Catalytic oxidation of organic sulfides by new iron-chloro Schiff base complexes: The effect of methoxy substitution and ligand isomerism on the electronic, electrochemical and catalytic performance of the complexes

Four new iron-chloro Schiff base complexes were used as catalyst for selective oxidation of sulfides and the results are discussed based on the presence of OMe substitution and ligand isomerism. [Display omitted] Four new Fe(III)-Chloro Schiff base complexes were synthesized and characterized. The N...

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Vydáno v:	Polyhedron Ročník 200; s. 115135 - 115142
Hlavní autoři:	Aghvami, Fatemeh, Ghaffari, Abolfazl, Kucerakova, Monika, Dusek, Michal, Karimi-Nami, Rahman, Amini, Mojtaba, Behzad, Mahdi
Médium:	Journal Article
Jazyk:	angličtina
Vydáno:	OXFORD Elsevier Ltd 15.05.2021 Elsevier
Témata:	Catalysis Chemistry Chemistry, Inorganic & Nuclear Crystallography Iron-chloro Physical Sciences Schiff base Science & Technology Sulfoxidation Schiff base Catalysis Sulfoxidation Iron-chloro SULFOXIDES FE(III) SELECTIVE OXIDATION COPPER(II) SALEN CRYSTAL
ISSN:	0277-5387, 1873-3719
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Abstract	Four new iron-chloro Schiff base complexes were used as catalyst for selective oxidation of sulfides and the results are discussed based on the presence of OMe substitution and ligand isomerism. [Display omitted] Four new Fe(III)-Chloro Schiff base complexes were synthesized and characterized. The N2O2 type tetradentate Schiff base ligands were synthesized from the condensation of meso-1,2-diphenyl-1,2-ethylenediamine with salicylaldehyde (H2L1), 3-methoxysalicylaldehyde (H2L2), 4-methoxysalicylaldehyde (H2L3) and 5-methoxysalicylaldehyde (H2L4). The corresponding iron-chloro complexes with the general formula [Fe(Ln)Cl] (n = 1–4 for complexes (1–4)) were characterized by FTIR and UV–Vis spectroscopy and elemental analysis. Crystal structure of (1) was obtained by single-crystal X-ray crystallography. Cyclic voltammetry was used to study the electrochemistry of the complexes. The complexes were used as catalysts for the selective oxidation of organic sulfide compounds to sulfoxides. High catalytic performance and selectivity were obtained. The spectroscopic, electrochemical and catalytic data are discussed based on the electronic, steric and electrochemical properties of the complexes.
AbstractList	Four new Fe(III)-Chloro Schiff base complexes were synthesized and characterized. The N2O2 type tetradentate Schiff base ligands were synthesized from the condensation of meso-1,2-diphenyl-1,2-ethylenediamine with salicylaldehyde (H2L1), 3-methoxysalicylaldehyde (H2L2), 4-methoxysalicylaldehyde (H2L3) and 5-methoxysalicylaldehyde (H2L4). The corresponding iron-chloro complexes with the general formula [Fe(L-n)Cl] (n = 1-4 for complexes (1-4)) were characterized by FTIR and UV-Vis spectroscopy and elemental analysis. Crystal structure of (1) was obtained by single-crystal X-ray crystallography. Cyclic voltammetry was used to study the electrochemistry of the complexes. The complexes were used as catalysts for the selective oxidation of organic sulfide compounds to sulfoxides. High catalytic performance and selectivity were obtained. The spectroscopic, electrochemical and catalytic data are discussed based on the electronic, steric and electrochemical properties of the complexes. (C) 2021 Elsevier Ltd. All rights reserved. Four new iron-chloro Schiff base complexes were used as catalyst for selective oxidation of sulfides and the results are discussed based on the presence of OMe substitution and ligand isomerism. [Display omitted] Four new Fe(III)-Chloro Schiff base complexes were synthesized and characterized. The N2O2 type tetradentate Schiff base ligands were synthesized from the condensation of meso-1,2-diphenyl-1,2-ethylenediamine with salicylaldehyde (H2L1), 3-methoxysalicylaldehyde (H2L2), 4-methoxysalicylaldehyde (H2L3) and 5-methoxysalicylaldehyde (H2L4). The corresponding iron-chloro complexes with the general formula [Fe(Ln)Cl] (n = 1–4 for complexes (1–4)) were characterized by FTIR and UV–Vis spectroscopy and elemental analysis. Crystal structure of (1) was obtained by single-crystal X-ray crystallography. Cyclic voltammetry was used to study the electrochemistry of the complexes. The complexes were used as catalysts for the selective oxidation of organic sulfide compounds to sulfoxides. High catalytic performance and selectivity were obtained. The spectroscopic, electrochemical and catalytic data are discussed based on the electronic, steric and electrochemical properties of the complexes.
ArticleNumber	115135
Author	Amini, Mojtaba Aghvami, Fatemeh Kucerakova, Monika Ghaffari, Abolfazl Dusek, Michal Karimi-Nami, Rahman Behzad, Mahdi
Author_xml	– sequence: 1 givenname: Fatemeh surname: Aghvami fullname: Aghvami, Fatemeh organization: Faculty of Chemistry, Semnan University, Semnan 35351-1911, Iran – sequence: 2 givenname: Abolfazl surname: Ghaffari fullname: Ghaffari, Abolfazl organization: Faculty of Chemistry, Semnan University, Semnan 35351-1911, Iran – sequence: 3 givenname: Monika orcidid: 0000-0001-9797-2559 surname: Kucerakova fullname: Kucerakova, Monika organization: Institute of Physics ASCR, v.v.i, Na Slovance 2, 182 21 Praha 8, Czech Republic – sequence: 4 givenname: Michal surname: Dusek fullname: Dusek, Michal organization: Institute of Physics ASCR, v.v.i, Na Slovance 2, 182 21 Praha 8, Czech Republic – sequence: 5 givenname: Rahman surname: Karimi-Nami fullname: Karimi-Nami, Rahman organization: Department of Chemistry, Faculty of Science, University of Maragheh, Maragheh, Iran – sequence: 6 givenname: Mojtaba surname: Amini fullname: Amini, Mojtaba organization: Department of Chemistry, Faculty of Science, University of Maragheh, Maragheh, Iran – sequence: 7 givenname: Mahdi orcidid: 0000-0001-5957-0778 surname: Behzad fullname: Behzad, Mahdi email: mbehzad@semnan.ac.ir organization: Faculty of Chemistry, Semnan University, Semnan 35351-1911, Iran
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Keywords	Schiff base Catalysis Sulfoxidation Iron-chloro SULFOXIDES FE(III) SELECTIVE OXIDATION COPPER(II) SALEN CRYSTAL
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Snippet	Four new iron-chloro Schiff base complexes were used as catalyst for selective oxidation of sulfides and the results are discussed based on the presence of OMe... Four new Fe(III)-Chloro Schiff base complexes were synthesized and characterized. The N2O2 type tetradentate Schiff base ligands were synthesized from the...
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SubjectTerms	Catalysis Chemistry Chemistry, Inorganic & Nuclear Crystallography Iron-chloro Physical Sciences Schiff base Science & Technology Sulfoxidation
Title	Catalytic oxidation of organic sulfides by new iron-chloro Schiff base complexes: The effect of methoxy substitution and ligand isomerism on the electronic, electrochemical and catalytic performance of the complexes
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