Trace element geochemistry of sphalerite in contrasting hydrothermal fluid systems of the Freiberg district, Germany: insights from LA-ICP-MS analysis, near-infrared light microthermometry of sphalerite-hosted fluid inclusions, and sulfur isotope geochemistry

The historic silver mining district of Freiberg (Germany) comprises hydrothermal vein-style mineralization of Permian and Cretaceous age. We compare sphalerite compositions with associated ore-forming fluids and constrain the behavior of critical metals such as In, Ge, and Ga in contrasting hydrothe...

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Vydáno v:Mineralium deposita Ročník 54; číslo 2; s. 237 - 262
Hlavní autoři: Bauer, Matthias E., Burisch, Mathias, Ostendorf, Jörg, Krause, Joachim, Frenzel, Max, Seifert, Thomas, Gutzmer, Jens
Médium: Journal Article
Jazyk:angličtina
Vydáno: Berlin/Heidelberg Springer Berlin Heidelberg 01.02.2019
Springer Nature B.V
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ISSN:0026-4598, 1432-1866
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Abstract The historic silver mining district of Freiberg (Germany) comprises hydrothermal vein-style mineralization of Permian and Cretaceous age. We compare sphalerite compositions with associated ore-forming fluids and constrain the behavior of critical metals such as In, Ge, and Ga in contrasting hydrothermal environments. Fluid inclusion studies reveal that the Permian veins formed due to boiling and cooling of a low-salinity (0 to 6% eq. w [NaCl]) magmatic-hydrothermal fluid at 350 to 230 °C. In contrast, Cretaceous veins formed by mixing of highly saline (17 to 24% eq. w [NaCl + CaCl 2 ] and variable Na/(Na + Ca) ratios) brines at low temperatures (~ 120 °C). Sulfides of the Permian ore stage have a narrow range of δ 34 S VCDT from − 2.3 to + 0.9‰, while the sulfides of the Cretaceous stage have a large scatter and significantly more negative δ 34 S VCDT values (− 30.9 to − 5.5‰), supporting the different nature of the hydrothermal systems. Contrasting fluid systems and ore-forming mechanisms correspond to markedly different trace element systematics in sphalerite. Permian sphalerite is significantly enriched in In (up to 2500 μg/g In) relative to two sphalerite generations of Cretaceous veins. The latter have higher Ge (up to 2700 μg/g Ge) and Ga (up to 1000 μg/g Ga) concentrations. The observed trace element systematics of different sphalerite generations imply that In is enriched in high-temperature, low- to intermediate-salinity fluids with a significant magmatic-hydrothermal fluid component, while Ge and Ga are more concentrated in low-temperature, high-salinity crustal fluids with no obvious magmatic-hydrothermal affiliation.
AbstractList The historic silver mining district of Freiberg (Germany) comprises hydrothermal vein-style mineralization of Permian and Cretaceous age. We compare sphalerite compositions with associated ore-forming fluids and constrain the behavior of critical metals such as In, Ge, and Ga in contrasting hydrothermal environments. Fluid inclusion studies reveal that the Permian veins formed due to boiling and cooling of a low-salinity (0 to 6% eq. w[NaCl]) magmatic-hydrothermal fluid at 350 to 230 °C. In contrast, Cretaceous veins formed by mixing of highly saline (17 to 24% eq. w[NaCl + CaCl2] and variable Na/(Na + Ca) ratios) brines at low temperatures (~ 120 °C). Sulfides of the Permian ore stage have a narrow range of δ34SVCDT from − 2.3 to + 0.9‰, while the sulfides of the Cretaceous stage have a large scatter and significantly more negative δ34SVCDT values (− 30.9 to − 5.5‰), supporting the different nature of the hydrothermal systems. Contrasting fluid systems and ore-forming mechanisms correspond to markedly different trace element systematics in sphalerite. Permian sphalerite is significantly enriched in In (up to 2500 μg/g In) relative to two sphalerite generations of Cretaceous veins. The latter have higher Ge (up to 2700 μg/g Ge) and Ga (up to 1000 μg/g Ga) concentrations. The observed trace element systematics of different sphalerite generations imply that In is enriched in high-temperature, low- to intermediate-salinity fluids with a significant magmatic-hydrothermal fluid component, while Ge and Ga are more concentrated in low-temperature, high-salinity crustal fluids with no obvious magmatic-hydrothermal affiliation.
The historic silver mining district of Freiberg (Germany) comprises hydrothermal vein-style mineralization of Permian and Cretaceous age. We compare sphalerite compositions with associated ore-forming fluids and constrain the behavior of critical metals such as In, Ge, and Ga in contrasting hydrothermal environments. Fluid inclusion studies reveal that the Permian veins formed due to boiling and cooling of a low-salinity (0 to 6% eq. w [NaCl]) magmatic-hydrothermal fluid at 350 to 230 °C. In contrast, Cretaceous veins formed by mixing of highly saline (17 to 24% eq. w [NaCl + CaCl 2 ] and variable Na/(Na + Ca) ratios) brines at low temperatures (~ 120 °C). Sulfides of the Permian ore stage have a narrow range of δ 34 S VCDT from − 2.3 to + 0.9‰, while the sulfides of the Cretaceous stage have a large scatter and significantly more negative δ 34 S VCDT values (− 30.9 to − 5.5‰), supporting the different nature of the hydrothermal systems. Contrasting fluid systems and ore-forming mechanisms correspond to markedly different trace element systematics in sphalerite. Permian sphalerite is significantly enriched in In (up to 2500 μg/g In) relative to two sphalerite generations of Cretaceous veins. The latter have higher Ge (up to 2700 μg/g Ge) and Ga (up to 1000 μg/g Ga) concentrations. The observed trace element systematics of different sphalerite generations imply that In is enriched in high-temperature, low- to intermediate-salinity fluids with a significant magmatic-hydrothermal fluid component, while Ge and Ga are more concentrated in low-temperature, high-salinity crustal fluids with no obvious magmatic-hydrothermal affiliation.
Author Bauer, Matthias E.
Ostendorf, Jörg
Krause, Joachim
Gutzmer, Jens
Seifert, Thomas
Burisch, Mathias
Frenzel, Max
Author_xml – sequence: 1
  givenname: Matthias E.
  orcidid: 0000-0002-3363-2333
  surname: Bauer
  fullname: Bauer, Matthias E.
  email: matthias.bauer@mineral.tu-freiberg.de
  organization: Institut für Mineralogie, Technische Universität Bergakademie Freiberg
– sequence: 2
  givenname: Mathias
  surname: Burisch
  fullname: Burisch, Mathias
  email: mathias.burisch@mineral.tu-freiberg.de
  organization: Institut für Mineralogie, Technische Universität Bergakademie Freiberg
– sequence: 3
  givenname: Jörg
  surname: Ostendorf
  fullname: Ostendorf, Jörg
  organization: Institut für Mineralogie, Technische Universität Bergakademie Freiberg
– sequence: 4
  givenname: Joachim
  surname: Krause
  fullname: Krause, Joachim
  organization: Helmholtz-Zentrum Dresden-Rossendorf, Helmholtz Institute Freiberg for Resource Technology
– sequence: 5
  givenname: Max
  surname: Frenzel
  fullname: Frenzel, Max
  organization: Institut für Mineralogie, Technische Universität Bergakademie Freiberg, Helmholtz-Zentrum Dresden-Rossendorf, Helmholtz Institute Freiberg for Resource Technology
– sequence: 6
  givenname: Thomas
  surname: Seifert
  fullname: Seifert, Thomas
  organization: Institut für Mineralogie, Technische Universität Bergakademie Freiberg
– sequence: 7
  givenname: Jens
  surname: Gutzmer
  fullname: Gutzmer, Jens
  organization: Institut für Mineralogie, Technische Universität Bergakademie Freiberg, Helmholtz-Zentrum Dresden-Rossendorf, Helmholtz Institute Freiberg for Resource Technology
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Mineralium Deposita is a copyright of Springer, (2018). All Rights Reserved.
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Issue 2
Keywords Sphalerite
Gallium
Critical metals
Erzgebirge
Germanium
LA-ICP-MS
Sulfur isotopes
Indium
Near-infrared light microthermometry
Geothermometer
EPMA
Fluid inclusions
Language English
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springer_journals_10_1007_s00126_018_0850_0
PublicationCentury 2000
PublicationDate 2019-02-01
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  year: 2019
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  day: 01
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PublicationPlace Berlin/Heidelberg
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PublicationSubtitle International Journal for Geology, Mineralogy and Geochemistry of Mineral Deposits
PublicationTitle Mineralium deposita
PublicationTitleAbbrev Miner Deposita
PublicationYear 2019
Publisher Springer Berlin Heidelberg
Springer Nature B.V
Publisher_xml – name: Springer Berlin Heidelberg
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Snippet The historic silver mining district of Freiberg (Germany) comprises hydrothermal vein-style mineralization of Permian and Cretaceous age. We compare sphalerite...
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StartPage 237
SubjectTerms Brines
Calcium chloride
Concentrates (ores)
Cretaceous
Earth and Environmental Science
Earth Sciences
Fluid inclusions
Fluids
Gallium
Geochemistry
Geology
Germanium
Heavy metals
High temperature
Historical metallurgy
Hydrothermal systems
Infrared analysis
Isotopes
Low temperature
Metals
Mineral Resources
Mineralization
Mineralogy
Permian
Ratios
Salinity
Salinity effects
Silver
Sodium chloride
Sphalerite
Sulfides
Sulfur
Sulfur isotopes
Sulphur
Systematics
Temperature
Trace elements
Trace metals
Veins (geology)
Zincblende
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Title Trace element geochemistry of sphalerite in contrasting hydrothermal fluid systems of the Freiberg district, Germany: insights from LA-ICP-MS analysis, near-infrared light microthermometry of sphalerite-hosted fluid inclusions, and sulfur isotope geochemistry
URI https://link.springer.com/article/10.1007/s00126-018-0850-0
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Volume 54
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