Facile fabrication of Au/SiO2 nanostructures from 1D to 3D nanotubes networks using templating methods
We report a facile fabrication method for free-standing gold (Au) or silica (SiO2) nanotubes with highly controlled geometry and ordered porosity (pNTs) and their nanostructuration from 1D to 3D interconnected networks. A dual nano-templating method was employed using polycarbonate membranes as firs...
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| Vydané v: | Catalysis today Ročník 429; s. 114472 |
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| Hlavní autori: | , , , |
| Médium: | Journal Article |
| Jazyk: | English |
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Elsevier B.V
01.03.2024
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| ISSN: | 0920-5861, 1873-4308 |
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| Abstract | We report a facile fabrication method for free-standing gold (Au) or silica (SiO2) nanotubes with highly controlled geometry and ordered porosity (pNTs) and their nanostructuration from 1D to 3D interconnected networks. A dual nano-templating method was employed using polycarbonate membranes as first mold for the nanotubes, together with stacked polystyrene (PS) nanospheres to induce porosity. The pore size in the final nanotube walls can be controlled by adjusting the ratio x (where x = internal diameter of the nanotube divided by the diameter of the nanospheres), which determines the packing order of the spheres in the tubes. Then, gold electroless or silica sol-gel deposition were performed in the dual-templated structure to obtain Au or SiO2 pNTs, respectively. The templates removal was performed in one step using dichloromethane. A further functionalization of the silica pNTs with Au NPs using the electroless deposition method was successfully implemented as well, leading to a homogeneous dispersion of Au NPs with a size of 11 ± 2.8 nm. Chemical compositions and optical properties of the so-obtained materials were determined by XPS and UV–visible analyses, respectively.
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| AbstractList | We report a facile fabrication method for free-standing gold (Au) or silica (SiO2) nanotubes with highly controlled geometry and ordered porosity (pNTs) and their nanostructuration from 1D to 3D interconnected networks. A dual nano-templating method was employed using polycarbonate membranes as first mold for the nanotubes, together with stacked polystyrene (PS) nanospheres to induce porosity. The pore size in the final nanotube walls can be controlled by adjusting the ratio x (where x = internal diameter of the nanotube divided by the diameter of the nanospheres), which determines the packing order of the spheres in the tubes. Then, gold electroless or silica sol-gel deposition were performed in the dual-templated structure to obtain Au or SiO2 pNTs, respectively. The templates removal was performed in one step using dichloromethane. A further functionalization of the silica pNTs with Au NPs using the electroless deposition method was successfully implemented as well, leading to a homogeneous dispersion of Au NPs with a size of 11 ± 2.8 nm. Chemical compositions and optical properties of the so-obtained materials were determined by XPS and UV–visible analyses, respectively.
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| ArticleNumber | 114472 |
| Author | Drault, Fabien Eloy, Pierre Hermans, Sophie Demoustier-Champagne, Sophie |
| Author_xml | – sequence: 1 givenname: Fabien orcidid: 0000-0002-2887-1700 surname: Drault fullname: Drault, Fabien email: fabien.drault@uclouvain.be organization: Institute of Condensed Matter and Nanosciences (BSMA division), UCLouvain, Croix du Sud 1, B-1348 Louvain-la-Neuve, Belgium – sequence: 2 givenname: Pierre surname: Eloy fullname: Eloy, Pierre organization: Institute of Condensed Matter and Nanosciences (MOST division), UCLouvain, 1 Place Louis Pasteur, B-1348 Louvain-la, Neuve, Belgium – sequence: 3 givenname: Sophie surname: Demoustier-Champagne fullname: Demoustier-Champagne, Sophie email: sophie.demoustier@uclouvain.be organization: Institute of Condensed Matter and Nanosciences (BSMA division), UCLouvain, Croix du Sud 1, B-1348 Louvain-la-Neuve, Belgium – sequence: 4 givenname: Sophie surname: Hermans fullname: Hermans, Sophie email: sophie.hermans@uclouvain.be organization: Institute of Condensed Matter and Nanosciences (MOST division), UCLouvain, 1 Place Louis Pasteur, B-1348 Louvain-la, Neuve, Belgium |
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| Keywords | Interconnected porous nanotube networks Electroless plating Gold nanoparticles Sol-gel deposition Dual-templates method Silica nanotubes |
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| Title | Facile fabrication of Au/SiO2 nanostructures from 1D to 3D nanotubes networks using templating methods |
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