Suchergebnisse - Operando diffraction
-
1
In Operando Synchrotron Diffraction and in Operando X-ray Absorption Spectroscopy Investigations of Orthorhombic V2O5 Nanowires as Cathode Materials for Mg-Ion Batteries
ISSN: 1520-5126, 1520-5126Veröffentlicht: 13.02.2019Veröffentlicht in Journal of the American Chemical Society (13.02.2019)“… In operando synchrotron diffraction and in operando X-ray absorption spectroscopy together with ex situ Raman and X-ray photoelectron spectroscopy reveal the reversibility of magnesium insertion …”
Weitere Angaben
Journal Article -
2
Slab-Gliding-Induced Structural Evolution in β‑V2O5 Enables Reversible High Na-Ion Storage: A Combined Operando Synchrotron Diffraction and Operando XAS Study
ISSN: 0897-4756Veröffentlicht: 11.11.2025Veröffentlicht in Chemistry of materials (11.11.2025)“… -V2O5 during sodium intercalation. Operando synchrotron diffraction and operando X-ray absorption spectroscopy together with X-ray photoelectron spectroscopy, reveal the reversibility of sodium (de …”
Weitere Angaben
Journal Article -
3
ID15A at the ESRF – a beamline for high speed operando X‐ray diffraction, diffraction tomography and total scattering
ISSN: 1600-5775, 0909-0495, 1600-5775Veröffentlicht: 5 Abbey Square, Chester, Cheshire CH1 2HU, England International Union of Crystallography 01.03.2020Veröffentlicht in Journal of synchrotron radiation (01.03.2020)“… ID15A is a newly refurbished beamline at the ESRF devoted to operando and time‐resolved diffraction and imaging, total scattering and diffraction computed tomography …”
Volltext
Journal Article -
4
Real-time observations of lithium battery reactions—operando neutron diffraction analysis during practical operation
ISSN: 2045-2322, 2045-2322Veröffentlicht: London Nature Publishing Group UK 30.06.2016Veröffentlicht in Scientific reports (30.06.2016)“… Here, we report an operando diffraction technique that uses high-intensity neutrons to detect reactions in non-equilibrium states driven by high-current operation in commercial 18650 cells …”
Volltext
Journal Article -
5
Slab-Gliding-Induced Structural Evolution in β‑V 2 O 5 Enables Reversible High Na-Ion Storage: A Combined Operando Synchrotron Diffraction and Operando XAS Study
ISSN: 0897-4756Veröffentlicht: United States 11.11.2025Veröffentlicht in Chemistry of materials (11.11.2025)“… -V O during sodium intercalation. synchrotron diffraction and X-ray absorption spectroscopy together with X-ray photoelectron spectroscopy, reveal the reversibility of sodium (de …”
Weitere Angaben
Journal Article -
6
Metastable precursor structures in hydrogen-infused super duplex stainless steel microstructure – An operando diffraction experiment
ISSN: 0010-938X, 1879-0496, 1879-0496Veröffentlicht: Amsterdam Elsevier Ltd 01.11.2020Veröffentlicht in Corrosion science (01.11.2020)“… Grazing-incidence x-ray diffraction was employed to monitor, operando, the lattice degradation of the austenite and ferrite phases …”
Volltext
Journal Article -
7
Phase Transformation Behavior and Stability of LiNiO2 Cathode Material for Li‐Ion Batteries Obtained from In Situ Gas Analysis and Operando X‐Ray Diffraction
ISSN: 1864-5631, 1864-564X, 1864-564XVeröffentlicht: Weinheim Wiley Subscription Services, Inc 21.05.2019Veröffentlicht in ChemSusChem (21.05.2019)“… In this work, the multistep phase transformation process and associated effects are analyzed by galvanostatic cycling, operando X …”
Volltext
Journal Article -
8
Nature of Li2O2 oxidation in a Li-O2 battery revealed by operando X-ray diffraction
ISSN: 1520-5126, 1520-5126Veröffentlicht: United States 19.11.2014Veröffentlicht in Journal of the American Chemical Society (19.11.2014)“… ) remains less understood. Here, using operando X-ray diffraction, we show that oxidation of electrochemically generated Li2O2 occurs in two stages, but in one step for bulk crystalline (commercial …”
Weitere Angaben
Journal Article -
9
5D operando tomographic diffraction imaging of a catalyst bed
ISSN: 2041-1723, 2041-1723Veröffentlicht: London Nature Publishing Group UK 12.11.2018Veröffentlicht in Nature communications (12.11.2018)“… We report the results from the first 5D tomographic diffraction imaging experiment of a complex Ni–Pd/CeO 2 …”
Volltext
Journal Article -
10
Suppression of Electrochemically Driven Phase Transitions in Nanostructured MoS2 Pseudocapacitors Probed Using Operando X‑ray Diffraction
ISSN: 1936-0851, 1936-086X, 1936-086XVeröffentlicht: American Chemical Society 26.02.2019Veröffentlicht in ACS nano (26.02.2019)“… Quantitative electrochemistry demonstrated that the current response is capacitive. In this work, we perform a series of operando X-ray diffraction studies upon …”
Volltext
Journal Article -
11
Revealing Lattice Expansion of Small-Pore Zeolite Catalysts during the Methanol-to-Olefins Process Using Combined Operando X-ray Diffraction and UV-vis Spectroscopy
ISSN: 2155-5435, 2155-5435Veröffentlicht: United States 02.03.2018Veröffentlicht in ACS catalysis (02.03.2018)“… °C was followed using operando UV-vis spectroscopy. During the same experiment, using operando X-ray Diffraction (XRD …”
Weitere Angaben
Journal Article -
12
Effect of Temperature on Intermediate Phases of Na3V2(PO4)3 during Cycling by Operando X-ray Diffraction
ISSN: 1944-8252, 1944-8252Veröffentlicht: 30.10.2024Veröffentlicht in ACS applied materials & interfaces (30.10.2024)“… In this study, the performance of NVP at low, room, and high temperatures during cycling is thoroughly investigated using synchrotron operando X-ray diffraction. The (de …”
Weitere Angaben
Journal Article -
13
IGUAPE, a graphical user interface for in situ/operando X‐ray diffraction experiments at the PAINEIRA beamline: development and application
ISSN: 1600-5767, 0021-8898, 1600-5767Veröffentlicht: 5 Abbey Square, Chester, Cheshire CH1 2HU, England International Union of Crystallography 01.06.2025Veröffentlicht in Journal of applied crystallography (01.06.2025)“… Synchrotron radiation X‐ray diffraction facilities equipped with fast area detectors can generate X‐ray diffraction (XRD …”
Volltext
Journal Article -
14
High-Performance Li-Ion Batteries Using Nickel-Rich Lithium Nickel Cobalt Aluminium Oxide-Nanocarbon Core-Shell Cathode: In Operando X-ray Diffraction
ISSN: 1944-8252, 1944-8252Veröffentlicht: United States 28.08.2019Veröffentlicht in ACS applied materials & interfaces (28.08.2019)“… X-ray diffraction studies show that both materials experience anisotropic structural change, i.e …”
Weitere Angaben
Journal Article -
15
Operando Synchrotron X-ray Diffraction in Calcium Batteries: Insights into the Redox Activity of 1D Ca3CoMO6 (M = Co and Mn)
ISSN: 0887-0624Veröffentlicht: 01.07.2021Veröffentlicht in Energy & fuels (01.07.2021)“… high-energy battery technologies and were investigated by operando synchrotron X-ray diffraction …”
Weitere Angaben
Journal Article -
16
A 3D free-standing lithiophilic silver nanowire aerogel for lithium metal batteries without lithium dendrites and volume expansion: in operando X-ray diffraction
ISSN: 1364-548X, 1364-548XVeröffentlicht: England 14.05.2019Veröffentlicht in Chemical communications (Cambridge, England) (14.05.2019)“… A 3D free-standing lithiophilic silver nanowire aerogel (AgNWA) can stop the dendritic growth of lithium metal at the initial nucleation process. The 3D …”
Weitere Angaben
Journal Article -
17
Insights into Structural Transformations in the Local Structure of Li2VO2F Using Operando X-ray Diffraction and Total Scattering: Amorphization and Recrystallization
ISSN: 1944-8252, 1944-8252Veröffentlicht: 17.06.2020Veröffentlicht in ACS applied materials & interfaces (17.06.2020)“… Disordered rock salt Li2VO2F cathode material for lithium-ion batteries was investigated using operando X-ray diffraction and total scattering to gain insight into the structural changes of the short …”
Weitere Angaben
Journal Article -
18
Commercial Sodium‐Ion Batteries: Understanding Mechanism and Function Using In Operando Neutron Diffraction and X‐Ray Tomography Studies
ISSN: 1616-301X, 1616-3028Veröffentlicht: 14.10.2025Veröffentlicht in Advanced functional materials (14.10.2025)“… In this study, X‐ray diffraction (XRD) and energy‐dispersive X‐ray spectroscopy confirm the presence of O3 …”
Volltext
Journal Article -
19
The Origin of Capacity Fade in the Li2MnO3·LiMO2 (M = Li, Ni, Co, Mn) Microsphere Positive Electrode: An Operando Neutron Diffraction and Transmission X-ray Microscopy Study
ISSN: 1520-5126Veröffentlicht: United States 20.07.2016Veröffentlicht in Journal of the American Chemical Society (20.07.2016)“… of operando neutron powder diffraction and transmission X-ray microscopy methods, enabling the phase …”
Weitere Angaben
Journal Article -
20
Universal phase dynamics in VO2 switches revealed by ultrafast operando diffraction
ISSN: 1095-9203, 1095-9203Veröffentlicht: 16.07.2021Veröffentlicht in Science (American Association for the Advancement of Science) (16.07.2021)“… Using stroboscopic electron diffraction, we perform synchronized time-resolved measurements of atomic motions and electronic transport in operating vanadium dioxide (VO2) switches …”
Weitere Angaben
Journal Article