A Simple Sonochemical Synthesis of Nanosized ZnO from Zinc Acetate and Sodium Hydroxide

An efficient sonochemical route for synthesis of nano sized zinc oxide is reported. The method employs zinc acetate and sodium hydroxide as precursors with isopropyl alcohol as a solvent. As prepared powders were characterized by XRD, SEM and FTIR. These show that the resulting powder is composed of...

Ausführliche Beschreibung

Gespeichert in:
Bibliographische Detailangaben
Veröffentlicht in:Journal of Nano- and Electronic Physics Jg. 10; H. 5; S. 5023 - 5023-4
Hauptverfasser: Zakirov, M. I., Semen'ko, M. P., Korotchenkov, O. A.
Format: Journal Article
Sprache:Englisch
Veröffentlicht: Sumy Ukraine Sumy State University, Journal of Nano - and Electronic Physics 2018
Schlagworte:
Caustic soda
Crystallites
Isopropanol
Metal hydroxides
Sodium hydroxide
Synthesis
Wurtzite
Zinc acetate
Zinc oxide
Zinc oxides
ISSN:2077-6772, 2306-4277
Online-Zugang:Volltext
Tags: Tag hinzufügen
Keine Tags, Fügen Sie den ersten Tag hinzu!
Abstract An efficient sonochemical route for synthesis of nano sized zinc oxide is reported. The method employs zinc acetate and sodium hydroxide as precursors with isopropyl alcohol as a solvent. As prepared powders were characterized by XRD, SEM and FTIR. These show that the resulting powder is composed of multi-domain crystallites of ZnO wurtzite, zincite and Zn(OH)2. The XRD-measured coherent domain size varies from about 20 to 30 nm, whereas SEM exhibits 200 nm crystallites. The wurtzite phase is found to dominate at sonication times smaller than 30 min. It is also found that the powders produced sonochemically exhibit smaller and narrower size-distributed particles compared to that in hydrothermally prepared powders.
AbstractList An efficient sonochemical route for synthesis of nano sized zinc oxide is reported. The method employs zinc acetate and sodium hydroxide as precursors with isopropyl alcohol as a solvent. As prepared powders were characterized by XRD, SEM and FTIR. These show that the resulting powder is composed of multi-domain crystallites of ZnO wurtzite, zincite and Zn(OH)2. The XRD-measured coherent domain size varies from about 20 to 30 nm, whereas SEM exhibits 200 nm crystallites. The wurtzite phase is found to dominate at sonication times smaller than 30 min. It is also found that the powders produced sonochemically exhibit smaller and narrower size-distributed particles compared to that in hydrothermally prepared powders.
Author Korotchenkov, O. A.
Zakirov, M. I.
Semen'ko, M. P.
Author_xml – sequence: 1
  givenname: M. I.
  surname: Zakirov
  fullname: Zakirov, M. I.
– sequence: 2
  givenname: M. P.
  surname: Semen'ko
  fullname: Semen'ko, M. P.
– sequence: 3
  givenname: O. A.
  surname: Korotchenkov
  fullname: Korotchenkov, O. A.
BookMark eNotkE9LAzEQxYNUsNZ-AG8BL3rYmj-7SXMsRa1Q7KGK0EtIk1ma0k1qsgXrp3drhQfzHryZgd816oUYAKFbSkaMMsketwH2I0ruq4cRqQjjF6jPOBFFyaTsdZ5IWQgp2RUa5uzXhFLFFBOijz4neOmb_Q7wMoZoN9B4a3Z4eQztBrLPONb4zYSY_Q84vAoLXKfY4JUPFk8stKYFbILrtp0_NHh2dCl-ewc36LI2uwzD_zlAH89P79NZMV-8vE4n88LSMeOFFWNQhFdOEFoaVkFNRa24UbwuhbM1VSAdNUqMqbHKlAYYFdKVYIBYsl7zAbo7392n-HWA3OptPKTQvdSMlZ1UxWnXoueWTTHnBLXeJ9-YdNSU6D-E-oTwlCqt_xDyX8sZZow
ContentType Journal Article
Copyright Copyright Sumy State University, Journal of Nano - and Electronic Physics 2018
Copyright_xml – notice: Copyright Sumy State University, Journal of Nano - and Electronic Physics 2018
CorporateAuthor Faculty of Physics, Taras Shevchenko Kyiv National University, 01601 Kyiv, Ukraine
CorporateAuthor_xml – name: Faculty of Physics, Taras Shevchenko Kyiv National University, 01601 Kyiv, Ukraine
DBID AAYXX
CITATION
7SP
7SR
7U5
8BQ
8FD
8FE
8FG
AFKRA
ARAPS
BENPR
BGLVJ
CCPQU
DWQXO
HCIFZ
JG9
L7M
P5Z
P62
PHGZM
PHGZT
PKEHL
PQEST
PQGLB
PQQKQ
PQUKI
PRINS
DOI 10.21272/jnep.10(5).05023
DatabaseName CrossRef
Electronics & Communications Abstracts
Engineered Materials Abstracts
Solid State and Superconductivity Abstracts
METADEX
Technology Research Database
ProQuest SciTech Collection
ProQuest Technology Collection
ProQuest Central UK/Ireland
Advanced Technologies & Computer Science Collection
ProQuest Central
ProQuest Technology Collection
ProQuest One Community College
ProQuest Central Korea
SciTech Premium Collection
Materials Research Database
Advanced Technologies Database with Aerospace
Advanced Technologies & Aerospace Database
ProQuest Advanced Technologies & Aerospace Collection
ProQuest Central Premium
ProQuest One Academic (New)
ProQuest One Academic Middle East (New)
ProQuest One Academic Eastern Edition (DO NOT USE)
ProQuest One Applied & Life Sciences
ProQuest One Academic (retired)
ProQuest One Academic UKI Edition
ProQuest Central China
DatabaseTitle CrossRef
Materials Research Database
Technology Collection
Technology Research Database
ProQuest One Academic Middle East (New)
ProQuest Advanced Technologies & Aerospace Collection
SciTech Premium Collection
ProQuest One Community College
ProQuest Central China
ProQuest Central
ProQuest One Applied & Life Sciences
Engineered Materials Abstracts
ProQuest Central Korea
ProQuest Central (New)
Advanced Technologies Database with Aerospace
Advanced Technologies & Aerospace Collection
ProQuest One Academic Eastern Edition
Electronics & Communications Abstracts
ProQuest Technology Collection
ProQuest SciTech Collection
METADEX
Advanced Technologies & Aerospace Database
ProQuest One Academic UKI Edition
Solid State and Superconductivity Abstracts
ProQuest One Academic
ProQuest One Academic (New)
DatabaseTitleList Materials Research Database
Database_xml – sequence: 1
  dbid: BENPR
  name: ProQuest Central
  url: https://www.proquest.com/central
  sourceTypes: Aggregation Database
DeliveryMethod fulltext_linktorsrc
EISSN 2306-4277
EndPage 5023-4
ExternalDocumentID 10_21272_jnep_10_5__05023
GroupedDBID 9MQ
AAYXX
ALMA_UNASSIGNED_HOLDINGS
CITATION
7SP
7SR
7U5
8BQ
8FD
8FE
8FG
AFKRA
ARAPS
BENPR
BGLVJ
CCPQU
DWQXO
HCIFZ
JG9
L7M
P62
PHGZM
PHGZT
PKEHL
PQEST
PQGLB
PQQKQ
PQUKI
PRINS
ID FETCH-LOGICAL-c1823-c68e9035d6014a25ef16f93a93f46dcf19e7d1a9681ac9a4ae2167d4eae0c0bb3
IEDL.DBID BENPR
ISSN 2077-6772
IngestDate Sun Nov 09 05:50:15 EST 2025
Sat Nov 29 04:54:46 EST 2025
IsDoiOpenAccess false
IsOpenAccess true
IsPeerReviewed true
IsScholarly true
Issue 5
Language English
LinkModel DirectLink
MergedId FETCHMERGED-LOGICAL-c1823-c68e9035d6014a25ef16f93a93f46dcf19e7d1a9681ac9a4ae2167d4eae0c0bb3
Notes ObjectType-Article-1
SourceType-Scholarly Journals-1
ObjectType-Feature-2
content type line 14
OpenAccessLink https://doi.org/10.21272/jnep.10(5).05023
PQID 2242249531
PQPubID 2032533
ParticipantIDs proquest_journals_2242249531
crossref_primary_10_21272_jnep_10_5__05023
PublicationCentury 2000
PublicationDate 2018-00-00
20180101
PublicationDateYYYYMMDD 2018-01-01
PublicationDate_xml – year: 2018
  text: 2018-00-00
PublicationDecade 2010
PublicationPlace Sumy Ukraine
PublicationPlace_xml – name: Sumy Ukraine
PublicationTitle Journal of Nano- and Electronic Physics
PublicationYear 2018
Publisher Sumy State University, Journal of Nano - and Electronic Physics
Publisher_xml – name: Sumy State University, Journal of Nano - and Electronic Physics
SSID ssib011929266
ssib017388558
ssib061739424
ssib058969622
Score 2.1929293
Snippet An efficient sonochemical route for synthesis of nano sized zinc oxide is reported. The method employs zinc acetate and sodium hydroxide as precursors with...
SourceID proquest
crossref
SourceType Aggregation Database
Index Database
StartPage 5023
SubjectTerms Caustic soda
Crystallites
Isopropanol
Metal hydroxides
Sodium hydroxide
Synthesis
Wurtzite
Zinc acetate
Zinc oxide
Zinc oxides
Title A Simple Sonochemical Synthesis of Nanosized ZnO from Zinc Acetate and Sodium Hydroxide
URI https://www.proquest.com/docview/2242249531
Volume 10
hasFullText 1
inHoldings 1
isFullTextHit
isPrint
journalDatabaseRights – providerCode: PRVHPJ
  databaseName: ROAD: Directory of Open Access Scholarly Resources
  customDbUrl:
  eissn: 2306-4277
  dateEnd: 99991231
  omitProxy: false
  ssIdentifier: ssib058969622
  issn: 2077-6772
  databaseCode: M~E
  dateStart: 20120101
  isFulltext: true
  titleUrlDefault: https://road.issn.org
  providerName: ISSN International Centre
link http://cvtisr.summon.serialssolutions.com/2.0.0/link/0/eLvHCXMwpV1NT9swGLagcODCQDBRPiofOIxJHrGdOPYJFVTEZaVaNw31Ern-kIJEUhqK1h3223mdpOq47LJLpCTKIe_z5v2y8zwInStlqTRKEaG1ILH0nmhDJfFUeA8JyCeyEZtIh0P58KBG7cCtardVrmJiHahtacKM_BJSDQs6yZxezZ5JUI0Kq6uthMYm2gpMZXEHbV0PhqNvK4-Ca0yxdcFCUy7lXwRXiQzkMGsCO0jnXMW1Ei6L0pQIqD2bpdBAhM4uHws3g373U3LxJUoixt8ns_exvE5Qtx_-99X20G5bmuJ-40v7aGO-OEA_-3icBwZhPC6LoK5V0wvg8bKAyrHKK1x6DBG6rPLfzuJJcY_DDyt4khcG903Yy-iwLiw8bfPFE75b2nn5K7fuEP24HXy_uSOtGAMB6BgnRkinIp5Y6OBizRIX0FRcK-5jYQ3g6lJLtRKSaqN0rB2jIrWx0y4y0XTKP6JOURbuCGHLIgt9GniIj2KaBoJnL7iFSsb7dKpcF31eWTWbNZwbGfQqNQRZgCCcJVlWQ9BFpyujZu3nV2Vrix7_-_YJ2oEKSDYzlVPUeZkv3BnaNq8veTXvtd7UQ5tf_wzgOEombwbP0GY
linkProvider ProQuest
linkToHtml http://cvtisr.summon.serialssolutions.com/2.0.0/link/0/eLvHCXMw1V3LbtQwFLVKQaIbHgJEaSlegARIpvEjjr2oqhFQTdUyVJoiqtkEjx9SKpFMJx3a6Uf1G3udTDR0w64LllGUyMm59j3Xj3MQequ1o8pqTaQxkggVAjGWKhKoDAESUEhVazaRDQbq5EQfraDr7ixM3FbZjYnNQO0qG-fItyHVsOiTzOnu5IxE16i4utpZaLRhceDnF1Cy1Tv7XwDfd4ztfT3-3CcLVwECbWCcWKm8TnjqoBQRhqU-Nktzo3kQ0llooM8cNVoqaqw2wnhGZeaENz6xyXjM4b330H0hoFiC_nOUjrr4pcCWNFvSI5pxpf6S00pVlKJZyuUBeeBaNL67LMkyIoHptguvUXadbZ-WfgLV9fv0w6ckTRi_nTpvZ44mHe49_t9-5BP0aEG8ca_tKU_RynT2DP3s4WER9ZHxsCqjd1gjnoCH8xJ4cV3UuAoY8k9VF1fe4VH5HcfjOHhUlBb3bNyp6bEpHTztitlv3J-7aXVZOP8c_biTb3mBVsuq9C8RdixxUIVC_IdE0CzKVwfJHfC0ELKx9uvoY4diPmkVRXKoxBrI8wh5vErzvIF8HW12IOaLwaXOlwi--vftN-hh__jbYX64PzjYQGvA9VQ7e7SJVs-nM_8aPbB_zot6utXEMUa_7hrvG-J5KoQ
openUrl ctx_ver=Z39.88-2004&ctx_enc=info%3Aofi%2Fenc%3AUTF-8&rfr_id=info%3Asid%2Fsummon.serialssolutions.com&rft_val_fmt=info%3Aofi%2Ffmt%3Akev%3Amtx%3Ajournal&rft.genre=article&rft.atitle=A+Simple+Sonochemical+Synthesis+of+Nanosized+ZnO+from+Zinc+Acetate+and+Sodium+Hydroxide&rft.jtitle=Journal+of+Nano-+and+Electronic+Physics&rft.au=Zakirov%2C+M.+I.&rft.au=Semen%27ko%2C+M.+P.&rft.au=Korotchenkov%2C+O.+A.&rft.date=2018&rft.issn=2077-6772&rft.eissn=2306-4277&rft.volume=10&rft.issue=5&rft.spage=5023&rft.epage=5023-4&rft_id=info:doi/10.21272%2Fjnep.10%285%29.05023&rft.externalDBID=n%2Fa&rft.externalDocID=10_21272_jnep_10_5__05023
thumbnail_l http://covers-cdn.summon.serialssolutions.com/index.aspx?isbn=/lc.gif&issn=2077-6772&client=summon
thumbnail_m http://covers-cdn.summon.serialssolutions.com/index.aspx?isbn=/mc.gif&issn=2077-6772&client=summon
thumbnail_s http://covers-cdn.summon.serialssolutions.com/index.aspx?isbn=/sc.gif&issn=2077-6772&client=summon