Sub‑4 nm Nanodiamonds from Graphene-Oxide and Nitrated Polycyclic Aromatic Hydrocarbons at 423 K

Nanodiamonds are interesting materials from the point of view of their biocompatibility and their chemical, spectroscopic, and mechanical properties. Current synthetic methods for nanodiamonds involve harsh environments, which are potentially hazardous in addition to being expensive. We report a low...

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Vydané v:ACS nano Ročník 15; číslo 11; s. 17392 - 17400
Hlavní autori: Shen, Yuting, Su, Shi, Zhao, Wen, Cheng, Shaobo, Xu, Tao, Yin, Kuibo, Chen, Linjiang, He, Longbing, Zhou, Yilong, Bi, Hengchang, Wan, Shu, Zhang, Qiubo, Wang, Liang, Ni, Zhenhua, Banhart, Florian, Botton, Gianluigi A, Ding, Feng, Ruoff, Rodney S, Sun, Litao
Médium: Journal Article
Jazyk:English
Vydavateľské údaje: American Chemical Society 23.11.2021
Predmet:
nitrated-PAHs
nanodiamond
low-temperature
hydrothermal treatment
HRTEM
ISSN:1936-0851, 1936-086X, 1936-086X
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Abstract Nanodiamonds are interesting materials from the point of view of their biocompatibility and their chemical, spectroscopic, and mechanical properties. Current synthetic methods for nanodiamonds involve harsh environments, which are potentially hazardous in addition to being expensive. We report a low-temperature (423 K) hydrothermal approach to form nanodiamonds by using graphene-oxide or nitrated polycyclic aromatic hydrocarbons (naphthalene, anthracene, phenanthrene, or pyrene) as a starting material. The reaction products contain single-crystalline or twinned nanodiamonds with average diameters in the 2–3 nm range. Theoretical calculations prove that, at the nanoscale, sub-4 nm nanodiamonds may adopt a structure that is more stable than graphene-oxide and nitrated polycyclic aromatic hydrocarbons. Our findings show that sp 2 carbon in the polycyclic aromatic precursor can be converted to sp 3 carbon under unexpectedly moderate temperature conditions by using nanoscale precursors and thus offer a low-temperature approach for the synthesis of sub-4 nm nanodiamonds.
AbstractList Nanodiamonds are interesting materials from the point of view of their biocompatibility and their chemical, spectroscopic, and mechanical properties. Current synthetic methods for nanodiamonds involve harsh environments, which are potentially hazardous in addition to being expensive. We report a low-temperature (423 K) hydrothermal approach to form nanodiamonds by using graphene-oxide or nitrated polycyclic aromatic hydrocarbons (naphthalene, anthracene, phenanthrene, or pyrene) as a starting material. The reaction products contain single-crystalline or twinned nanodiamonds with average diameters in the 2–3 nm range. Theoretical calculations prove that, at the nanoscale, sub-4 nm nanodiamonds may adopt a structure that is more stable than graphene-oxide and nitrated polycyclic aromatic hydrocarbons. Our findings show that sp 2 carbon in the polycyclic aromatic precursor can be converted to sp 3 carbon under unexpectedly moderate temperature conditions by using nanoscale precursors and thus offer a low-temperature approach for the synthesis of sub-4 nm nanodiamonds.
Nanodiamonds are interesting materials from the point of view of their biocompatibility and their chemical, spectroscopic, and mechanical properties. Current synthetic methods for nanodiamonds involve harsh environments, which are potentially hazardous in addition to being expensive. We report a low-temperature (423 K) hydrothermal approach to form nanodiamonds by using graphene-oxide or nitrated polycyclic aromatic hydrocarbons (naphthalene, anthracene, phenanthrene, or pyrene) as a starting material. The reaction products contain single-crystalline or twinned nanodiamonds with average diameters in the 2-3 nm range. Theoretical calculations prove that, at the nanoscale, sub-4 nm nanodiamonds may adopt a structure that is more stable than graphene-oxide and nitrated polycyclic aromatic hydrocarbons. Our findings show that sp2 carbon in the polycyclic aromatic precursor can be converted to sp3 carbon under unexpectedly moderate temperature conditions by using nanoscale precursors and thus offer a low-temperature approach for the synthesis of sub-4 nm nanodiamonds.Nanodiamonds are interesting materials from the point of view of their biocompatibility and their chemical, spectroscopic, and mechanical properties. Current synthetic methods for nanodiamonds involve harsh environments, which are potentially hazardous in addition to being expensive. We report a low-temperature (423 K) hydrothermal approach to form nanodiamonds by using graphene-oxide or nitrated polycyclic aromatic hydrocarbons (naphthalene, anthracene, phenanthrene, or pyrene) as a starting material. The reaction products contain single-crystalline or twinned nanodiamonds with average diameters in the 2-3 nm range. Theoretical calculations prove that, at the nanoscale, sub-4 nm nanodiamonds may adopt a structure that is more stable than graphene-oxide and nitrated polycyclic aromatic hydrocarbons. Our findings show that sp2 carbon in the polycyclic aromatic precursor can be converted to sp3 carbon under unexpectedly moderate temperature conditions by using nanoscale precursors and thus offer a low-temperature approach for the synthesis of sub-4 nm nanodiamonds.
Author Sun, Litao
Banhart, Florian
Zhou, Yilong
Ni, Zhenhua
Bi, Hengchang
Zhang, Qiubo
Cheng, Shaobo
Botton, Gianluigi A
Ruoff, Rodney S
Su, Shi
Xu, Tao
He, Longbing
Shen, Yuting
Yin, Kuibo
Ding, Feng
Zhao, Wen
Wan, Shu
Wang, Liang
Chen, Linjiang
AuthorAffiliation Department of Chemistry
Institut de Physique et Chimie des Matériaux de Strasbourg (IPCMS)
Department of Materials Science and Engineering and Canadian Centre for Electron Microscopy
McMaster University
School of Materials Science and Engineering
Center for Multidimensional Carbon Materials (CMCM)
SEU−FEI Nano−Pico Center, Key Lab of MEMS of Ministry of Education, Collaborative Innovation Center for Micro/Nano Fabrication, Device and System
Nanjing Vocational University of Industry Technology
Institute of Nanochemistry and Nanobiology
Institute for Basic Science (IBS)
School of Aeronautic Engineering
Department of Physics
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Title Sub‑4 nm Nanodiamonds from Graphene-Oxide and Nitrated Polycyclic Aromatic Hydrocarbons at 423 K
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