Côte d’Azur, Institut de Chimie de Nice (ICN) UMR CNRS 7272, Parc Valrose, Nice, France – sequence: 2 givenname: George Z. orcidid: 0000-0003-2239-6985 surname: Papageorgiou fullname: Papageorgiou, George Z. organization: Chemistry Department, University of Ioannina, P.O. Box 1186, 45110, Ioannina, Greece – sequence: 3 givenname: Nikki orcidid: 0000-0001-7119-551X surname: Poulopoulou fullname: Poulopoulou, Nikki organization: Chemistry Department, University of Ioannina, P.O. Box 1186, 45110, Ioannina, Greece – sequence: 4 givenname: Dimitrios N. orcidid: 0000-0001-8458-4952 surname: Bikiaris fullname: Bikiaris, Dimitrios N. organization: Laboratory of Polymer Chemistry and Technology, Department of Chemistry, Aristotle University of Thessaloniki, GR-541 24, Greece – sequence: 5 givenname: Nicolas orcidid: 0000-0002-6031-5448 surname: Sbirrazzuoli fullname: Sbirrazzuoli, Nicolas email: Nicolas.SBIRRAZZUOLI@univ-cotedazur.fr organization: Université Côte d’Azur, Institut de Chimie de Nice (ICN) UMR CNRS 7272, Parc Valrose, Nice, France |
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| CitedBy_id | crossref_primary_10_1021_acs_macromol_5c00826 crossref_primary_10_1016_j_polymer_2025_128845 crossref_primary_10_1016_j_tca_2024_179688 crossref_primary_10_1016_j_cej_2025_166848 crossref_primary_10_1016_j_polymertesting_2025_108924 crossref_primary_10_3390_separations12050131 |
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| Keywords | Sbirrazzuoli crystallization method Biobased polyester Isoconversional methods Crystallization kinetics 2,5-furandicarboxylic acid |
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| SubjectTerms | 2,5-furandicarboxylic acid Biobased polyester Crystallization kinetics Isoconversional methods Sbirrazzuoli crystallization method |
| Title | Kinetics and mechanism of nonisothermal crystallization of biobased poly(hexamethylene 2,5-furan dicarboxylate) |
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