Water sorption on coal: effects of oxygen-containing function groups and pore structure

Coal-water interactions have profound influences on gas extraction from coal and coal utilization. Experimental measurements on three coals using X-ray photoelectron spectroscopy (XPS), low-temperature nitrogen adsorption and dynamic water vapor sorption (DVS) were conducted. A mechanism-based isoth...

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Published in:International journal of coal science & technology Vol. 8; no. 5; pp. 983 - 1002
Main Authors: Liu, Ang, Liu, Shimin, Liu, Peng, Wang, Kai
Format: Journal Article
Language:English
Published: Singapore Springer Singapore 01.10.2021
Springer
Springer Nature B.V
Subjects:
Adsorption
Analysis
Coal
Energy
Fossil Fuels (incl. Carbon Capture)
Geotechnical Engineering & Applied Earth Sciences
Heat
High temperature
Humidity
Isotherms
Latent heat
Low temperature
Mineral Resources
Relative humidity
Research Article
Sorption
Water vapor
X-ray spectroscopy
China
Isotherm
Pore collapse
Isosteric heat of adsorption
Water vapor
Surface oxidation
ISSN:2095-8293, 2198-7823
Online Access:Get full text
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Abstract Coal-water interactions have profound influences on gas extraction from coal and coal utilization. Experimental measurements on three coals using X-ray photoelectron spectroscopy (XPS), low-temperature nitrogen adsorption and dynamic water vapor sorption (DVS) were conducted. A mechanism-based isotherm model was proposed to estimate the water vapor uptake at various relative humidities, which is well validated with the DVS data. The validated isotherm model of sorption was further used to derive the isosteric heat of water vapor sorption. The specific surface area of coal pores is not the determining parameter that controls water vapor sorption at least during the primary adsorption stage. Oxidation degree dominates the primary adsorption, and which togethering with the cumulative pore volume determine the secondary adsorption. Higher temperature has limited effects on primary adsorption process.The isosteric heat of water adsorption decreases as water vapor uptake increases, which is found to be close to the latent heat of bulk water condensation at higher relative humidity. The results confirmed that the primary adsorption is controlled by the stronger bonding energy while the interaction energy between water molecules during secondary adsorption stage is relatively weak. However, the thermodynamics of coal-water interactions are complicated since the internal bonding interactions within the coal are disrupted at the same time as new bonding interactions take place within water molecules. Coal has a shrinkage/swelling colloidal structure with moisture loss/gain and it may exhibit collapse behavior with some collapses irreversible as a function of relative humidity, which further plays a significant role in determining moisture retention.
AbstractList Coal-water interactions have profound influences on gas extraction from coal and coal utilization. Experimental measurements on three coals using X-ray photoelectron spectroscopy (XPS), low-temperature nitrogen adsorption and dynamic water vapor sorption (DVS) were conducted. A mechanism-based isotherm model was proposed to estimate the water vapor uptake at various relative humidities, which is well validated with the DVS data. The validated isotherm model of sorption was further used to derive the isosteric heat of water vapor sorption. The specific surface area of coal pores is not the determining parameter that controls water vapor sorption at least during the primary adsorption stage. Oxidation degree dominates the primary adsorption, and which togethering with the cumulative pore volume determine the secondary adsorption. Higher temperature has limited effects on primary adsorption process.The isosteric heat of water adsorption decreases as water vapor uptake increases, which is found to be close to the latent heat of bulk water condensation at higher relative humidity. The results confirmed that the primary adsorption is controlled by the stronger bonding energy while the interaction energy between water molecules during secondary adsorption stage is relatively weak. However, the thermodynamics of coal-water interactions are complicated since the internal bonding interactions within the coal are disrupted at the same time as new bonding interactions take place within water molecules. Coal has a shrinkage/swelling colloidal structure with moisture loss/gain and it may exhibit collapse behavior with some collapses irreversible as a function of relative humidity, which further plays a significant role in determining moisture retention.
Audience Academic
Author Liu, Shimin
Liu, Peng
Liu, Ang
Wang, Kai
Author_xml – sequence: 1
  givenname: Ang
  surname: Liu
  fullname: Liu, Ang
  organization: Department of Energy and Mineral Engineering, G3 Center and Energy Institute, The Pennsylvania State University
– sequence: 2
  givenname: Shimin
  orcidid: 0000-0001-9612-0047
  surname: Liu
  fullname: Liu, Shimin
  email: szl3@psu.edu
  organization: Department of Energy and Mineral Engineering, G3 Center and Energy Institute, The Pennsylvania State University
– sequence: 3
  givenname: Peng
  surname: Liu
  fullname: Liu, Peng
  organization: State Key Laboratory of Coal Mine Disaster Dynamics and Control, Chongqing University
– sequence: 4
  givenname: Kai
  surname: Wang
  fullname: Wang, Kai
  organization: School of Emergency Management and Safety Engineering, China University of Mining and Technology (Beijing)
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Pore collapse
Isosteric heat of adsorption
Water vapor
Surface oxidation
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Snippet Coal-water interactions have profound influences on gas extraction from coal and coal utilization. Experimental measurements on three coals using X-ray...
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SubjectTerms Adsorption
Analysis
Coal
Energy
Fossil Fuels (incl. Carbon Capture)
Geotechnical Engineering & Applied Earth Sciences
Heat
High temperature
Humidity
Isotherms
Latent heat
Low temperature
Mineral Resources
Relative humidity
Research Article
Sorption
Water vapor
X-ray spectroscopy
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Title Water sorption on coal: effects of oxygen-containing function groups and pore structure
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