Effect of Metallic Nanocoatings Deposited on Silicon Oxide on Wetting by Filler Melts II. Effect from the Annealing of Nanocoatings Deposited on SiO2 on their Structure and Interaction with the Oxide

The sessile drop method using capillary melt cleaning was employed in the experiment to study the effect of metallic nanocoatings (single Ti, Nb, and Mo coatings and binary Ti–Cu, Nb–Cu, and Mo–Cu coatings with a copper layer of constant thickness) on the wetting of silicon oxide by Pb–15 wt.% In me...

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Vydané v:	Powder metallurgy and metal ceramics Ročník 59; číslo 3-4; s. 134 - 140
Hlavní autori:	Krasovskyy, V.P., Kostyuk, B.D., Gab, I.I., Krasovskaya, N.A., Stetsyuk, T.V.
Médium:	Journal Article
Jazyk:	English
Vydavateľské údaje:	New York Springer US 01.07.2020 Springer Nature B.V
Predmet:	Affinity Aluminum base alloys Annealing Brazing alloys Ceramics Characterization and Evaluation of Materials Chemistry and Materials Science Chromium Coatings Composites Contact angle Copper Dispersion Electron beams Glass Integrity Islands Materials Science Metallic Materials Molybdenum Nanostructured Materials Natural Materials Nickel Niobium Sessile drop method Silicon dioxide Silicon oxides Substrates Surface tension Thickness Titanium Wetting silicon oxide wetting metal nanocoatings annealing coating dispersion
ISSN:	1068-1302, 1573-9066
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Abstract	The sessile drop method using capillary melt cleaning was employed in the experiment to study the effect of metallic nanocoatings (single Ti, Nb, and Mo coatings and binary Ti–Cu, Nb–Cu, and Mo–Cu coatings with a copper layer of constant thickness) on the wetting of silicon oxide by Pb–15 wt.% In melt in 1 ∙ 10 –3 Pa vacuum at 500°C after their annealing at 900°C. The metallic coatings were applied by electron beam evaporation in vacuum. The binary coatings were produced by sequential deposition of layers. The dependences of contact angle on coating thickness show that the ‘threshold’ thickness is determined by the annealing temperature of the coating or, in other words, its structure. The threshold coating thickness for different metals depends on their chemical affinity to oxygen. When freshly applied and annealed single Mo, Nb, and Ti coatings are wetted, their threshold thickness increases from 70 to 80 nm for the titanium coating, from 63 to 70 nm for the niobium coating, and from 50 to 60 nm for the molybdenum coating. The structure of Cu, Ni, Mo, Cr, Nb, and Ti coatings annealed at 600, 900, and 1200°C was studied. The initial (freshly deposited) metallic coatings showed high integrity. The coatings became dispersed after annealing and their integrity decreased with increasing temperature. The dispersed metallic coatings formed ‘islands’ of various shapes, round shape being predominant, depending on the chemical affinity of the coating metal to oxygen. The so-called ‘solid’ wetting was observed. The shape of the islands is determined by equilibrium between the metal–substrate attraction forces (interaction, adhesion) and the very strong surface tension of the metal (at such a small coating thickness). To use metallic coatings for brazing quartz with aluminum alloys, coatings of adhesive metals (Mo, Cr, Nb, Ti) should be annealed at temperatures of 900–1000°C with a holding time of 10 min. The coating thickness should be within the threshold range.
AbstractList	The sessile drop method using capillary melt cleaning was employed in the experiment to study the effect of metallic nanocoatings (single Ti, Nb, and Mo coatings and binary Ti–Cu, Nb–Cu, and Mo–Cu coatings with a copper layer of constant thickness) on the wetting of silicon oxide by Pb–15 wt.% In melt in 1 ∙ 10 –3 Pa vacuum at 500°C after their annealing at 900°C. The metallic coatings were applied by electron beam evaporation in vacuum. The binary coatings were produced by sequential deposition of layers. The dependences of contact angle on coating thickness show that the ‘threshold’ thickness is determined by the annealing temperature of the coating or, in other words, its structure. The threshold coating thickness for different metals depends on their chemical affinity to oxygen. When freshly applied and annealed single Mo, Nb, and Ti coatings are wetted, their threshold thickness increases from 70 to 80 nm for the titanium coating, from 63 to 70 nm for the niobium coating, and from 50 to 60 nm for the molybdenum coating. The structure of Cu, Ni, Mo, Cr, Nb, and Ti coatings annealed at 600, 900, and 1200°C was studied. The initial (freshly deposited) metallic coatings showed high integrity. The coatings became dispersed after annealing and their integrity decreased with increasing temperature. The dispersed metallic coatings formed ‘islands’ of various shapes, round shape being predominant, depending on the chemical affinity of the coating metal to oxygen. The so-called ‘solid’ wetting was observed. The shape of the islands is determined by equilibrium between the metal–substrate attraction forces (interaction, adhesion) and the very strong surface tension of the metal (at such a small coating thickness). To use metallic coatings for brazing quartz with aluminum alloys, coatings of adhesive metals (Mo, Cr, Nb, Ti) should be annealed at temperatures of 900–1000°C with a holding time of 10 min. The coating thickness should be within the threshold range. The sessile drop method using capillary melt cleaning was employed in the experiment to study the effect of metallic nanocoatings (single Ti, Nb, and Mo coatings and binary Ti–Cu, Nb–Cu, and Mo–Cu coatings with a copper layer of constant thickness) on the wetting of silicon oxide by Pb–15 wt.% In melt in 1 ∙ 10–3 Pa vacuum at 500°C after their annealing at 900°C. The metallic coatings were applied by electron beam evaporation in vacuum. The binary coatings were produced by sequential deposition of layers. The dependences of contact angle on coating thickness show that the ‘threshold’ thickness is determined by the annealing temperature of the coating or, in other words, its structure. The threshold coating thickness for different metals depends on their chemical affinity to oxygen. When freshly applied and annealed single Mo, Nb, and Ti coatings are wetted, their threshold thickness increases from 70 to 80 nm for the titanium coating, from 63 to 70 nm for the niobium coating, and from 50 to 60 nm for the molybdenum coating. The structure of Cu, Ni, Mo, Cr, Nb, and Ti coatings annealed at 600, 900, and 1200°C was studied. The initial (freshly deposited) metallic coatings showed high integrity. The coatings became dispersed after annealing and their integrity decreased with increasing temperature. The dispersed metallic coatings formed ‘islands’ of various shapes, round shape being predominant, depending on the chemical affinity of the coating metal to oxygen. The so-called ‘solid’ wetting was observed. The shape of the islands is determined by equilibrium between the metal–substrate attraction forces (interaction, adhesion) and the very strong surface tension of the metal (at such a small coating thickness). To use metallic coatings for brazing quartz with aluminum alloys, coatings of adhesive metals (Mo, Cr, Nb, Ti) should be annealed at temperatures of 900–1000°C with a holding time of 10 min. The coating thickness should be within the threshold range.
Author	Krasovskaya, N.A. Krasovskyy, V.P. Stetsyuk, T.V. Kostyuk, B.D. Gab, I.I.
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References	Naidich, Gab, Stetsyuk, Kostyuk (CR4) 2018; 51 Naidich (CR8) 1981; 14 Shank (CR12) 1970 CR5 CR7 Naidich, Kostyuk, Kolesnichenko, Shaikevich (CR3) 1975 Naidich, Gab, Stetsyuk, Kostyuk (CR10) 2014; 3 Kolesnichenko, Kostyuk, Roshchin (CR6) 1985; 14 Naidich, Gab, Stetsyuk, Kostyuk (CR9) 2018; 40 Naidich, Chuvashov, Ishchuk, Krasovskyy (CR2) 1983; 22 Hansen, Anderko (CR11) 1958 Krasovskyy, Kostyuk, Gab, Krasovskaya, Stetsyuk (CR1) 2020; 59 GA Kolesnichenko (146_CR6) 1985; 14 YV Naidich (146_CR3) 1975 YV Naidich (146_CR4) 2018; 51 F Shank (146_CR12) 1970 YV Naidich (146_CR8) 1981; 14 M Hansen (146_CR11) 1958 146_CR5 YV Naidich (146_CR10) 2014; 3 YV Naidich (146_CR9) 2018; 40 VP Krasovskyy (146_CR1) 2020; 59 146_CR7 YV Naidich (146_CR2) 1983; 22
References_xml	– volume: 40 start-page: 1359 issue: 10 year: 2018 end-page: 1373 ident: CR9 article-title: Dispersion kinetics in vacuum annealing of molybdenum nanocoatings deposited on oxide materials publication-title: Metallofiz. Noveish. Tekhnol. doi: 10.15407/mfint.40.10.1359 – year: 1958 ident: CR11 doi: 10.1149/1.2428700 – volume: 14 start-page: 353 year: 1981 end-page: 484 ident: CR8 article-title: The wettability of solids by liquid metals publication-title: Prog. Surf. Membr. Sci. doi: 10.1016/B978-0-12-571814-1.50011-7 – volume: 59 start-page: 29 issue: 1–2 year: 2020 end-page: 34 ident: CR1 article-title: Effect of metallic nanocoatings deposited on silicon oxide on wetting by filler melts. I. Wetting of Ti, Nb, Cr, V, and Mo nanocoatings deposited on SiO with filler melts publication-title: Powder Metall. Met. Ceram. doi: 10.1007/s11106-020-00135-8 – ident: CR5 – ident: CR7 – year: 1970 ident: CR12 – volume: 22 start-page: 481 issue: 6 year: 1983 end-page: 483 ident: CR2 article-title: Wetting of some nonmetallic materials by aluminum publication-title: Powder Metall. Met. Ceram. doi: 10.1007/BF00793227 – volume: 51 start-page: 54 year: 2018 end-page: 61 ident: CR4 article-title: Dispersion kinetics for chromium nanofilms deposited onto oxide materials in vacuum annealing publication-title: Adhez. Raspl. Paika Mater., Issue – volume: 14 start-page: 55 year: 1985 end-page: 61 ident: CR6 article-title: Interaction of thin Cu, Ge, V, and V–Cu films with quartz and their structure in high-temperature annealing publication-title: Adhez. Raspl. Paika Mater., Issue – start-page: 15 year: 1975 end-page: 27 ident: CR3 publication-title: “Wettability in the metallic melt–thin metallic coating–nonmetallic substrate system,” in: [in Russian] – volume: 3 start-page: 516 year: 2014 end-page: 522 ident: CR10 article-title: Dispersion kinetics in vacuum annealing of chromium and nickel nanocoatings deposited on oxide materials publication-title: Fiz. Khim. Tverd. Tela – volume: 22 start-page: 481 issue: 6 year: 1983 ident: 146_CR2 publication-title: Powder Metall. Met. Ceram. doi: 10.1007/BF00793227 – ident: 146_CR5 – volume: 3 start-page: 516 year: 2014 ident: 146_CR10 publication-title: Fiz. Khim. Tverd. Tela – ident: 146_CR7 – volume: 40 start-page: 1359 issue: 10 year: 2018 ident: 146_CR9 publication-title: Metallofiz. Noveish. Tekhnol. doi: 10.15407/mfint.40.10.1359 – volume-title: Constitution of Binary Alloys year: 1958 ident: 146_CR11 doi: 10.1149/1.2428700 – volume: 14 start-page: 55 year: 1985 ident: 146_CR6 publication-title: Adhez. Raspl. Paika Mater., Issue – start-page: 15 volume-title: “Wettability in the metallic melt–thin metallic coating–nonmetallic substrate system,” in: Physical Chemistry of Condensed Phases, Superhard Materials, and Their Interfaces [in Russian] year: 1975 ident: 146_CR3 – volume: 59 start-page: 29 issue: 1–2 year: 2020 ident: 146_CR1 publication-title: Powder Metall. Met. Ceram. doi: 10.1007/s11106-020-00135-8 – volume-title: Constitution of Binary Alloys year: 1970 ident: 146_CR12 – volume: 14 start-page: 353 year: 1981 ident: 146_CR8 publication-title: Prog. Surf. Membr. Sci. doi: 10.1016/B978-0-12-571814-1.50011-7 – volume: 51 start-page: 54 year: 2018 ident: 146_CR4 publication-title: Adhez. Raspl. Paika Mater., Issue
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SubjectTerms	Affinity Aluminum base alloys Annealing Brazing alloys Ceramics Characterization and Evaluation of Materials Chemistry and Materials Science Chromium Coatings Composites Contact angle Copper Dispersion Electron beams Glass Integrity Islands Materials Science Metallic Materials Molybdenum Nanostructured Materials Natural Materials Nickel Niobium Sessile drop method Silicon dioxide Silicon oxides Substrates Surface tension Thickness Titanium Wetting
Title	Effect of Metallic Nanocoatings Deposited on Silicon Oxide on Wetting by Filler Melts II. Effect from the Annealing of Nanocoatings Deposited on SiO2 on their Structure and Interaction with the Oxide
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