Effects of Inorganic Fillers on the Thermal and Mechanical Properties of Poly(lactic acid)
Addition of filler to polylactic acid (PLA) may affect its crystallization behavior and mechanical properties. The effects of talc and hydroxyapatite (HA) on the thermal and mechanical properties of two types of PLA (one amorphous and one semicrystalline) have been investigated. The composites were...
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| Vydáno v: | International Journal of Polymer Science Ročník 2014; číslo 2; s. 129 - 136 |
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| Hlavní autoři: | , , , , |
| Médium: | Journal Article |
| Jazyk: | angličtina |
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Cairo, Egypt
Hindawi Limiteds
01.01.2014
Hindawi Publishing Corporation John Wiley & Sons, Inc Wiley |
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| ISSN: | 1687-9422, 1687-9430 |
| On-line přístup: | Získat plný text |
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| Abstract | Addition of filler to polylactic acid (PLA) may affect its crystallization behavior and mechanical properties. The effects of talc and hydroxyapatite (HA) on the thermal and mechanical properties of two types of PLA (one amorphous and one semicrystalline) have been investigated. The composites were prepared by melt blending followed by injection molding. The molecular weight, morphology, mechanical properties, and thermal properties have been characterized by gel permeation chromatography (GPC), scanning electron microscope (SEM), instron tensile tester, thermogravimetric analysis (TGA), differential scanning calorimetry (DSC), and dynamic mechanical analysis (DMA). It was found that the melting blending led to homogeneous distribution of the inorganic filler within the PLA matrix but decreased the molecular weight of PLA. Regarding the filler, addition of talc increased the crystallinity of PLA, but HA decreased the crystallinity of PLA. The tensile strength of the composites depended on the crystallinity of PLA and the interfacial properties between PLA and the filler, but both talc and HA filler increased the toughness of PLA. |
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| AbstractList | Addition of filler to polylactic acid (PLA) may affect its crystallization behavior and mechanical properties. The effects of talc and hydroxyapatite (HA) on the thermal and mechanical properties of two types of PLA (one amorphous and one semicrystalline) have been investigated. The composites were prepared by melt blending followed by injection molding. The molecular weight, morphology, mechanical properties, and thermal properties have been characterized by gel permeation chromatography (GPC), scanning electron microscope (SEM), instron tensile tester, thermogravimetric analysis (TGA), differential scanning calorimetry (DSC), and dynamic mechanical analysis (DMA). It was found that the melting blending led to homogeneous distribution of the inorganic filler within the PLA matrix but decreased the molecular weight of PLA. Regarding the filler, addition of talc increased the crystallinity of PLA, but HA decreased the crystallinity of PLA. The tensile strength of the composites depended on the crystallinity of PLA and the interfacial properties between PLA and the filler, but both talc and HA filler increased the toughness of PLA. Addition of filler to polylactic acid (PLA) may affect its crystallization behavior and mechanical properties. The effects of talc and hydroxyapatite (HA) on the thermal and mechanical properties of two types of PLA (one amorphous and one semicrystalline) have been investigated. The composites were prepared by melt blending followed by injection molding. The molecular weight, morphology, mechanical properties, and thermal properties have been characterized by gel permeation chromatography (GPC), scanning electron microscope (SEM), instron tensile tester, thermogravimetric analysis (TGA), differential scanning calorimetry (DSC), and dynamic mechanical analysis (DMA). It was found that the melting blending led to homogeneous distribution of the inorganic filler within the PLA matrix but decreased the molecular weight of PLA. Regarding the filler, addition of talc increased the crystallinity of PLA, but HA decreased the crystallinity of PLA. The tensile strength of the composites depended on the crystallinity of PLA and the interfacial properties between PLA and the filler, but both talc and HA filler increased the toughness of PLA.Addition of filler to polylactic acid (PLA) may affect its crystallization behavior and mechanical properties. The effects of talc and hydroxyapatite (HA) on the thermal and mechanical properties of two types of PLA (one amorphous and one semicrystalline) have been investigated. The composites were prepared by melt blending followed by injection molding. The molecular weight, morphology, mechanical properties, and thermal properties have been characterized by gel permeation chromatography (GPC), scanning electron microscope (SEM), instron tensile tester, thermogravimetric analysis (TGA), differential scanning calorimetry (DSC), and dynamic mechanical analysis (DMA). It was found that the melting blending led to homogeneous distribution of the inorganic filler within the PLA matrix but decreased the molecular weight of PLA. Regarding the filler, addition of talc increased the crystallinity of PLA, but HA decreased the crystallinity of PLA. The tensile strength of the composites depended on the crystallinity of PLA and the interfacial properties between PLA and the filler, but both talc and HA filler increased the toughness of PLA. |
| Audience | Academic |
| Author | Liu, Xingxun Mitchell, James W. Chow, Laurence C. Yang, Mingshu Wang, Tongxin |
| AuthorAffiliation | 2 Crest Center for Nanomaterials, College of Engineering, Howard University, Washington, DC 20059, USA 1 College of Dentistry, Howard University, Washington, DC 20059, USA 4 CAS Key Laboratory of Engineering Plastics, Institute of Chemistry, Chinese Academy of Sciences, Beijing 100190, China 3 American Dental Association Foundation, Dr. Anthony Volpe Research Center, National Institute of Standards and Technology, Gaithersburg, MD 20899, USA |
| AuthorAffiliation_xml | – name: 2 Crest Center for Nanomaterials, College of Engineering, Howard University, Washington, DC 20059, USA – name: 1 College of Dentistry, Howard University, Washington, DC 20059, USA – name: 4 CAS Key Laboratory of Engineering Plastics, Institute of Chemistry, Chinese Academy of Sciences, Beijing 100190, China – name: 3 American Dental Association Foundation, Dr. Anthony Volpe Research Center, National Institute of Standards and Technology, Gaithersburg, MD 20899, USA |
| Author_xml | – sequence: 1 fullname: Yang, Mingshu – sequence: 2 fullname: Chow, Laurence C. – sequence: 3 fullname: Wang, Tongxin – sequence: 4 fullname: Liu, Xingxun – sequence: 5 fullname: Mitchell, James W. |
| BackLink | https://www.ncbi.nlm.nih.gov/pubmed/25717339$$D View this record in MEDLINE/PubMed |
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| ContentType | Journal Article |
| Copyright | Copyright © 2014 Xingxun Liu et al. COPYRIGHT 2014 John Wiley & Sons, Inc. Copyright © 2014 Xingxun Liu et al. Xingxun Liu et al. This is an open access article distributed under the Creative Commons Attribution License, which permits unrestricted use, distribution, and reproduction in any medium, provided the original work is properly cited. Copyright © 2014 Xingxun Liu et al. 2014 |
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| Snippet | Addition of filler to polylactic acid (PLA) may affect its crystallization behavior and mechanical properties. The effects of talc and hydroxyapatite (HA) on... |
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| SubjectTerms | Annealing Colleges & universities Crystallinity Crystallization Differential scanning calorimetry Fillers Hydroxyapatite Mechanical properties Methods Molecular weight Phase transitions Polyesters Polylactic acid Scanning electron microscopy Talcs Tensile strength Thermal properties |
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| Title | Effects of Inorganic Fillers on the Thermal and Mechanical Properties of Poly(lactic acid) |
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